WO1992004097A1 - Electrostatically dissipative fuel filter - Google Patents
Electrostatically dissipative fuel filter Download PDFInfo
- Publication number
- WO1992004097A1 WO1992004097A1 PCT/US1990/006983 US9006983W WO9204097A1 WO 1992004097 A1 WO1992004097 A1 WO 1992004097A1 US 9006983 W US9006983 W US 9006983W WO 9204097 A1 WO9204097 A1 WO 9204097A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- fuel
- housing
- electrically conductive
- common electrical
- fibers
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D27/00—Cartridge filters of the throw-away type
- B01D27/08—Construction of the casing
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F02—COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
- F02M—SUPPLYING COMBUSTION ENGINES IN GENERAL WITH COMBUSTIBLE MIXTURES OR CONSTITUENTS THEREOF
- F02M37/00—Apparatus or systems for feeding liquid fuel from storage containers to carburettors or fuel-injection apparatus; Arrangements for purifying liquid fuel specially adapted for, or arranged on, internal-combustion engines
- F02M37/22—Arrangements for purifying liquid fuel specially adapted for, or arranged on, internal-combustion engines, e.g. arrangements in the feeding system
- F02M37/32—Arrangements for purifying liquid fuel specially adapted for, or arranged on, internal-combustion engines, e.g. arrangements in the feeding system characterised by filters or filter arrangements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2201/00—Details relating to filtering apparatus
- B01D2201/04—Supports for the filtering elements
- B01D2201/0461—Springs
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2201/00—Details relating to filtering apparatus
- B01D2201/50—Means for dissipating electrostatic charges
Definitions
- This invention relates to a fuel filter for use in the fuel line that delivers fuel to a motor vehicle engine.
- the housings for filters used to filter the fuel delivered to a motor vehicle engine have commonly been made of metal or a polymer material, such as Nylon 12.
- non-metallic fuel filters are preferred. Such non-metallic fuel filters have been commonly used on vehicles having carbureted engines without problems for many years. However, when such prior art non-metallic fuel filters were used on vehicles equipped with electronic fuel injection (EFI) systems, the non-metallic material occasionally broke down and started leaking.
- EFI electronic fuel injection
- a fuel filter for a motor vehicle is made from a moldable material which may be safely used in vehicles equipped with electronic fuel injection system.
- a fuel filter generally indicated by the numeral 10 includes a housing 12 which is manufactured from a material which is non-conductive, such as Nylon 12 or another polymer material to which a conductive filler has been added, as will hereinafter be described.
- the housing 12 is equipped with an inlet fitting 14 and outlet fitting 16.
- the inlet fitting 14 and outlet fitting 16 are connected into the fuel line which delivers fuel from the fuel tank to the engine.
- the fuel line may also be made of a non-conductive material.
- a filter element generally indicated by the numeral 18 is mounted within the housing 12 to filter fuel communicated through the fuel line.
- Element 18 includes a ⁇ conventional circumferentially extending array of pleated filter media generally indicated by the numeral 20.
- the pleats forming the filtering media 20 define outer tips 22 and inner tips 24.
- a closed end cap 26 closes the end of the element 18 adjacent to inlet fitting 14 snd bridges across the inner cavity 28 defined within the array of media 20.
- a circumferentially extending band of sealing material 30 is dispensed into the end cap 26, and seals the edges of the pleats comprising the media 20 to prevent bypass of fuel around the ends of the pleats.
- a corresponding circumferentially extending band of sealing material 32 is dispensed in end cap 34 which closes the opposite end of the inner cavity 28.
- the sealing material 32 seals the opposite edges of the pleats comprising the media 20.
- the outlet fitting 16 extends through the end cap 34 to communicate with the inner cavity 28.
- a spring 36 is disposed in the inner cavity 28 and engages the inner tips 24 of the media 20 to prevent inward collapse of the media.
- the housing 12 is secured to the metal vehicle body, a portion of which is indicated at 38, by a bracket 40.
