WO1989005196A1 - Procede et equipement de microvaporisation de liquides, tels que de preference des metaux en fusion - Google Patents

Procede et equipement de microvaporisation de liquides, tels que de preference des metaux en fusion Download PDF

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Publication number
WO1989005196A1
WO1989005196A1 PCT/SE1988/000662 SE8800662W WO8905196A1 WO 1989005196 A1 WO1989005196 A1 WO 1989005196A1 SE 8800662 W SE8800662 W SE 8800662W WO 8905196 A1 WO8905196 A1 WO 8905196A1
Authority
WO
WIPO (PCT)
Prior art keywords
liquid
barrier
media
jet
gas
Prior art date
Application number
PCT/SE1988/000662
Other languages
English (en)
Inventor
Hans-Gunnar Larsson
Original Assignee
Hg Tech Ab
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hg Tech Ab filed Critical Hg Tech Ab
Priority to BR888807838A priority Critical patent/BR8807838A/pt
Priority to AT89900667T priority patent/ATE93750T1/de
Publication of WO1989005196A1 publication Critical patent/WO1989005196A1/fr
Priority to FI902863A priority patent/FI87053C/fi

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/02—Making metallic powder or suspensions thereof using physical processes
    • B22F9/06—Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08—Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082—Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B7/00—Spraying apparatus for discharge of liquids or other fluent materials from two or more sources, e.g. of liquid and air, of powder and gas
    • B05B7/02—Spray pistols; Apparatus for discharge
    • B05B7/08—Spray pistols; Apparatus for discharge with separate outlet orifices, e.g. to form parallel jets, i.e. the axis of the jets being parallel, to form intersecting jets, i.e. the axis of the jets converging but not necessarily intersecting at a point
    • B05B7/0807—Spray pistols; Apparatus for discharge with separate outlet orifices, e.g. to form parallel jets, i.e. the axis of the jets being parallel, to form intersecting jets, i.e. the axis of the jets converging but not necessarily intersecting at a point to form intersecting jets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/02—Making metallic powder or suspensions thereof using physical processes
    • B22F9/06—Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08—Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082—Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • B22F2009/088—Fluid nozzles, e.g. angle, distance

