US984886A - Manufacture of photographic films. - Google Patents
Manufacture of photographic films. Download PDFInfo
- Publication number
- US984886A US984886A US50919309A US1909509193A US984886A US 984886 A US984886 A US 984886A US 50919309 A US50919309 A US 50919309A US 1909509193 A US1909509193 A US 1909509193A US 984886 A US984886 A US 984886A
- Authority
- US
- United States
- Prior art keywords
- film
- bath
- films
- manufacture
- photographic films
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000004519 manufacturing process Methods 0.000 title description 5
- 238000000034 method Methods 0.000 description 8
- 230000001235 sensitizing effect Effects 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 4
- 229920002678 cellulose Polymers 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 description 3
- 239000001913 cellulose Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229910052709 silver Inorganic materials 0.000 description 2
- 239000004332 silver Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 230000008961 swelling Effects 0.000 description 2
- 241000861718 Chloris <Aves> Species 0.000 description 1
- 108010010803 Gelatin Proteins 0.000 description 1
- 206010028813 Nausea Diseases 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 229920000297 Rayon Polymers 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- ZOOODBUHSVUZEM-UHFFFAOYSA-N ethoxymethanedithioic acid Chemical compound CCOC(S)=S ZOOODBUHSVUZEM-UHFFFAOYSA-N 0.000 description 1
- 229920000159 gelatin Polymers 0.000 description 1
- 239000008273 gelatin Substances 0.000 description 1
- 235000019322 gelatine Nutrition 0.000 description 1
- 235000011852 gelatine desserts Nutrition 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000008693 nausea Effects 0.000 description 1
- -1 nitrateof silver Chemical compound 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 230000001172 regenerating effect Effects 0.000 description 1
- 238000009877 rendering Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 description 1
- 239000012991 xanthate Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/015—Apparatus or processes for the preparation of emulsions
Definitions
- This invention relates to a process by means of which it is possible to make sensitive to the light, cellulosic films obtained from watersolution, more particularly cellu-' losic films obtained by regenerating the cellulose of-a Water solution of celluloslc xanthate of sodium (viscose).
- the films thus obtained can be used in photography, for kinematographic stereoscopic purposes, etc., either as ositive or as negative films.
- cellulose -filmsjust mentioned are first of all'dipped-into a bath of water, so as to obtain a swelling of the said films. In that state the are at once dipped into a bath of a chlori bromid or iodld, as is generally done in photography, preferably using either.
- chlorid of sodium or iodid of potassium Owing to the particular state of the film at the moment of its immersion into the bath, on account of the swellingproduced by the water, the salt penetrates into the film in stead of merely forming a superficial layer. It is roperly impregnated when removed from the chlorid, bromid or iodid bath.”
- the film After removin' it from the chlorid, bro-' mid or iodid bath, the film can be dried or immediately d1pped into a bath of silver salt such as nitrateof silver, similar to that used in photo phy. After being removed fromthat bat the film could be subjected to. the action of any suitablebath used in photograhy, either in order to increase its zensitiveness, or for giving itsp'ecial properies. .50 Itgoes without saying that the order in which the film passes into the. successive baths is not absolutely essential, this order could-be modified according'to the process emplo ed.
- Cellulos'esheets could be treated eitherby treating'a continuous band, 'or by treating sheets cut to the desired size.
- sensitizing films which consistsin placing a cellulosic film in a liquid bath, allowing the film to "remain in' said bath until the film has swelled, and then impregnating the film with sensitizing substances.
- the herei described process of sensitizing films w ich consists n placing a cellulosic fihn in a bath of a huloid sult allowa silver Hall, and further treating the film 10 ing the film to remain in said bath until the for photographic purposes. fihn has swelled, and then impregnatlng the In testimony whereof I have signed this film with sensitizing substances. specification in'the presence of two subscrib 4.
- the herein described process of sensi-. ing ⁇ '-'itnesses. tizing films which consists in placing a cel- EDWIN BRANDENBERGER. lulosic filmin a bath of a haloid salt, allow- witnesseses:
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Manufacture Of Macromolecular Shaped Articles (AREA)
- Silver Salt Photography Or Processing Solution Therefor (AREA)
- Moulding By Coating Moulds (AREA)
Description
EDWIN nnannnnsnacnn, or rmoN-nEs-vosens, FRANCE.
No Drawing.
MANUFACTURE PHOTOGRAPHIG FILMS.
Patented use. 21, 1911.
To all whom 'it may concern:
Be it known that'l, Eowm BnAnnnN- nausea, a chemist, of Thaon-Les-Vosges,
, Vos es, France, have invented a new and use 111 Improved. Manufacture of Photographic Films, which is fully set forth in the following specification.
