US5271267A - Method and apparatus for determining fluid properties from sonic/temperature fluid signature - Google Patents
Method and apparatus for determining fluid properties from sonic/temperature fluid signature Download PDFInfo
- Publication number
- US5271267A US5271267A US07/848,266 US84826692A US5271267A US 5271267 A US5271267 A US 5271267A US 84826692 A US84826692 A US 84826692A US 5271267 A US5271267 A US 5271267A
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- 239000012530 fluid Substances 0.000 title claims abstract description 126
- 238000000034 method Methods 0.000 title claims abstract description 24
- 230000001902 propagating effect Effects 0.000 claims abstract description 6
- 239000007788 liquid Substances 0.000 description 29
- 230000005540 biological transmission Effects 0.000 description 4
- 230000001934 delay Effects 0.000 description 4
- 238000010586 diagram Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000001514 detection method Methods 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 230000003321 amplification Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000003199 nucleic acid amplification method Methods 0.000 description 1
- 239000003209 petroleum derivative Substances 0.000 description 1
- 230000000644 propagated effect Effects 0.000 description 1
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Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N9/00—Investigating density or specific gravity of materials; Analysing materials by determining density or specific gravity
- G01N9/002—Investigating density or specific gravity of materials; Analysing materials by determining density or specific gravity using variation of the resonant frequency of an element vibrating in contact with the material submitted to analysis
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N11/00—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
- G01N11/10—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material
- G01N11/16—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material by measuring damping effect upon oscillatory body
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N29/00—Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
- G01N29/02—Analysing fluids
- G01N29/024—Analysing fluids by measuring propagation velocity or propagation time of acoustic waves
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2291/00—Indexing codes associated with group G01N29/00
- G01N2291/02—Indexing codes associated with the analysed material
- G01N2291/028—Material parameters
- G01N2291/02818—Density, viscosity
Definitions
- the present invention relates to a method and apparatus for determining the properties of a fluid traversing through a container or pipe. More particularly, the present invention relates to such a method and apparatus for non-invasively determining such fluid properties as density and viscosity using sonic energy propagated into the fluid to determine sonic propagation velocity of the sonic energy in the fluid in the container or pipe. The determined sonic propagation velocity can then be used as a "signature" along with fluid temperature to determine the fluid properties such as density and viscosity. Additionally, if the fluid identity is known, the pressure can also be determined. Furthermore, if the user has advance knowledge of the types of fluids conveyed in the pipeline, the fluid identity from amongst the possible fluids carried in the pipeline may be determined.
- U.S. Pat. No. 3,942,381 to Brown discloses a clamp-on type transducer for measuring the time taken for an echo to travel through a pressurized bottle and for thereby determining the pressure of gas within the bottle.
- U.S. Pat. No. 3,859,846 to Asada discloses a system with ultrasonic wave transmitting and receiving elements for locating an interface between different liquids flowing through a pipeline.
- a system for determining the properties of a fluid present in a container for example, the density and viscosity of a fluid in a pipeline, based upon non-invasive determination of sonic propagation velocity and fluid temperature, or which allows the determination, based upon advance knowledge of the types of fluids carried by the pipeline, of the fluid type from amongst several types.
- the invention provides a method based upon a knowledge of the fluid type, of determining the pressure of the fluid.
- a method for determining a property of a fluid in a container comprising the steps of propagating from a transmitter sonic energy into the fluid in the container; receiving the sonic energy at a reception site after a defined time delay determined by the nature of the fluid in the container; determining the time for the sonic energy to propagate from the transmitter to the reception site; determining the sonic velocity of the sonic energy from the determined time and from knowledge of the distance from transmitter to reception site; determining the temperature of the fluid in the container; and determining the fluid property from the relationship between the sonic propagation velocity in the fluid and temperature.