Definitions

  • a method and equipment for microatomizing liquids preferably melts
  • the present invention relates to a method of atomizing liquids, pre ⁇ ferably metal melts, in which liquid, preferably metal melt, is mixed into a media jet consisting of gas and/or liquid, so that the liquid is disintegrated into small particles, i.e. atomization is achieved.
  • the invention also relates to a means for performing said method.
  • Such atomization is effected by disintegration of a preferably vertical tapping stream, or other pool of liquid, with the aid of preferably horizontal or vertical media flows consisting of gas or liquid.
  • Powder-metallurgy processes using inertly manufactured powder encounter various problems relating to the size of the powder particles and/or their distribution. Finer and/or more restricted fractions of inertly manufactured powder are desirable for many applications nowadays. Such powder is conventionally obtained by screening off a coarser fraction, resulting in low yield, or via atomization processes using extreme gas flows and pressures. This powder is only used to a limited extent due to its high cost.
  • the size of particles formed in a certain volume element in the atomi ⁇ zation process is affected by a number of parameters.
  • the surface tension of the melt and the density and velocity of the atomizing medium are the most influencial parameters, besides the geometrical design of the atomization process.
  • a larger or smaller proportion of the melt will be disintegrated to particles in a region further away from the nozzle, where the velocity is considerably less, in some cases even as low at 10 % of the maximum velocity. This gives a coarse powder with a wide spread between the smallest and largest particles.
  • Another problem entails the difficulty of getting the atomizing medium to get a "grip" on the liquid, and a large quantity thus passes outside the actual atomizing region, with low effectivity as a result.
  • the method according to the invention aims at a solution of the problems mentioned above and others related thereto, and is characterised in that close to the blow-out nozzle, i.e. when velocity of the media jet is still high, a barrier is effected to spread said jet in order to greatly increase the contact surface between liquid/melt and media, at the same time producing greatly increased turbulence which is bene ⁇ ficial to the atomization process, and thus efficiently dispersing the liquid in the media whereupon the liquid is disintegrated into small particles, i.e. atomization is effectivized.
  • the atomization process takes place within a short distance of the nozzle, where the velocity of the atomizing medium is still high, as well as a large proportion of the gas participating in the atomizing process. A high degree of efficiency is thereby obtained.
  • This method thus enables a radical reduction in the average particle size and less spread in the size distribution, at low cost.
  • the barrier may consist of a solid body, possibly cooled by water, for instance, or of a material which is thermically and chemically resistant to the mixed jet.
  • the barrier may also be formed by a counter- directed media flow of gas and/or fluid, i.e. the barrier in this case constitutes the limit/contact surface between the mixed stream and the counter-directed media jet.
  • the method can be applied to both vertical and horizontal atomizing processes. With a suitable choice of barrier, it is even possible to atomize a steel melt or alloys with an even higher melting point.
  • the invention also relates to a means for performing said method, and the features characteristic of this means are defined in the appended claims.
  • the medium for the media flow or the counter-directed media flow may be water, some other liquid such as liquid gas, or only gas such as nitrogen or argon or mixtures thereof.
  • the barrier may consist of a stationary or rotating plate, or the gas being blown in can be rotated.
  • Figure 1 shows a means for performing the method according to the. invention
  • Figure 2a shows the actual atomization process with a gas barrier
  • Figure 2b shows an example of a nozzle producing the barrier
  • Figure 3 shows another embodiment of the barrier.
  • Figure 4 shows an alternative means for performing the method
  • Figure 5a shows the corresponding atomizing process with a gas barrier, seen from above
  • Figure 5b shows this process seen from the side with a detail of the nozzle producing the barrier
  • Figure 6 shows an alternative atomizing process.
  • a vertical atomizing chamber 1 having a casting box 2 for metal melt.
  • Media gas and/or fluid
  • a gas cooler 3 and a compressor to nozzles in the chamber 1.
  • Atomized powder is carried from the chamber 1 via a pipe system to a cyclone 5 for treatment and separation.
  • Metal melt e.g. steel
  • Metal melt is tapped from the casting box 2 ( Figure 2a) through a tapping arrangement in the bottom of this box, in the form of a preferably circular tapping stream 6 flowing vertically downwards into an atomizing chamber 1 filled with inert gas.
  • a gas nozzle 7 consisting of an annular nozzle or several smaller nozzles.
  • the nozzle(s) create(s) an annular gas curtain 9 around the tapping stream which encounters (8) the tappin stream at an acute angle, some way from the nozzle(s) 7.
  • the barrier 10 of the invention is located at a suitable distance below the point of encounter.
  • the barrier 10 consists of metals having a high melting point, such as steel, or preferably of a gas barrier 11. This is produced by directing a gas and/or fluid jet upwardly, preferably in the same centre line as the tapping stream and the gas curtain, at a suitable distance below the nozzle(s), i.e. a second jet is directed preferably immediately towards the first jet 9-6 which contains fragments of melt 13 in its central portion.
  • the velocity decreases in the region of the collision, and the pressure thus increases. Due to the increase in pressure, the gas expands radially outwards so that the velocity again increases. If the kinetic energy is equal in the two jets, the resulting direction will be substantially radial, i.e. perpen ⁇ dicular to the direction of the jets. The melt in the central portion of the first jet 13 will alter course in the collision region and will accompany the radially expanding gas, thus achieving efficient atomization.
  • the atomization process is further improved if the kinetic energy of the counter-directed jet is chosen less or greater than that of the first.
  • the expanding gas will assume a curved path, most resembling parabolic shape, ( Figure 2a).
  • the improved atomizing process is due to fragments of the melt drawn along with the gas are constantly forced to change direction, thus giving them greater exposure of the gas.