- the bracket 40 may be either a separate metallic member attached to the housing 12 or molded as a part of the housing 12 from the same material used for the housing 12. Accordingly, fuel communicated into the inlet fitting 14 is received in inlet cavity 42 which is defined between the element 18 and the housing 12. Fuel in the inlet cavity 42 communicates through the media 20 into the inner or outlet cavity 28 which is communicated directly with the outlet fitting 16.
- the charge generation due to the impact of the hydrocarbon paraffin against the media 20 may be as much as several orders of magnitude higher than the generation taking place in the lines themselves.
- the magnitude of the charge generated in the inlet cavity 42 will also be a function of the flow rate through the housing 12. In fact, as studies have shown, the charge generation in the inlet chamber 42 is almost directly proportional to the flow rate through the filter media 20. Accordingly, fuel filters used in recirculatory fueling systems, such as electronic fuel injection systems where flows through the fuel line are substantially higher than flows in older carbureted systems, will generate a proportionally higher charge level in the inlet chamber 42.
- the charge generated in the inlet cavity 42 would be evenly distributed about the filter. Accordingly, the charge would then be evenly dissipated or passed through the filter.
- a grounding plane is within "striking distance ** of the electrostatic charge in the inlet cavity 42, a discharge takes place from the portion of housing 12 closest to the plane 38 whenever the charges in the cavity 42 exceed the strength of the dielectric between the inlet cavity 42 through the housing 12 to the grounding plane.
- the grounding plane is provided by the body of the vehicle indicated at 38.
- the grounding is effected by connecting the body to the negative terminal of the vehicle battery. This provides a grounding plane that is slightly positive with respect to an earth ground. Since the grounding plane provided by the body 38 is slightly positive, the charges in the inlet cavity 42 will be attracted towards the body 38. Accordingly, the charges will be concentrated in that part of the cavity 42 closest to the body 38. Tests have shown that electrical charges move around a curved body, such as the housing 12, much more easily than in bodies having other shapes.
- the voltage level of an electrostatic charge in that portion of the inlet chamber 42 closest to the body 38 may be as high as 8kV to lOkV. Since the dielectric strength between the cavity 42 and the body 38 is approximately 7kV, the dielectric begins to allow the charge to pass through the material of the housing 12 when the voltage level of the electrostatic charge exceeds
- the material of which the housing 12 is made is required to absorb a portion of the energy associated with the charge. If the charge was evenly distributed about the housing 12, the strength of the material would exceed the absorption energy during the lifetime of the filter, but as discussed above, most of the charge is concentrated in that part of the cavity 42 5 closest to the body 38. When a grounding plane, such as the body 38, is within "striking** distance of a charged body, the plane itself is a target for electron current flow. The energy which makes up the charge will then no longer pass through the body in an evenly distributed 10 manner. This absorption of energy breaks down the material of which the housing 12 is made and results in microscopic pin holes in the housing 12. When a large concentration of these pin holes occurs in a small area, the material comprising the housing 12 breaks down and the • j c housing leaks. Tests have shown that the striking distance is always less than or equal to the radius of the curved body.
- an electrically conductive path is provided between the fuel within the inlet cavity 42 and the body 38. Accordingly, 0 the electrostatic buildup in the cavity 42 will be discharged through the electrically conductive path in bracket 40 to the body 38, thus avoiding the aforementioned material erosion that causes leaks.
- An electrical path through the housing 12 is most easily 5 provided by incorporating small amounts of a conductive filler material in the base Nylon 12 material, thus making the housing electrically conductive while substantially retaining the moldability and other desirable properties of the polymer material. 0
- Stainless steel fiber product with a high aspect ratio was selected as the filler material.
- Stainless steel also has the advantage of requiring smaller quantities for 5 providing the required conductivity than other conductive fillers, such as carbon black, metal flakes and powders, and metallized microspheres which possess small aspect ratios.
- Stainless steel fibers used in this application have a preferable upper limit on fiber diameter of about 8 microns. This small diameter, coupled with the low loadings of filler used, allows the matrix to stretch freely between and around fibers as long as the filler is properly compounded into the base resin. This reduces dewetting and disbonding between the filler and base resin, thus preventing cavitation under stress.
- Stainless steel also presents itself as a filler around which the base Nylon 12 material bonds to itself.
