US969625A - Still. - Google Patents

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Publication number
US969625A
US969625A US44596708A US1908445967A US969625A US 969625 A US969625 A US 969625A US 44596708 A US44596708 A US 44596708A US 1908445967 A US1908445967 A US 1908445967A US 969625 A US969625 A US 969625A
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Prior art keywords
boiler
casing
coil
still
head
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US44596708A
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John Hoffhine
Norman F Harriman
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/02Treatment of water, waste water, or sewage by heating
    • C02F1/04Treatment of water, waste water, or sewage by heating by distillation or evaporation

Definitions

  • Another object is to provide a device of the above type whichlshall' be substantially automatic in action.
  • Another object is to provide a device of the type first mentioned characterized by efiicientsnd economical running qualities.
  • Another object is toprovide a still so formed as to he reudily cleaned and in which the chance of contamination of the distillate isroduced, to a minimum.
  • Fig. 2' is a. plan view of a supporting frame or holder
  • Fig. 3 is a detail view of a sup- "portling block
  • 4 is aside elevation of a j'condensing coil and associated parts
  • Fig. 61s a sectional view taken substantially along the line w view taken substantially along the line c y invention .miore readily and fully understood, it may here be noted that in the'use of many stills there is a tendency to contamination by the carryingover from the boiler of small particles of the fluid acted u on in a liquid instead of vaporous-form.
  • I11 casing 1.6 isrivcted ii -flanged head 17 on which is supported; as by :thebrackets 18, .a .'ooolingor C9I,1 so01le19 "which leads.”frqm the nip ple or fittnlig l i.
  • Thesefbrackets 18 are pre stably formed, as shown, of sheet metal ahdserve tohold-th'e'coil in properreliitmn with respectito the walls of the casing, as well as. to hold the several turns of the cod pro erly spaced one from another.
  • ooling coil l9 discharges, as at 20, into "the lower portion of the casing 16 which forms astorage tank 21 communicating, as at 22, with-the lower portion of the casing v1 which also is adapted for storage purposes.
  • the upper ortionof the casing 16, which forms a 00nd of the casing," 1, which forms a boiler, are connected one with another, as at 2-7, and
  • the head 12 is provided with screens 29 and 30 serially'disposed, as shown, in the passage of the vapor passin from the boiler and adapted, even with t e' most violent ebullition in the latter to prevent any particles of liquid. passing to, the cooling coil.
  • a check valve 31 adapt edto admit am from without, in the event of a vacuum forming at any point in the apparatus, and thus relieve thesame from strain.
  • a check valve 31 adaptedto admit am from without, in the event of a vacuum forming at any point in the apparatus, and thus relieve thesame from strain.
  • 32- an outlet port normally held closed, as b' a cap, but adapted to be opened if it is desired to wash out the interior of the boiler.
  • vapor is used throughoutin a broad sense to denote any fluid passing over. from the boiler to the condenser.
  • the operation of the abovedescribed embodiment of this invention is substantially as 'follo'ws-z
  • the ni ple' S' is connected to "any desired source 0 steam supply, and the inlet 28'connected with the source of supply of the liquid which is to be distilled, in the "present case assumed to be water.-
  • These two inlets are adjusted as to admit water through h'econdenser and-connection 2'1 at ust such rate as tomaintain the level in the boiler justabove the heatin coil 7 and as y to substantially condense aj1, we ave shown an 'ordinah'y 4 i of the steam passln into the latter member.” :In Fig.
  • a still comprising a pair of vertical drums; a partition-dividing the first drum into an upper boiler portion and a lower Y seconddrum into an upper condensing port1on and a .lower storage port-ion; connecstorage ,portion; a partition dividing the tions between said stora e portions of the two drums; a heating coi in the boiler portion oft-he first drum; aconde in'g c011 in 12.1% secmfi drum he iswer siomga befier portlon. een boflm in testlmany whereof We affix our sxgnamartian I a I an 111- imes 1n the resenceof two wltnesss.