- FIG. 1A shows one arrangement of transducers for transmitting sonic energy into a fluid-carrying container and for receiving the energy after a predetermined time depending on the fluid identity;
- FIG. 1B shows signals and time periods in the diagram of FIG. 1A
- FIG. 2 shows the block diagram of a system for implementing the present invention
- FIG. 3 is a graph showing how once the temperature and sonic propagation velocity of the fluid are determined, a general relationship between temperature and sonic propagation velocity is defined;
- FIG. 4 shows how once the general relationship of FIG. 3 is defined, properties of the liquid, such as its density and viscosity, and if the liquid type is known, its pressure, can be determined;
- FIG. 5 shows an exemplary table for determining fluid properties based on the calculated sonic propagation velocity related to a standard temperature using a temperature coefficient.
- liquids at least many petroleum products, have a characteristic "signature” in terms of their sonic propagation velocity (V s ) versus temperature characteristic.
- V s sonic propagation velocity
- they appear to have a characteristic "family” temperature coefficient. This means that a liquid's properties, and possibly its identification, can be determined by its V s at some reference temperature, say 60° fahrenheit. This information, together with the temperature coefficient, is sufficient to identify the liquid properties if its temperature coefficient is constant over the temperature range, as appears to be the case for most liquids.
- a family of curves can be generated, thereby taking into account nonlinearities, and from these families of curves relating temperature and sonic propagation velocity for particular liquids, once the temperature and sonic propagation velocity are determined, the liquid properties can be found by determining which curve the measured variables intersect. These properties include density and viscosity, and if the liquid type is known, pressure. In the case where the temperature coefficient is known to be linear, although it need not be, a measure of V s at any temperature can be related back to a standard temperature, for example 60° fahrenheit, and thus the properties of the liquid can be determined based on the calculated value of V s at the standard temperature.
- the properties of mixture of liquids may be determined by an interpolation technique, to be described below.
- FIG. 1A shows a typical arrangement of the transducers in accordance with a system implementing the invention.
- a first transducer 12 transmits sonic energy into a pipeline 19. The energy travels through the walls at a first refraction angle, as known to those of skill in the art. The energy travels into the fluid in the pipeline with a sonic propagation velocity V s , at a second refraction angle ⁇ . The sonic energy is reflected off the pipeline far wall and returned to a receiving transducer 18.
- the pipeline has a diameter d.
- a temperature sensor 30 is disposed on the pipeline 19 as shown.
- transducer 18 may be disposed on the other side of the pipeline, as known to those of skill in the art, so that a reflection off the other side is not necessary.
- FIG. 1B shows the relationship between the transmitted pulse T X and the received pulse R X .
- the total transit time T N time T L (time in liquid)+time T F (fixed delays)+time T P (time in pipe and transducer housings).
- FIG. 2 shows the basic block diagram of a system in accordance with the present invention. This system determines the sonic propagation velocity of the sonic energy through a liquid.
- the transmitting and receiving transducers 12 and 18 are coupled into the circuit of FIG. 2 as shown. As shown in FIG. 1A, the transmitting and receiving transducers may be disposed on the same side of a pipeline, but it is also possible to dispose the transducers on opposite sides of the pipeline, as shown, for example, in commonly owned U.S. Pat. No. 4,232,548.
- the system shown in FIG. 2 measures the transit time and accounts for the time for transmission of the sonic energy in nonliquid paths, e.g., within the pipe or within the mounting structure for the transducers, so as to be able to calculate directly the sonic velocity V s .
- a transmit pulse is generated by a transmitter generator 10 initiated by a transmit command 9 and transmitted to the transmitting transducer 12.
- a counter 14 is started.
- the counter 14 collects the counts generated by a high frequency oscillator 16.
- the value of the counter when the sonic signal is received is a measure of the total time, T N , of the pulse through the liquid plus the transducer structures and pipe 19.
- the sonic pulse is received by the receive transducer 18 and is provided to an amplifier 20.
- the receive transducer is located in a position to receive the transmitted energy after it has passed through the liquid and been affected by its temperature and internal properties, e.g., density, viscosity and pressure.
- the location accommodates the intended sonic path, whether direct or reflected, and whether it is subjected to refraction or not.
- the counter 14 is preferably designed to count at a 35 Mhz rate, and is started at the time of transmission, and stopped by arrival of the detected, received signal.
- the received signal after amplification by amplifier 20, is provided to a detector 22.