  • the kinetic energy in the counter-directed gas flow is advantageously chosen less than that in the first, thus producing the effect described above, while the overall direction of the gas/particle mixture will be obliquely downwards. If the ratio of kinetic energy is inverted the overall flow will be obliquely upwards.
  • the kinetic energy in the counter-directed jet may be 10 to 1000 % of the first, preferably 30 - 60 % .
  • the barrier may be obtained from a nozzle as shown in Figure 2b, with one or more central nozzles 14 for barrier jets.
  • auxiliar nozzles 15 can be arranged to prevent liquid (melt) from coming into contact with undesired parts of the barrier nozzle.
  • the barrier consists of a solid body, such as a circular plate located at right angles to and having the same central line as the mixed jet.
  • the compression of the gas thus occurs against this plate 16, after which expansion occurring radially outwards will pull with it a thin fi m o t.
  • this film of melt reaches the edge of the plate it will be disinte ⁇ grated into particles in a process similar to that described above.
  • the body constituting the barrier may be uncooled or cooled in some suitable manner from below, e.g. by means of water channels 17.
  • the bodies are uncooled, they should be made of a material which is thermically and chemically resistant to the hot melt and the gas. If the body is cooled, a protective layer will be formed against the hot metal by the metal nearest the plate solidifying.
  • the barrier may preferably have a geometry congruent with the cross section of the portion of the gas jet mixed with melt 13-
  • the size of the barrier is suitably such that its longitudinal dimensions are equal to the cross section of the part of the gas stream mixed with melt, at the point of encounter, or up to 20 times greater, preferably 4 to 10 times greater than said cross section.
  • a solid barrier (such as in Figure 3) may also be used, which is gradual melted and included in the atomized powder (not shown).
  • auxiliar nozzles suitably located, with the object of eliminating turbulence in critical areas, thus preventing molten particles from becoming attached.
  • auxiliar nozzles may have the appearance of those shown at 15 in Figure 2b, or at 18 in Figure 3-
  • Figure 4 shows a horizontal atomizing equipment with its atomizing chamber 19 and cyclone 20.
  • the atomizing equipment comprises a closed system, preferably kept under a certain overpressure (see Figures 1 and 4). This may be 500 mm water column, for instance, so that air is prevented from entering.
  • the casting box 2 is arranged at one end of the box (1, 19).
  • Figures 5a and 5b show atomization as performed in the equipment shown in Figure 4.
  • Medium 22 flows from nozzles 21 (for instance elongate, slot-shaped or a row or small nozzles) towards the tapping stream 23.
  • the mixed stream thus obtained then encounters a barrier (solid or produced by one or more nozzles 25) and is deflected thereby, thus producing excellent atomization.
  • the auxiliary nozzles are arranged in Figure 5b as one slot-shaped nozzle 26 and several small, separate nozzles 27. The nozzle 26 may even produce the barrier itself.
  • a flow phenomenum which arises when two jets of gas or fluid encounter each other at a certain angle is utilized to create the mixed jet 24 in Figures 5a-b.
  • Both these phenomena can be exploited by selecting an angle between two media jets 22, 22 so that a backward flow of media occurs and that, within a short distance, it is drawn back into the media jets by the injector action.
  • the result will be that a zone is formed in front of the intersection point, where there is no defined direction, but two vortex eddies with a constant exchange between returning media and media drawn in. Altering the angle will increase or decrease the extent of this zone.
  • the angle between the media jets may be 0 - 60 , but is preferably 5 - 20°.
  • the nozzles 21, 21 may be arranged to give two horizontally directed media jets, parallel in vertical equipment, with great extension verti ⁇ cally as compared with the width, and with an angle in the horizontal plane in relation to each other.
  • the zone described above will then be formed.
  • the tapping stream 23 will flow from the top, down in the vertical zone formed all along the height of the nozzle.
  • the stream will be successively disintegrated on its way. down, and mixed into the passing atomizing medium.
  • Media jets with considerable extension in one direction can be achieved by means of slot-shaped nozzles or by a number of circule nozzles, for instance, arranged close together in a row.
  • the nozzles for the media jets may be designed for sub-pressure or over-critical pressure conditions (Laval nozzle) .
  • the advantage of the arrangement of nozzles 21 described above is that a more homogeneous mixing (partial atomization) of the liquid into the media can be achieved which, even after passing a barrier, results in a narrower fraction for the particles.
  • the nozzle arrange ⁇ ment 21 can also be used for complete atomization, without a barrier, wereby particles can be produced within a narrow size interval but with a larger average particle size.
  • FIG. 6 shows an alternative embodiment of the method and means accordi to the invention.
  • An electric arc 30 is arranged between two electrodes 28, 29- Media streams 31 (gas and/or fluid) are directed towards the electric arc, and media jets from the opposite direction 32 act as barrier. Efficient atomization of the liquid 35 formed in the electric arc is obtained.
  • the liquid to be atomized is obtained from at least one of the electrodes 29.
  • liquid can also be obtained from a solid body which is melted by a laser or the like (not shown) in similar manner.
  • Feeding the electrodes in Figure 6 along, or the laser, can be arranged by means of a feeder 34.
  • the nozzles for both the first media and the barrier media may be annular, or may consist of several small nozzles.
  • the method according to Figure 6 is preferably carried out in a chamber similar to that described earlier (not shown). Particles formed at the atomization, at drawn into the gas jets towards the other end of the chamber, and before encountering the end of the chamber, they will have solidified to powder due to radiation and convective heat dissipation to the gas.
  • An outlet is arranged in the chamber, preferably at its end, towards which the gas/powder mixture flows.
  • the chamber is connected from the outlet by pipes, to a cyclone where the powder and gas are separated. After separation, the gas may travel to a compressor via a gas cooler, for recirculation to the atomizing nozzles.
  • the system includes other requisite valves, cooling equipment and control means for regulating gas pressure, temperature and the various media flows, etc.