Description

J. HOPPHINE 62 N. F. HARBIMAN.
sTILL. APPLICATION I'll-ED JULY 29, 190E.
Patented Sept. 6, 1910.
0 mu T M Wang 1 m W. w N mw H m W s p T "H .e E An S n n m H m v H t x nm 7 ll a 1 AT. w; I f 2 NEYS I STILL.
APPLICATION FILED JULY 29, 1908.
' as v elements and arrangement of parts which JOHN HOFFHINE AND NORMIAN F. HARRIMAN, =01? OMAHA, NEBRASKA.
STILL.
Specification of Letters Patent.
Patented Sept. 6, 1910.
Application filed July 29, 1908. Serial Ho. 445,967.
To. all whom it may concern:
lie it known that we, Jon HOFFHIN-E and .clcmimn F. HARRIMAN, citizens of the United Stet-es, residing at Omaha, in the county of Douglas and State of Nebraska, have, iii-- vented certain new and useful Improvements in Stills, of which the following is a full, clear, and exact description, such as will on- .abie' others skilled in the artto which it appertains to make and use the same This invention relates'to stills.
@no of the objects thereof is, to provide is device of the above type of simple, cheap, and strong construction and having all parts so compactly disposed as to consume small space andyet be of large capacity. I
Another object is to provide a device of the above type whichlshall' be substantially automatic in action.
Another object is to provide a device of the type first mentioned characterized by efiicientsnd economical running qualities.
Another object is toprovide a still so formed as to he reudily cleaned and in which the chance of contamination of the distillate isroduced, to a minimum. (Ether objects will he ii in part pointed out liez'ei' The invention accordingly consists in the features of construction, combinations of obvious and will be exemplified in the construction hereinafter set forth, and the scope of the application ofiivhich will be indicated in the following claim. Y
"In the accompanying drawings, wherein. is show-n one of various possible embodiment's'of this invention,'l igure 1 is a side elevation thereof, partially in section in. or
der' to show the construction more -eclearly Fig; 2' is a. plan view of a supporting frame or holder; Fig. 3 is a detail view of a sup- "portling block; 4 is aside elevation of a j'condensing coil and associated parts; Fi 5 'Fised-et'ail view ofa coil support; Fig. 61s a sectional view taken substantially along the line w view taken substantially along the line c y invention .miore readily and fully understood, it may here be noted that in the'use of many stills there is a tendency to contamination by the carryingover from the boiler of small particles of the fluid acted u on in a liquid instead of vaporous-form. his is especially the case when the boiling is violent and is especially annoying when a high degree of'puri'ty is desired in the distillate. It may also be noted that if a large output is desired in apparatus of the general nature dealt with in this invention, a large outlay of heat is required, which, unless the distil lute 'is innnediately used in warm condition, is largely thrown away, being taken up in the latent heat of vaporization and carried all by the cooling water as the" distillate c on- "enses.
Anothen'feeture which may be noted is the fact that in distilli'nga liquid which leaves-a residue or scale upon the heating surfaee,"unless means are provided whereby ready access can be had to all parts'of the device this deposit or scale will gradually reduce the efficiency of the apparatus.
The above and, other-defects are done away with inconstructionsof the nature of that hereinafter described.
, l teferringnnow to the accompanying :lra wings, there is shown in Figrle shelter easing '1 having fitted therein a head. 2,
fiang'ed'ns at 3, and riveted in place, as shownat 33 in said figure. Upon thls head is laid a plate 4 which he's mounted thereon a supporting spider or bracket 5, best shown in Fig. 5 of the drawings, theendszof which rest in the severallooks 6. Upon this spider is afiat heatin coil 7, preferably of copper, one end of w llCll' lends to a" nipple 8 and thev other end to a nipple 9, both mounted in-thewall ,of the casing and form ing a" tight joint therewith. v
Removably. secured to the upper" end of the casing 1, as byflangfes l0 and bolts 11 is a cap or head 12 forfning a, passage 13 leading to a nipple 14 in the head '15 of a second casing-or receptacle l6.' I11 casing 1.6 isrivcted ii -flanged head 17 on which is supported; as by :thebrackets 18, .a .'ooolingor C9I,1 so01le19 "which leads."frqm the nip ple or fittnlig l i. Thesefbrackets 18 are pre stably formed, as shown, of sheet metal ahdserve tohold-th'e'coil in properreliitmn with respectito the walls of the casing, as well as. to hold the several turns of the cod pro erly spaced one from another.
ooling coil l9 discharges, as at 20, into "the lower portion of the casing 16 which forms astorage tank 21 communicating, as at 22, with-the lower portion of the casing v1 which also is adapted for storage purposes.
of the drawings.
The upper ortionof the casing 16, which forms a 00nd of the casing," 1, which forms a boiler, are connected one with another, as at 2-7, and