- the received signal can be detected by suitable zero crossover and comparator circuitry having a reference level.
- AGC stage 24 when a transmitted pulse is received by receiving transducer 18, it is amplified by the amplifier 20 and gain controlled by AGC stage 24 so as to produce a fixed and predetermined peak amplitude.
- the detector 22 may include a comparator, with the comparator producing a pulse when the reference level of the comparator has been exceeded. The pulse from the detector stops the counter 14 and the counter value is directly related to the travel time of the sonic pulse from transmitter to receiver.
- a microcomputer 28 uses the calculated value of V s , as well as the measured temperature from a temperature sensor 30.
- the measured temperature value is provided to an analog temperature computer 32 which converts the sensor 30 value (e.g., a resistance) to an analog voltage.
- the analog voltage is fed to an analog to digital converter 34, which converts the analog value into a digital signal.
- Computer 28 determines the fluid properties based upon the determined sonic propagation velocity and a stored temperature coefficient (i.e., an equation) or from a family of curves relating temperature and sonic propagation velocity, stored in digital memory 36.
- a communications port 40 may be provided for transmission of data to other data receiving devices, and an alarm can be provided in the event of an extreme condition, e.g., high temperature, pressure, etc., to be discussed below.
- the characteristic curve identified may also uniquely specify the particular fluid.
- the fluid type from amongst the plurality of fluid types, can be identified. It is not always possible to identify the fluid type if one does not have knowledge of the types of fluid carried by the pipeline. For example, even though the temperature/sonic propagation velocity measures fall on curve Y, it is still possible that the fluid might be a mixture of a fluid with characteristic X and a fluid with characteristic Z, or W, for that matter. Should the intersection point of temperature and sonic propagation velocity not fall on a curve, e.g., point A in FIG. 3, an interpolation procedure can be used to determine the mixture's properties, as explained below.
- the fluid properties such as density and viscosity can be displayed on the display device 38, in user selected units.
- the pressure of the fluid can also be determined and displayed if the fluid type is known. This is shown in FIG. 4. Should a dangerous pressure be determined, the alarm 40 can be sounded.
- FIG. 4 also shows that an interpolation technique can be used to determine the fluid properties of a fluid which does not fall on one of the characteristic curves of FIG. 3. See, e.g., point A in FIG. 3 which corresponds to point B in FIG. 4.
- the velocity calculation for a measured temperature can be related to a standard temperature, e.g., 60° F., and the liquid properties identified based on the V s value stored in a table which is closest to the temperature compensated V s value calculated using the temperature coefficient.
- FIG. 5 shows an example of such a table wherein the measured V s value is shown in the left column, and the compensated sonic propagation velocity at a standard temperature of 60° F., shown in the second column from the left, is used to determine the fluid characteristic.
- the fluid characteristic is known, e.g., curve X, Y, Z or W, a look-up table having the data in FIG.
- a suitable equation using the temperature coefficient to relate the particular fluid property, e.g., density or viscosity, to temperature can be used to determine that property.
- the particular fluid property at 60° F. the standard temperature
- V s at the standard temperature can be determined once V s at the standard temperature is known.
- a temperature coefficient can then be used to relate the property at the standard temperature to the actual temperature (fourth column from left).
- the numbers and letters in FIG. 5 are directly related to the graphs show in FIG. 3, as should be clear from a comparison of the two charts.