Landscapes

  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
  • Nozzles (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Steroid Compounds (AREA)
  • Saccharide Compounds (AREA)

Abstract

La présente invention se rapporte à un procédé et à un moyen, qui servent à vaporiser des liquides tels que des métaux en fusion et dans lesquels un courant de coulée (6) du liquide rencontre un ou plusieurs jets (9) de milieux tels qu'un gaz et/ou un liquide. On dirige ensuite un courant mélangé obtenu vers une barrière (10) dans le but d'obtenir une dispersion effective du liquide dans les milieux, c'est-à-dire une vaporisation.
PCT/SE1988/000662 1987-12-09 1988-12-05 Procede et equipement de microvaporisation de liquides, tels que de preference des metaux en fusion WO1989005196A1 (fr)

Priority Applications (3)

Application Number Priority Date Filing Date Title
BR888807838A BR8807838A (pt) 1987-12-09 1988-12-05 Processo e equipamento para microatomizacao de liquidos,de preferencia materiais em fusao
AT89900667T ATE93750T1 (de) 1987-12-09 1988-12-05 Vorrichtung und verfahren zur mikroatomisierung von fluessigkeiten, insbesondere schmelzen.
FI902863A FI87053C (fi) 1987-12-09 1990-06-08 Foerfarande och apparatur foer att finfoerdela vaetskor, laempligen smaeltor

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
SE8704905-2 1987-12-09
SE8704905A SE462704B (sv) 1987-12-09 1987-12-09 Foerfarande vid atomisering av vaetskor och anordning foer genomfoerande av foerfarandet

Publications (1)

Publication Number Publication Date
WO1989005196A1 true WO1989005196A1 (fr) 1989-06-15

Family

ID=20370540

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/SE1988/000662 WO1989005196A1 (fr) 1987-12-09 1988-12-05 Procede et equipement de microvaporisation de liquides, tels que de preference des metaux en fusion

Country Status (9)

Country Link
EP (1) EP0419479B1 (fr)
JP (1) JP2703378B2 (fr)
AT (1) ATE93750T1 (fr)
AU (1) AU2821589A (fr)
BR (1) BR8807838A (fr)
DE (1) DE3883788T2 (fr)
FI (1) FI87053C (fr)
SE (1) SE462704B (fr)
WO (1) WO1989005196A1 (fr)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1993014877A1 (fr) * 1992-01-28 1993-08-05 Hg Tech Ab Procede d'atomisation
WO1998036825A1 (fr) * 1997-02-21 1998-08-27 Bradford Particle Design Ltd. Procede et appareil pour la formation de particules
DE19831335A1 (de) * 1998-07-13 2000-02-10 Michael Angermann Tröpfchenerzeuger für leitfähige Flüssigkeiten
WO2000067892A1 (fr) * 1999-05-07 2000-11-16 Astrazeneca Ab Procede et dispositif de formation de particules
WO2003068378A1 (fr) * 2002-02-13 2003-08-21 Mepura Metallpulvergesellschaft M. B. H. Procede de production de materiau particulaire
WO2004047797A2 (fr) * 2002-11-27 2004-06-10 Pfizer Products Inc. Procede et dispositif de cristallisation mettant en application un ensemble plaque de choc de courants contraries
WO2011144748A1 (fr) * 2010-05-21 2011-11-24 Centre National De La Recherche Scientifique (Cnrs) Procede de production d'un materiau nanometrique et reacteur pour sa mise en oeuvre

