US89279A - Improved method of utilizing the waste products prom sxjcrar-refineries - Google Patents
Improved method of utilizing the waste products prom sxjcrar-refineries Download PDFInfo
- Publication number
- US89279A US89279A US89279DA US89279A US 89279 A US89279 A US 89279A US 89279D A US89279D A US 89279DA US 89279 A US89279 A US 89279A
- Authority
- US
- United States
- Prior art keywords
- refineries
- utilizing
- sxjcrar
- prom
- waste products
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000002699 waste material Substances 0.000 title description 8
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 12
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 10
- 238000004519 manufacturing process Methods 0.000 description 10
- 235000015320 potassium carbonate Nutrition 0.000 description 10
- 239000002253 acid Substances 0.000 description 8
- 239000003337 fertilizer Substances 0.000 description 8
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 8
- 229940072033 potash Drugs 0.000 description 8
- KWYUFKZDYYNOTN-UHFFFAOYSA-M potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 8
- 239000000047 product Substances 0.000 description 8
- 150000001875 compounds Chemical class 0.000 description 6
- XFXPMWWXUTWYJX-UHFFFAOYSA-N cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 6
- 210000004369 Blood Anatomy 0.000 description 4
- 210000003608 Feces Anatomy 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 239000008280 blood Substances 0.000 description 4
- 229910052742 iron Inorganic materials 0.000 description 4
- 239000010871 livestock manure Substances 0.000 description 4
- 235000011149 sulphuric acid Nutrition 0.000 description 4
- 239000001117 sulphuric acid Substances 0.000 description 4
- 235000002918 Fraxinus excelsior Nutrition 0.000 description 2
- 229940063680 RAW SUGAR Drugs 0.000 description 2
- 108060007338 SDHAF4 Proteins 0.000 description 2
- 210000002268 Wool Anatomy 0.000 description 2
- 235000019631 acid taste sensations Nutrition 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 230000001464 adherent Effects 0.000 description 2
- 239000002956 ash Substances 0.000 description 2
- 239000003818 cinder Substances 0.000 description 2
- 238000005352 clarification Methods 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 239000006071 cream Substances 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 235000013601 eggs Nutrition 0.000 description 2
- 238000000855 fermentation Methods 0.000 description 2
- 230000004151 fermentation Effects 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 239000002515 guano Substances 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 235000012054 meals Nutrition 0.000 description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 2
- 235000020357 syrup Nutrition 0.000 description 2
- UTYXJYFJPBYDKY-UHFFFAOYSA-N tetrapotassium;iron(2+);hexacyanide;trihydrate Chemical compound O.O.O.[K+].[K+].[K+].[K+].[Fe+2].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-] UTYXJYFJPBYDKY-UHFFFAOYSA-N 0.000 description 2
- 235000013311 vegetables Nutrition 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F11/00—Other organic fertilisers
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Fertilizers (AREA)
Description
-matter, such as albumen ttnitml filtrate fltftm.
I we" I VICTOR G. BLOEDE, OF BROOKLYN, NEW YORK. Letters Patent No. 89,279, dated April 27, 1869.
IMPROVED METHOD OF UTILIZING THE WASTE PRODUCTS FROM SUGAR-REFINERIES. m The Schedule referred to in these Letters Patent and making part of the same.
To all whom it may concern:
Be it known that I, VICTOR G. BLOEDE, of the city of Brooklyn, county of Kings, and State of New York, have invented a new and useful Method of Utilizing the Waste Products and Refuse of Sugar-Refineries; and
I do hereby declare that the following is a full and exact description of my processes.
The nature of my invention consists in utilizing the nitrogenous and phosphatic compounds contained in the refuse of sugar-refineries. The first for the manufacture of the yellow prussiate of potash, the second.
for the manufacture of a cheap and efiicicnt manure,
, or both combined for the manufacture of a fertilizer,
scarcely if any inferior to second-grade guanos. To enable others skilled in the art to make use of my invention, I will proceed to give a detailed account of my invention.