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Abstract
Description
Claims (14)
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US07/848,266 US5271267A (en) | 1992-03-09 | 1992-03-09 | Method and apparatus for determining fluid properties from sonic/temperature fluid signature |
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US07/848,266 US5271267A (en) | 1992-03-09 | 1992-03-09 | Method and apparatus for determining fluid properties from sonic/temperature fluid signature |
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Cited By (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5467321A (en) * | 1994-09-26 | 1995-11-14 | Baumoel; Joseph | Insertion ultrasonic transducer with mode conversion and method for reducing multiple signal reception |
WO1997006433A1 (en) * | 1995-08-03 | 1997-02-20 | Milltronics Ltd. | Method of detecting characteristics of liquids in pipes and pump controlling |
US5869745A (en) * | 1996-12-20 | 1999-02-09 | Morton International, Inc. | Ultrasonic gas pressure measurement for inflators of vehicular airbag systems |
US6032516A (en) * | 1996-10-08 | 2000-03-07 | Toyota Jidosha Kabushiki Kaisha | Method and apparatus for determining gasoline characteristics by using ultrasonic wave |
US6082180A (en) * | 1998-10-21 | 2000-07-04 | Battelle Memorial Institute | Ultrasonic fluid densitometer for process control |
US6151956A (en) * | 1997-10-14 | 2000-11-28 | Toyota Jidosha Kabushiki Kaisha | Oil deterioration sensor |
US6227040B1 (en) * | 1998-02-03 | 2001-05-08 | Caldon, Inc. | Method and apparatus for determining the viscosity of a fluid in a container |
WO2003004999A1 (en) * | 2001-06-29 | 2003-01-16 | Robert Bosch Gmbh | Device for evaluating the signal of a viscosity sensor |
WO2004032702A2 (en) | 2002-10-03 | 2004-04-22 | Coulter International Corp. | Apparatus and method for hematologic analysis |
US20040149013A1 (en) * | 2003-01-31 | 2004-08-05 | Joseph Baumoel | Wide beam clamp-on ultrasonic densitometer |
US20050076704A1 (en) * | 2001-12-05 | 2005-04-14 | Wu Sean F. | Acoustic particulates density sensor |
US20080110262A1 (en) * | 2004-02-12 | 2008-05-15 | Nexense Ltd. | Method and Apparatus For Detecting Panel Conditions |
US20090078912A1 (en) * | 2007-09-26 | 2009-03-26 | Air Products And Chemicals, Inc. | Method For Determining Carbon Content Of A Hydrocarbon-Containing Mixture |
US9752911B2 (en) | 2014-12-29 | 2017-09-05 | Concentric Meter Corporation | Fluid parameter sensor and meter |
US10107784B2 (en) | 2014-12-29 | 2018-10-23 | Concentric Meter Corporation | Electromagnetic transducer |
US10126266B2 (en) | 2014-12-29 | 2018-11-13 | Concentric Meter Corporation | Fluid parameter sensor and meter |
AT520557B1 (en) * | 2018-01-24 | 2019-05-15 | Anton Paar Gmbh | Method for determining a corrected value for the viscosity-dependent speed of sound in a fluid to be examined |
US20230184655A1 (en) * | 2021-12-14 | 2023-06-15 | Saudi Arabian Oil Company | Fluid flow sensor using driver and reference electromechanical resonators |
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US4235099A (en) * | 1978-12-27 | 1980-11-25 | Terumo Corporation | Ultrasonic apparatus and method for measuring the density of liquid |
US4331025A (en) * | 1980-10-14 | 1982-05-25 | Mapco, Inc. | Methods of measuring fluid viscosity and flow rate |
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Cited By (32)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5467321A (en) * | 1994-09-26 | 1995-11-14 | Baumoel; Joseph | Insertion ultrasonic transducer with mode conversion and method for reducing multiple signal reception |
WO1997006433A1 (en) * | 1995-08-03 | 1997-02-20 | Milltronics Ltd. | Method of detecting characteristics of liquids in pipes and pump controlling |
US6112254A (en) * | 1995-08-03 | 2000-08-29 | Milltronics Ltd. | Method of detecting characteristics of liquids in pipes and pump controlling |