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5662274B2 (ja) * 2011-07-28 2015-01-28 株式会社東芝 流速及び粒径計測方法、ならびにそのシステム

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE901855C (de) * 1939-12-13 1954-01-14 Degussa Vorrichtung zum UEberfuehren von schmelzfluessigen Stoffen oder Stoffgemischen in feinverteilte Form
US4559187A (en) * 1983-12-14 1985-12-17 Battelle Development Corporation Production of particulate or powdered metals and alloys

Family Cites Families (3)

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Publication number Priority date Publication date Assignee Title
JPS59171307A (ja) * 1983-03-18 1984-09-27 Fujitsu Ltd タツプ係数切替方式
JPS59214340A (ja) * 1983-12-15 1984-12-04 Nec Corp 振幅等化方式および振幅等化装置
NO853772L (no) * 1984-11-02 1986-05-05 Universal Data Systems Inc Fremgangsmaate for etablering av en kommunikasjonskanal, modem-kommunikasjonssystem og mikroprossesorstyrt modem.

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE901855C (de) * 1939-12-13 1954-01-14 Degussa Vorrichtung zum UEberfuehren von schmelzfluessigen Stoffen oder Stoffgemischen in feinverteilte Form
US4559187A (en) * 1983-12-14 1985-12-17 Battelle Development Corporation Production of particulate or powdered metals and alloys

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
DERWENT'S ABSTRACT AN 1980-76336C & SU,A,719802, Sibe Metal Inst., publ. 1980-03-15 *
DERWENT'S ABSTRACT AN 1982-30615E & SU,A,839694, Sibe Metal Inst. publ. 1981-06-26 *
DERWENT'S ABSTRACT AN 1986-257345 & SU,A,1210989, Zaporo Mech Eng Cons, publ. 86-02-15 see figure *

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1993014877A1 (fr) * 1992-01-28 1993-08-05 Hg Tech Ab Procede d'atomisation
WO1998036825A1 (fr) * 1997-02-21 1998-08-27 Bradford Particle Design Ltd. Procede et appareil pour la formation de particules
US6440337B1 (en) 1997-02-21 2002-08-27 Inhale Therapeutic Systems, Inc. Method and apparatus for the formation of particles
DE19831335A1 (de) * 1998-07-13 2000-02-10 Michael Angermann Tröpfchenerzeuger für leitfähige Flüssigkeiten
WO2000067892A1 (fr) * 1999-05-07 2000-11-16 Astrazeneca Ab Procede et dispositif de formation de particules
US6551532B1 (en) 1999-05-07 2003-04-22 Astrazeneca Ab Method and device for forming particles
WO2003068378A1 (fr) * 2002-02-13 2003-08-21 Mepura Metallpulvergesellschaft M. B. H. Procede de production de materiau particulaire
WO2004047797A2 (fr) * 2002-11-27 2004-06-10 Pfizer Products Inc. Procede et dispositif de cristallisation mettant en application un ensemble plaque de choc de courants contraries
WO2004047797A3 (fr) * 2002-11-27 2005-05-26 Pfizer Prod Inc Procede et dispositif de cristallisation mettant en application un ensemble plaque de choc de courants contraries
WO2011144748A1 (fr) * 2010-05-21 2011-11-24 Centre National De La Recherche Scientifique (Cnrs) Procede de production d'un materiau nanometrique et reacteur pour sa mise en oeuvre
FR2960164A1 (fr) * 2010-05-21 2011-11-25 Centre Nat Rech Scient Procede de production d'un materiau nanometrique et reacteur pour sa mise en oeuvre

Also Published As

Publication number Publication date
JPH03501629A (ja) 1991-04-11
SE8704905D0 (sv) 1987-12-09
EP0419479B1 (fr) 1993-09-01
AU2821589A (en) 1989-07-05
FI87053B (fi) 1992-08-14
SE8704905L (sv) 1989-06-10
ATE93750T1 (de) 1993-09-15
EP0419479A1 (fr) 1991-04-03
SE462704B (sv) 1990-08-20
FI87053C (fi) 1992-11-25
JP2703378B2 (ja) 1998-01-26
DE3883788D1 (de) 1993-10-07
FI902863A0 (fi) 1990-06-08
BR8807838A (pt) 1990-10-23
DE3883788T2 (de) 1993-12-16

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