- Other electrically conductive fillers such as the aforementioned carbon, act as stress concentrators and, at the relatively high filler loadings required to achieve conductivity, restrict the ability of the resin matrix to yield under stress.
- the stainless steel fibers are ductile and non-rigid unlike straight or metallized carbon fibers or metallized inorganic fibers and whiskers. This allows stainless steel fibers to maintain their integrity better during melt-processing. Unlike the non-metallic fibers, stainless steel fibers also do not increase mechanical strength or stiffness of the base resin significantly. Other metal fibers with high aspect ratios can be satisfactorily substituted for stainless steel.
- the aspect ratio of the stainless steel fibers used must be large enough to easily conduct electricity at low loadings, but small enough to be easily molded with the base polymer material into the final part. Accordingly, stainless steel fibers having a diameter of about 8 microns and a nominal length of from 4-6 mm were selected. Longer steel fibers can also be used depending on design of the filter. The longest fiber length dictated by part design and moldability should be used in order to minimize filler usage.
- the stainless steel in the composite material is about 3% to 9% by weight, of the composite material, which is sufficient to provide a density of about 8 grams of stainless steel fibers per cubic centimeter of material, which provides volume and
- the stainless steel fibers should preferably be coated with small amounts of coupling agents like organofunctional silane or titanate compounds.
- graft or block copolymers with amide functional groups can also be used as coupling agents.
- small amounts of polymers with affinity for metal ' surfaces and having good compatibility with polyamides can be used. These interfacial agents help in wetting and increasing interfacial bonding through formation of molecular metal-polymer matrix bridges.
- mold-release agents, internal lubricants, and impact modifiers can be used to improve physical properties of the stainless-fiber filled resin.
Abstract
Description
Claims
Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP91901157A EP0545924B1 (en) | 1990-08-30 | 1990-11-15 | Electrostatically dissipative fuel filter |
KR1019930700595A KR0137117B1 (en) | 1990-08-30 | 1990-11-15 | Electrostatically dissipative fuel filter |
CA002089647A CA2089647C (en) | 1990-08-30 | 1990-11-15 | Electrostatically dissipative fuel filter |
DE69016464T DE69016464T2 (en) | 1990-08-30 | 1990-11-15 | ELECTROSTATICALLY DIVERSE FUEL FILTER. |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07575260 US5076920B2 (en) | 1990-08-30 | 1990-08-30 | Electrostatically dissipative fuel filter |
US575,260 | 1990-08-30 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO1992004097A1 true WO1992004097A1 (en) | 1992-03-19 |
Family
ID=24299574
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US1990/006983 WO1992004097A1 (en) | 1990-08-30 | 1990-11-15 | Electrostatically dissipative fuel filter |
Country Status (9)
Country | Link |
---|---|
US (3) | US5076920B2 (en) |
EP (1) | EP0545924B1 (en) |
JP (1) | JP2612657B2 (en) |
AU (1) | AU642616B2 (en) |
CA (1) | CA2089647C (en) |
DE (1) | DE69016464T2 (en) |
ES (1) | ES2067917T3 (en) |
NZ (1) | NZ239064A (en) |
WO (1) | WO1992004097A1 (en) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1997003744A1 (en) * | 1995-07-18 | 1997-02-06 | Parker-Hannifin Corporation | Conductive filter element |