In the solution and clarification of crude brown sugar by steam, orboiling, a large quantity of animal of the egg, blood, 850., is made use of. These matters combining with the impurities of the sugar-all of which are rich in nitrogenous, sulphnrous, and phosphatic compounds-by the action of heat are coagulated, and rise to the surfaceof the liquid in the form of a dark brown, muddy scum, which, being ladled oil, (and the adherent sirup pressed out,) is thrown into the river.
To make use of the valuable chemical compounds contained therein, I proceed as follows:
To make a first-class fertilizer, I place the scum into a large wooden or other convenient tank, and add dilute sulphuric acid until it has acquired a slight acid taste' To insure thorough admixture, the scum should be previously brought to the consistency of very thick cream, and the acid added under continuous stirring. The thick slimy mass is then thoroughly dried at a low temperature, and finally reduced to a powder as fine as fiour, the small gravel, 8220., having been pre viously removed by screening. It is then ready for immediate use, and will be found equal to most of the common guanos.- Muriatic, or even nitric acid may be substituted for the sulphuric acid.
To utilize the scum for the production of prussiate of potash, it is first thoroughly dried and screened, to remove the gravel, &c. It is then placed in a tightly closed iron retort, and exposd to a bright fire until the distillation of ammoniacal and tarry matters has entirely ceased. The remaining cinders or ashes in the retort are finally mixed with carbonate of potash, and exposed for several hours in an iron crucible to an intense red heat. The result is an impure prussiate of potash.
.The manure, produced as above directed, contains all the constituents that make guano so valuable.
By adding a small amount of acid, the ammoniacal salts are changed to sulphates, and are thus firmly bound, while by drying the weight of the mass is reduced fifteen to twenty-five per cent, and the bulk from twenty to forty per cent. Care must however be taken that the heat is not raised to a point at which the ammoniacal salts are decomposed.
As a rule, the more dirt the sugar contains the richer will be the scum. Raw sugar contains a considerable quantity of vegetable albumen, fibres of wool fromthe filters, &c., which, added to the albumen or blood used in clarifying, makes the amount of sulphurons, phosphoric, and nitrogenous compounds contained in the prepared fertilizer very large.
To largely increase the amount of valuable salts contained in the scum, it is necessary to thoroughly decompose the insoluble compounds. To accomplish this in the best manner, I proceed as follows:
I make a round heap of the scum in some exposed place, where the sun has free access to it, and shelter it from rain by means of a shed. The mass soon begins to heat and ferment, and should then occasionally be stirred or raked until the fermentation ceases.
During the continuation of the process, (which will last from two to six weeks,) the heap should be frequently sprinkled with water containing a small amount of sulphuric or other acid, in order to prevent a loss of ammoniacal products. When the process has been completed, the fermented mass should be carefully dried, ground to meal, and filled into-bags for use.
What I claim as my invention, and desire to secure by Letters Patent, is-
1. The utilization of the waste scum of sugar-refineries as a fertilizer.
2. The mode of treating it with acids, to prevent loss of ammoniacal products.
3. The thorough desiccation of the scum to increase its strength and portability.
4. The utilization of the scum for the manufacture of the prussiate of potash.
5. The method of increasing the fertilizing strength of the scum, by heaping and fermenting it, substantially in the manner and for the purpose herein set forth.
VICTOR G. BLOEDE. Witnesses:
ED. B. BARTLEMAN, J N0. E. HEYWOOD.
Publications (1)
Publication Number | Publication Date |
---|---|
US89279A true US89279A (en) | 1869-04-27 |
Family
ID=2158761
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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US89279D Expired - Lifetime US89279A (en) | Improved method of utilizing the waste products prom sxjcrar-refineries |
Country Status (1)
Country | Link |
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US (1) | US89279A (en) |
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0
- US US89279D patent/US89279A/en not_active Expired - Lifetime
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