' there is provided to the condenser an inletjconnection 28.
The head 12 is provided with screens 29 and 30 serially'disposed, as shown, in the passage of the vapor passin from the boiler and adapted, even with t e' most violent ebullition in the latter to prevent any particles of liquid. passing to, the cooling coil.
There is also proxdded' in head 12,101 at .any other suitable point, a check valve 31 adapt edto admit am from without, in the event of a vacuum forming at any point in the apparatus, and thus relieve thesame from strain. 'There' is also provided at 32- an outlet port normally held closed, as b' a cap, but adapted to be opened if it is desired to wash out the interior of the boiler.
It may here bef noted that the term vapor is used throughoutin a broad sense to denote any fluid passing over. from the boiler to the condenser.
The operation of the abovedescribed embodiment of this invention is substantially as 'follo'ws-z The ni ple' S' is connected to "any desired source 0 steam supply, and the inlet 28'connected with the source of supply of the liquid which is to be distilled, in the "present case assumed to be water.- These two inlets are adjusted as to admit water through h'econdenser and-connection 2'1 at ust such rate as tomaintain the level in the boiler justabove the heatin coil 7 and as y to substantially condense aj1, we ave shown an 'ordinah'y 4 i of the steam passln into the latter member." :In Fig.
' valve don- "trolling the in1et-pi1pe-, so that the quantity 0f Water ortother -;reg'ulated with referen'ce'to the rate of evape'oj "eliecting the ;adjustmentstated. In ---thisquid admitted maybe oration, asiafiorliing one simple means of,
manner, a largeheating surface relative to the volume of water acted upon is maintained and substantially all of the heat-of readers the steam economically used, The water in the boiler thus passes in the form of steam through the screens 29 and 30 and. to the" condensing coil 19 in which it again assumes a liquid form and passes to the storage tanks, as above-set forth. The latent heat given up by the water in condensing in coil 19, moreover, is largely absorbed by the,
carries on its functions automatically. enser and the upper portlon If it be desired to clean the interior of the boiler, as on account of the deposit of scale,
.the outlet 32 is opened and the boiler flushed objects of this invention are achieved and the above enumerated advantages are, among others, present. The construction 15 gained to the inner walls of the simple and inexpensive and the action not only automatic but highly efficient in that it utilizes the-heating agent in an economicalmanner and gives an output of a high degree of purity" under all conditions of running. As many changes could be made in the above construction and many apparently widely different embodiments of this inven "tion'could be made withoutdeparting from the scope thereof, it is intended that all matter contained inthe above description or shown in the accompanying -drawings shall be interpreted as illustrative and not in a.
. limiting sense.
.It is also to be understood that the langua e used in the following'claims is inten ed to cover all of the generic andspe V cific features of the invention herein described and allstatements of the see e of the invention, which, as a matter 0 lan-v gauge, might be said to fall tlierebetween.
Having described our invention, what we claim; as new and desire to secure by Letters Patent. is
A still, comprising a pair of vertical drums; a partition-dividing the first drum into an upper boiler portion and a lower Y seconddrum into an upper condensing port1on and a .lower storage port-ion; connecstorage ,portion; a partition dividing the tions between said stora e portions of the two drums; a heating coi in the boiler portion oft-he first drum; aconde in'g c011 in 12.1% secmfi drum he iswer siomga befier portlon. een boflm in testlmany whereof We affix our sxgnamartian I a I an 111- imes 1n the resenceof two wltnesss.
water from the comiensing portion to the I?! 2 JOHN HUFFHINE.
WEQ NORMAN F HARRIMAN. m pa sian; a m: Witnesses:
. m cs 0 sewn- 1 RALPH A. NEWELL,
drum; ma wnnecfsmn afi apteal x30 conduct g HENRY KOSMAN.
US44596708A 1908-07-29 1908-07-29 Still. Expired - Lifetime US969625A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4247369A (en) * 1979-06-11 1981-01-27 Bean Roy E Apparatus for continuous distillation
US4420374A (en) * 1981-06-03 1983-12-13 Ellis Jr John C Water degasification and distillation apparatus
US4612090A (en) * 1981-06-03 1986-09-16 Ellis Jr John C Water degasification and distillation apparatus

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4247369A (en) * 1979-06-11 1981-01-27 Bean Roy E Apparatus for continuous distillation
US4420374A (en) * 1981-06-03 1983-12-13 Ellis Jr John C Water degasification and distillation apparatus
US4612090A (en) * 1981-06-03 1986-09-16 Ellis Jr John C Water degasification and distillation apparatus

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