US5642718A (en) * | 1995-07-18 | 1997-07-01 | Nippondenso Co., Ltd. | In-tank fuel pump apparatus having improved structure for dissipating electrostatic charges |
DE19813204A1 (en) * | 1998-03-25 | 1999-09-30 | Bosch Gmbh Robert | Flange of a fuel delivery module and fuel delivery module |
DE19925098A1 (en) * | 1999-06-01 | 2000-12-07 | Bosch Gmbh Robert | Disposable filter for fuel |
US7927400B2 (en) | 2008-04-03 | 2011-04-19 | Cummins Filtration Ip, Inc. | Static dissipative filtration media |
CN105804905A (en) * | 2016-05-13 | 2016-07-27 | 安徽机电职业技术学院 | Electric spraying filter |
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---|---|---|---|---|
US6132645A (en) * | 1992-08-14 | 2000-10-17 | Eeonyx Corporation | Electrically conductive compositions of carbon particles and methods for their production |
US5498372A (en) * | 1992-08-14 | 1996-03-12 | Hexcel Corporation | Electrically conductive polymeric compositions |
US5382359A (en) * | 1993-05-13 | 1995-01-17 | Parr Manufacturing, Inc. | Plastic fuel filter with conductive coating for providing an evaporative barrier and for dissipating electrostatic charges |
US5380432A (en) * | 1993-05-13 | 1995-01-10 | Parr Manufacturing, Inc. | Fuel filter with electrostatic charge preventing media |
DE4329898A1 (en) | 1993-09-04 | 1995-04-06 | Marcus Dr Besson | Wireless medical diagnostic and monitoring device |
KR100302448B1 (en) * | 1994-11-04 | 2002-07-02 | 오카메 히로무 | Fuel supply |
KR100300739B1 (en) * | 1995-02-03 | 2002-07-03 | 오카메 히로무 | Fuel supply system |
JP3689935B2 (en) * | 1995-07-13 | 2005-08-31 | 株式会社デンソー | Filter element |
IL119432A0 (en) * | 1996-10-16 | 1997-01-10 | I R D Fuel Technologies Ltd | Filter for separating water from fuel |
JP3382808B2 (en) * | 1997-02-07 | 2003-03-04 | 株式会社日立ユニシアオートモティブ | Fuel supply device |
EP0969200B1 (en) | 1997-03-11 | 2004-02-11 | Aisan Kogyo Kabushiki Kaisha | In-tank fuel filter improved to resist electrification |
DE19712155A1 (en) * | 1997-03-22 | 1998-09-24 | Bosch Gmbh Robert | Fuel supply system |
FR2765632B1 (en) * | 1997-07-03 | 1999-09-24 | Marwal Systems | FUEL PUMP DEVICE FOR A MOTOR VEHICLE TANK |
JPH11200974A (en) * | 1998-01-07 | 1999-07-27 | Denso Corp | Fuel filter in-tank type fuel pump employing it |
JP3517773B2 (en) * | 1998-04-07 | 2004-04-12 | 豊田合成株式会社 | Resin fitting for fuel hose |
JP3956533B2 (en) | 1998-08-19 | 2007-08-08 | 株式会社デンソー | Fuel filtration device |
DE19844559A1 (en) * | 1998-09-29 | 2000-03-30 | Bosch Gmbh Robert | Fuel filter |
US6171492B1 (en) | 1999-02-04 | 2001-01-09 | Purolator Products Company | Filter for liquid fuel |
US6253463B1 (en) * | 1999-04-26 | 2001-07-03 | Niro A/S | Method of spray drying |
US6293410B1 (en) | 1999-06-29 | 2001-09-25 | Mahle-Parr Filter Systems, Inc. | No-cure fuel filter and method for making same |
KR20010047475A (en) * | 1999-11-20 | 2001-06-15 | 이계안 | Housing of fuel filter for automobile |
EP1235626B1 (en) | 1999-11-23 | 2007-04-04 | Pall Corporation | Conductive filter cartridge |
US6379564B1 (en) | 2000-05-08 | 2002-04-30 | Ronald Paul Rohrbach | Multi-stage fluid filter, and methods of making and using same |
US6651823B1 (en) | 2000-05-15 | 2003-11-25 | Honeywell International Inc. | Plastic filter housing formed from multiple sections and having a skewed weld seam, and filter incorporating same |
US6464870B1 (en) | 2000-08-08 | 2002-10-15 | Kuss Corporation | Filter assembly having plastic mesh conductive surround |
