US532660A - Process of manufacturing tin-plate - Google Patents

Process of manufacturing tin-plate Download PDF

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US532660A
US532660A US532660DA US532660A US 532660 A US532660 A US 532660A US 532660D A US532660D A US 532660DA US 532660 A US532660 A US 532660A
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plates
sand
tin
plate
metal
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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C2/00Hot-dipping or immersion processes for applying the coating material in the molten state without affecting the shape; Apparatus therefor

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  • My invention relates to an improved pro.- cess for manufacturing tin plate, terne, or lead plates, and consists in dipping the plates successively in two kettles each containing a quantity of pure tin, or a mixture of-lead and tin, reduced to a molten condition, and having in the first or coating kettle a covering of sand mixed with palm oil and a chem ical fiux to facilitate the finish of the plates, and in the second or finishing kettle a covering of sand mixed with palm, linseed oil or tallow, thereby reducing the labor, together with an improved apparatus for dipping several sheets at one and the same time, as will be fully described hereinafter.
  • Figure 1 is a side sectional elevation of a furnace provided with kettles and dipping apparatus for the manufacture of tin or terne plates in accordance with my invention.
  • Fig. 2 is a front elevation of the device for holding the sheets while being operated on.
  • Placed on the top of the metal (I, in the first kettle is a quantity of cleansand e, mixed with a suitable oil such as palm or linseed and also with a chemical fluxconsisting of about one third salammoniac and two thirds of nitrate of zinc.
  • Theplates to be coated or covered are first cleaned and treated in a manner well known in the art, and then forced down through the sand e of the first kettle a into the metal (1, and then withdrawn.
  • the plates h passing upward through the sand 6, clean or scour themselves leaving the surplus metal in the sand e, which being oiled will not retain the same, but permit the minute particles of tin to return to the main body below.
  • This operation is repeated several times until a proper coating is given the plates as the action of the sand will serve to clean .the plates and give an even and the desired thickness.
  • a cage consisting of a bent-bar g to which rack bars 7c are attached capable-of holding a number of plates h, which may be either sprung into position or run in at the end.
  • This cage may be attached to an overhead railwayt'provided with a trolley j, which will admit of the said cage being lowered to dip the said plates or elevated to withdraw the same out through the sand.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Coating With Molten Metal (AREA)

Description

(N0 Model.)
W. H. GRIFFITHS. PROCESS OF MANUFACTURING TIN PLATE.
Patented Jan. 15, 1895.
nmm.
v Amer UNITE STATES PAT NT Fries.
WILLIAM'H. GRIFFITHS, on PITTSBURG, PENNSYLVANIA.
PROCESS OF MANUFACTURING TIN-PLATE.
SPECIFICATION forming part of Letters Patent No. 532,660, dated January 15, 1895.
' APPIication filed 44, 18%. Serial No. 508.567. (N0 specimens.)
To all whom it may concern.-
1 3e it known that I, WILLIAM H. GRIFFITHS, a citizen of the United States, residing at Pittsburg, in the county of Allegheny and State of Pennsylvania, have invented certain new and useful Improvements in the Processes of Manufactufing'Iin-Plate; and I do hereby declare the following to be a full, clear, and exact description of the invention, such as will enable others skilled in the art to which it per- ,tains to make and use the same, reference being had to the accompanying drawings, which form a part of this specification.
My invention relates to an improved pro.- cess for manufacturing tin plate, terne, or lead plates, and consists in dipping the plates successively in two kettles each containing a quantity of pure tin, or a mixture of-lead and tin, reduced to a molten condition, and having in the first or coating kettle a covering of sand mixed with palm oil and a chem ical fiux to facilitate the finish of the plates, and in the second or finishing kettle a covering of sand mixed with palm, linseed oil or tallow, thereby reducing the labor, together with an improved apparatus for dipping several sheets at one and the same time, as will be fully described hereinafter.
In the accompanying drawings, Figure 1 is a side sectional elevation of a furnace provided with kettles and dipping apparatus for the manufacture of tin or terne plates in accordance with my invention. Fig. 2 is a front elevation of the device for holding the sheets while being operated on.
In order to manufacture tin plate in ac= cordance with my improved process, I provide two kettles 00-?) and arrange the same in -.a furnace c of suitable construct-ion whereby the-metal may be reduced to a molten condition. Placed on the top of the metal (I, in the first kettle is a quantity of cleansand e, mixed with a suitable oil such as palm or linseed and also with a chemical fluxconsisting of about one third salammoniac and two thirds of nitrate of zinc. The other or second kettle b,'c.ontains a quantity of tin having a covering of sand f, mixed with palm or linseed oil or tallow.
Theplates to be coated or covered are first cleaned and treated in a manner well known in the art, and then forced down through the sand e of the first kettle a into the metal (1, and then withdrawn. The plates h passing upward through the sand 6, clean or scour themselves leaving the surplus metal in the sand e, which being oiled will not retain the same, but permit the minute particles of tin to return to the main body below. This operation is repeated several times until a proper coating is given the plates as the action of the sand will serve to clean .the plates and give an even and the desired thickness.
To finish the plates the same are immersed in the metal d of the second kettle b, and withdrawn through the sand in the same mannor as before described, which regulates the thickness of the coating and makes a smooth surface. The sand f acting as a brush dispenses with what is known in the art as brushmen. p
By mixing the sand with an oil or other fatty substance, the same will prevent the minute particles of tin or other metals from adhering to the sand, and thereby rendering the same useless for the purpose of brushing or scouring and removing the surplus and uneven portions of the coating. By the use of this mixture of sand and oil on the top of the metal much time and labor is saved, as in the process now in use the operator is compelled tobrush the plate after each immersion with a bundle of hemp or tow.
To facilitate the dipping of the sheets I provide a cage consisting of a bent-bar g to which rack bars 7c are attached capable-of holding a number of plates h, which may be either sprung into position or run in at the end. This cage may be attached to an overhead railwayt'provided with a trolley j, which will admit of the said cage being lowered to dip the said plates or elevated to withdraw the same out through the sand.
Having thus described my invention, what I claim, and desire to secure by Letters Patent, is
The herein described process of manufacturing tin plates, tome, and the like which consists in first dipping the plates into a bath of molten metal through a layer of sand mixed with oil and a chemical-flux consisting of salammoniac and nitrate of zinc, which layer floats on the surface of the molten metal, and In testimony that I claim the foregoing I Withdrawingthe plates; andaseeond dipping hereunto affix my signature this 27th day of of the plates into another bath of molten November, A. D. 1893.
metal through a layer'of sand mixed with oil WILLIAM H. GRIFFITHS. [L. s.] 5 or tallow floating on said metal, and with- In presence of drawing the plates through the layer, as set P. B. REILLY,
forth. M. E. HARRISON.
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