US6032516A (en) * | 1996-10-08 | 2000-03-07 | Toyota Jidosha Kabushiki Kaisha | Method and apparatus for determining gasoline characteristics by using ultrasonic wave |
US6250137B1 (en) * | 1996-10-08 | 2001-06-26 | Toyota Jidosha Kabushiki Kaisha | Method and apparatus for determining gasoline characteristics by using ultrasonic wave |
US5869745A (en) * | 1996-12-20 | 1999-02-09 | Morton International, Inc. | Ultrasonic gas pressure measurement for inflators of vehicular airbag systems |
US6151956A (en) * | 1997-10-14 | 2000-11-28 | Toyota Jidosha Kabushiki Kaisha | Oil deterioration sensor |
US6227040B1 (en) * | 1998-02-03 | 2001-05-08 | Caldon, Inc. | Method and apparatus for determining the viscosity of a fluid in a container |
US6446494B2 (en) | 1998-02-03 | 2002-09-10 | Caldon, Inc. | Method and apparatus for determining the viscosity of a fluid in a container |
US6082180A (en) * | 1998-10-21 | 2000-07-04 | Battelle Memorial Institute | Ultrasonic fluid densitometer for process control |
US7089784B2 (en) | 2001-06-29 | 2006-08-15 | Robert Bosch Gmbh | Device for evaluating the signal from a viscosity sensor |
US20040045344A1 (en) * | 2001-06-29 | 2004-03-11 | Berhard Jakoby | Device for evaluating the signal from a viscosity sensor |
WO2003004999A1 (en) * | 2001-06-29 | 2003-01-16 | Robert Bosch Gmbh | Device for evaluating the signal of a viscosity sensor |
US20050076704A1 (en) * | 2001-12-05 | 2005-04-14 | Wu Sean F. | Acoustic particulates density sensor |
US7213445B2 (en) | 2001-12-05 | 2007-05-08 | Wayne State University | Acoustic particulates density sensor |
WO2004032702A2 (en) | 2002-10-03 | 2004-04-22 | Coulter International Corp. | Apparatus and method for hematologic analysis |
EP1572000A4 (en) * | 2002-10-03 | 2008-04-09 | Coulter Int Corp | Apparatus and method for analysing a liquid in a capillary tube of a hematology instrument |
US20040149013A1 (en) * | 2003-01-31 | 2004-08-05 | Joseph Baumoel | Wide beam clamp-on ultrasonic densitometer |
US6786077B2 (en) * | 2003-01-31 | 2004-09-07 | Joseph Baumoel | Wide beam clamp-on ultrasonic densitometer |
US7710124B2 (en) * | 2004-02-12 | 2010-05-04 | Nexense Ltd. | Method and apparatus for detecting panel conditions |
US20080110262A1 (en) * | 2004-02-12 | 2008-05-15 | Nexense Ltd. | Method and Apparatus For Detecting Panel Conditions |
US20090078912A1 (en) * | 2007-09-26 | 2009-03-26 | Air Products And Chemicals, Inc. | Method For Determining Carbon Content Of A Hydrocarbon-Containing Mixture |
US20100224834A1 (en) * | 2007-09-26 | 2010-09-09 | Air Products And Chemicals, Inc. | Method For Determining Carbon Content Of A Hydrocarbon-Containing Mixture |
US7871826B2 (en) * | 2007-09-26 | 2011-01-18 | Air Products And Chemicals, Inc. | Method for determining carbon content of a hydrocarbon-containing mixture |
CN101398420B (en) * | 2007-09-26 | 2013-07-17 | 气体产品与化学公司 | Method for determining carbon content of a hydrocarbon-containing mixture |
US9752911B2 (en) | 2014-12-29 | 2017-09-05 | Concentric Meter Corporation | Fluid parameter sensor and meter |
US10107784B2 (en) | 2014-12-29 | 2018-10-23 | Concentric Meter Corporation | Electromagnetic transducer |
US10126266B2 (en) | 2014-12-29 | 2018-11-13 | Concentric Meter Corporation | Fluid parameter sensor and meter |
AT520557B1 (en) * | 2018-01-24 | 2019-05-15 | Anton Paar Gmbh | Method for determining a corrected value for the viscosity-dependent speed of sound in a fluid to be examined |
AT520557A4 (en) * | 2018-01-24 | 2019-05-15 | Anton Paar Gmbh | Method for determining a corrected value for the viscosity-dependent speed of sound in a fluid to be examined |
US20230184655A1 (en) * | 2021-12-14 | 2023-06-15 | Saudi Arabian Oil Company | Fluid flow sensor using driver and reference electromechanical resonators |
US11860077B2 (en) * | 2021-12-14 | 2024-01-02 | Saudi Arabian Oil Company | Fluid flow sensor using driver and reference electromechanical resonators |
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