US6685854B2 (en) * | 2001-04-10 | 2004-02-03 | Honeywell International, Inc. | Electrically conductive polymeric mixture, method of molding conductive articles using same, and electrically conductive articles formed therefrom |
US6805383B2 (en) | 2001-11-12 | 2004-10-19 | Itt Manufacturing Enterprises, Inc. | Fluid quick connector with secure electrical contact |
US6755675B2 (en) | 2001-11-12 | 2004-06-29 | Itt Manufacturing Enterprises, Inc. | Fluid quick connector with secure electrical ground contact |
US6589420B1 (en) * | 2002-02-21 | 2003-07-08 | Mathson Industries | Fuel filter housing |
US6877373B2 (en) * | 2002-05-31 | 2005-04-12 | Ti Group Automotive Systems, Llc | Electrostatic charge control for in-tank modules |
WO2004073831A1 (en) * | 2003-02-19 | 2004-09-02 | Robert Joseph Scilinato | Axial depth filter |
US6920031B2 (en) * | 2003-04-24 | 2005-07-19 | Velcon Filters, Inc. | Static charge neutralizer |
US20050263202A1 (en) * | 2004-05-20 | 2005-12-01 | Cheng Paul P | Polymeric fuel system components |
US20060000454A1 (en) * | 2004-07-02 | 2006-01-05 | Visteon Global Technologies, Inc. | In-tank fuel supply unit having long life filter |
WO2006056533A1 (en) * | 2004-11-22 | 2006-06-01 | Mann+Hummel Gmbh | Filter, in particular for filtering fuel |
US7558044B2 (en) * | 2005-02-04 | 2009-07-07 | George Kent J | Static electricity eliminator |
US7527042B2 (en) * | 2005-04-05 | 2009-05-05 | Ti Group Automotive Systems, Llc | Electrostatic charge control for in-tank fuel module components |
US7467549B2 (en) * | 2005-04-05 | 2008-12-23 | Ti Group Automotive Systems, Llc | Electrostatic charge control for in-tank fuel module components |
US20070114165A1 (en) * | 2005-11-21 | 2007-05-24 | Buczynsky Andrew E | Fuel filter |
US7866711B2 (en) | 2006-08-22 | 2011-01-11 | Ti Group Automotive Systems, Llc | Quick connector with conductive path |
GB2450735B (en) * | 2007-07-05 | 2012-11-28 | Air Safety Ltd | Air filter assembly |
DE102007054857A1 (en) * | 2007-11-16 | 2009-05-20 | Continental Automotive Gmbh | Fuel delivery unit |
HUP1000158A2 (en) | 2010-03-24 | 2011-11-28 | Visteon Global Technologies | Fuel filter for motor vehicle |
DE102011078467A1 (en) | 2011-06-30 | 2013-01-03 | Robert Bosch Gmbh | Plastic housing |
WO2014093055A1 (en) | 2012-12-13 | 2014-06-19 | Ticona Llc | Laser-weldable electrostatically dissipative polyoxymethylene based on stainless steel fibers |
EP2938673B1 (en) | 2012-12-27 | 2018-10-03 | Ticona LLC | Conductive polyoxymethylene based on stainless steel fibers |
US9458810B2 (en) | 2013-02-06 | 2016-10-04 | GM Global Technology Operations LLC | Fuel module with electrostatic discharge mitigation |
DE102013220153A1 (en) | 2013-10-04 | 2015-04-09 | Mahle International Gmbh | Filter device for a motor vehicle |
CN103557040B (en) * | 2013-10-30 | 2016-03-23 | 中国航空动力机械研究所 | Automatic discharge equipment |
CN103552525B (en) * | 2013-11-12 | 2015-07-29 | 上海大众汽车有限公司 | Anti-electrostatic discharge structure for gasoline filter of automobile and method |
US10876606B2 (en) * | 2018-03-13 | 2020-12-29 | Gates Corporation | Orbital tensioner |
WO2020226911A1 (en) * | 2019-05-03 | 2020-11-12 | Entegris, Inc. | Filter with electrostatic discharge mitigation sleeve |
US11333223B2 (en) | 2019-08-06 | 2022-05-17 | Gates Corporation | Orbital tensioner |
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FR1541025A (en) * | 1967-08-01 | 1968-10-04 | Prec Mecanique Labinal | Improvements to filters, in particular of the replaceable type, and more especially of plastic |