This invention relates to a process by means of which it is possible to make sensitive to the light, cellulosic films obtained from watersolution, more particularly cellu-' losic films obtained by regenerating the cellulose of-a Water solution of celluloslc xanthate of sodium (viscose). The films thus obtained can be used in photography, for kinematographic stereoscopic purposes, etc., either as ositive or as negative films.
he process of manufacture is as follows: The cellulose -filmsjust mentioned are first of all'dipped-into a bath of water, so as to obtain a swelling of the said films. In that state the are at once dipped into a bath of a chlori bromid or iodld, as is generally done in photography, preferably using either.
chlorid of sodium or iodid of potassium. Owing to the particular state of the film at the moment of its immersion into the bath, on account of the swellingproduced by the water, the salt penetrates into the film in stead of merely forming a superficial layer. It is roperly impregnated when removed from the chlorid, bromid or iodid bath."
It will be understod that the'swelling required for the impregnating just'meritioned,
6 could be obtainedwlthout using the waterv bath, but using a water solution of thechlm rid, bromid or iodidi" In that single bath the film would become swollen and impregnoted with chlorid,-bromid or iodid'.
so After removin' it from the chlorid, bro-' mid or iodid bath, the film can be dried or immediately d1pped into a bath of silver salt such as nitrateof silver, similar to that used in photo phy. After being removed fromthat bat the film could be subjected to. the action of any suitablebath used in photograhy, either in order to increase its zensitiveness, or for giving itsp'ecial properies. .50 Itgoes without saying that the order in which the film passes into the. successive baths is not absolutely essential, this order could-be modified according'to the process emplo ed. In the same way, it is obvious that, nstead of immersing the films in the 'spbstance capable of rendering the film sensltivefto light, fdr instance, salts of. gold, salts of iron (ferro-cyanids) etc, and, gen-- erally, any saltsused in photography; The impregnation would take place in the same conditions, and the result desired, namely the production of a sensitive film without gelatin or any other method of fixing, would be obtained. Heat no longer has any effect onthe photographic impressions obt-ained', and no separation can take place such as often happens with all sensitive papers or plates, in which the sensitive portion is merely a superficial onc' and is not impregnated in the massof the support.
It will be understood that it is possible to fix cellulose films thus obtained, to a suitable su port, for instance glass or paper. The fixing would be effected by glue, either soluble or insoluble in water, according to the purposes desired, and the said fixing could be one either before the sensitizing of the film or after.
Cellulos'esheets could be treated eitherby treating'a continuous band, 'or by treating sheets cut to the desired size.
'Having now'iparticularly described and ascertained the nature of my said invention and in what manner the same is to be 'performed, I declare that what I claim is .1.- The hereinl,'described process of sensitizing film's, which consists in placing a film in a liquid bath, allowing the film toremain in said bat-h until the film has swelled,
and then impregnating thefilm with sensitizin substances.
2. %he herein described process of" sensitizing films, which consistsin placing a cellulosic film in a liquid bath, allowing the film to "remain in' said bath until the film has swelled, and then impregnating the film with sensitizing substances.
3. The herei described process of sensitizing films, w ich consists n placing a cellulosic fihn in a bath of a huloid sult allowa silver Hall, and further treating the film 10 ing the film to remain in said bath until the for photographic purposes. fihn has swelled, and then impregnatlng the In testimony whereof I have signed this film with sensitizing substances. specification in'the presence of two subscrib 4. The herein described process of sensi-. ing \\'-'itnesses. tizing films, which consists in placing a cel- EDWIN BRANDENBERGER. lulosic filmin a bath of a haloid salt, allow- Witnesses:
ing the film to remain in said bath until the EMILE LUBRET,
film is swelled, placing the film in 9. bath of H. C. COXE.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US50919309A US984886A (en) | 1909-07-23 | 1909-07-23 | Manufacture of photographic films. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US50919309A US984886A (en) | 1909-07-23 | 1909-07-23 | Manufacture of photographic films. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US984886A true US984886A (en) | 1911-02-21 |
Family
ID=3053234
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US50919309A Expired - Lifetime US984886A (en) | 1909-07-23 | 1909-07-23 | Manufacture of photographic films. |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US984886A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2422323A (en) * | 1944-11-24 | 1947-06-17 | Nat Steel Corp | Method of producing sheets and the products obtained |
| US3056676A (en) * | 1959-06-23 | 1962-10-02 | Du Pont | Polymeric film and process of preparation |
-
1909
- 1909-07-23 US US50919309A patent/US984886A/en not_active Expired - Lifetime
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2422323A (en) * | 1944-11-24 | 1947-06-17 | Nat Steel Corp | Method of producing sheets and the products obtained |
| US3056676A (en) * | 1959-06-23 | 1962-10-02 | Du Pont | Polymeric film and process of preparation |
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