EP0176866A2 (en) * | 1984-09-20 | 1986-04-09 | Mitsubishi Rayon Co., Ltd. | Electromagnetic interference-shielding, flame-retardant ABS resin compostion |
DE3918342C1 (en) * | 1989-06-06 | 1990-06-07 | Knecht Filterwerke Gmbh, 7000 Stuttgart, De |
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1990
- 1990-08-30 US US07575260 patent/US5076920B2/en not_active Expired - Lifetime
- 1990-11-15 ES ES91901157T patent/ES2067917T3/en not_active Expired - Lifetime
- 1990-11-15 WO PCT/US1990/006983 patent/WO1992004097A1/en active IP Right Grant
- 1990-11-15 JP JP3501562A patent/JP2612657B2/en not_active Expired - Lifetime
- 1990-11-15 CA CA002089647A patent/CA2089647C/en not_active Expired - Lifetime
- 1990-11-15 DE DE69016464T patent/DE69016464T2/en not_active Expired - Lifetime
- 1990-11-15 EP EP91901157A patent/EP0545924B1/en not_active Expired - Lifetime
- 1990-11-15 AU AU69161/91A patent/AU642616B2/en not_active Expired
-
1991
- 1991-07-01 US US07724240 patent/US5164879B1/en not_active Expired - Lifetime
- 1991-07-01 US US07724223 patent/US5164084B2/en not_active Expired - Lifetime
- 1991-07-22 NZ NZ239064A patent/NZ239064A/en not_active IP Right Cessation
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Publication number | Priority date | Publication date | Assignee | Title |
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FR1541025A (en) * | 1967-08-01 | 1968-10-04 | Prec Mecanique Labinal | Improvements to filters, in particular of the replaceable type, and more especially of plastic |
EP0176866A2 (en) * | 1984-09-20 | 1986-04-09 | Mitsubishi Rayon Co., Ltd. | Electromagnetic interference-shielding, flame-retardant ABS resin compostion |
DE3918342C1 (en) * | 1989-06-06 | 1990-06-07 | Knecht Filterwerke Gmbh, 7000 Stuttgart, De |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1997003744A1 (en) * | 1995-07-18 | 1997-02-06 | Parker-Hannifin Corporation | Conductive filter element |
US5642718A (en) * | 1995-07-18 | 1997-07-01 | Nippondenso Co., Ltd. | In-tank fuel pump apparatus having improved structure for dissipating electrostatic charges |
US6099726A (en) * | 1995-07-18 | 2000-08-08 | Parker-Hannifin Corporation | Static dissipating filter cartridge with conductive resilient seal |
DE19813204A1 (en) * | 1998-03-25 | 1999-09-30 | Bosch Gmbh Robert | Flange of a fuel delivery module and fuel delivery module |
DE19925098A1 (en) * | 1999-06-01 | 2000-12-07 | Bosch Gmbh Robert | Disposable filter for fuel |
US7927400B2 (en) | 2008-04-03 | 2011-04-19 | Cummins Filtration Ip, Inc. | Static dissipative filtration media |
US8080086B2 (en) | 2008-04-03 | 2011-12-20 | Kuss Filtration Inc. | Static dissipative filtration media |
CN105804905A (en) * | 2016-05-13 | 2016-07-27 | 安徽机电职业技术学院 | Electric spraying filter |
Also Published As
Publication number | Publication date |
---|---|
US5164879B1 (en) | 1998-09-08 |
US5164879A (en) | 1992-11-17 |
US5164084B2 (en) | 1998-05-05 |
NZ239064A (en) | 1993-11-25 |
US5164084A (en) | 1992-11-17 |
US5076920A (en) | 1991-12-31 |
US5164084B1 (en) | 1995-03-28 |
AU642616B2 (en) | 1993-10-21 |
DE69016464T2 (en) | 1995-10-05 |
CA2089647A1 (en) | 1992-03-01 |
CA2089647C (en) | 2001-04-17 |
EP0545924B1 (en) | 1995-01-25 |
EP0545924A1 (en) | 1993-06-16 |
DE69016464D1 (en) | 1995-03-09 |
JPH06500373A (en) | 1994-01-13 |
US5076920B1 (en) | 1996-06-25 |
US5076920B2 (en) | 1998-05-05 |
ES2067917T3 (en) | 1995-04-01 |
JP2612657B2 (en) | 1997-05-21 |
AU6916191A (en) | 1992-03-30 |
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