US495490A - Andrew honman and victor vulliez - Google Patents
Andrew honman and victor vulliez Download PDFInfo
- Publication number
- US495490A US495490A US495490DA US495490A US 495490 A US495490 A US 495490A US 495490D A US495490D A US 495490DA US 495490 A US495490 A US 495490A
- Authority
- US
- United States
- Prior art keywords
- honman
- vulliez
- victor
- andrew
- lead
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 229910000004 White lead Inorganic materials 0.000 description 6
- 238000000034 method Methods 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 3
- USFZMSVCRYTOJT-UHFFFAOYSA-N Ammonium acetate Chemical compound N.CC(O)=O USFZMSVCRYTOJT-UHFFFAOYSA-N 0.000 description 2
- 239000005695 Ammonium acetate Substances 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
- 235000019257 ammonium acetate Nutrition 0.000 description 2
- 229940043376 ammonium acetate Drugs 0.000 description 2
- 235000011118 potassium hydroxide Nutrition 0.000 description 2
- 235000011121 sodium hydroxide Nutrition 0.000 description 2
- 229910021653 sulphate ion Inorganic materials 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- 241000393496 Electra Species 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 229910052949 galena Inorganic materials 0.000 description 1
- 229940046892 lead acetate Drugs 0.000 description 1
- XCAUINMIESBTBL-UHFFFAOYSA-N lead(ii) sulfide Chemical compound [Pb]=S XCAUINMIESBTBL-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229940072033 potash Drugs 0.000 description 1
- BITYAPCSNKJESK-UHFFFAOYSA-N potassiosodium Chemical compound [Na].[K] BITYAPCSNKJESK-UHFFFAOYSA-N 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G21/00—Compounds of lead
- C01G21/14—Carbonates
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/54—Reclaiming serviceable parts of waste accumulators
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/84—Recycling of batteries or fuel cells
Definitions
- This invention relates to a method of manufacturing white lead in which the roasted ore is primarily subjected to the action of lead acetate, the clear solution from which subsequently having a stream of carbonic acid gas passed through it, and the object of the present invention is to'more completely treat the impoverished or residuum ore resulting from the above referred to operation.
- This solution we subject to heat in a suitable vessel, maintaining it at a temperature of about 60 centigrade in order that finer crystals may be produced than would otherwise be the case, and then precipitate the White lead by carbonate or bi-carbouate of sodium potassium or ammonium. The white lead thus produced is then thoroughly washed and then dried.
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Description
UNITED STATES PATENT OFFICE.
ANDREW HONMAN AND VICTOR VULLIEZ, OF WILLIAMSTOWN, VICTORIA.
PROCESS OF MANUFACTURING WHITE LEAD.
SPECIFICATION forming part of Letters Patent No. 495,490, dated April 18, 1893.
Application filed October 23, 1891. $erial No. 409,608. (No specimens.) Patented in Victoria September 24, 1889,11'0. 7,127, and in Western Australia April 29, 1891, No. 273- To all whom it may concern.-
Be it known that we, ANDREW HONMAN, residing at Electra Street, and VICTOR VULLIEZ, residing at Osborne Street, Williamstown, Victoria, subjects of the Queen of Great Britain, have invented certain new and useful Improvements in Processes for the Manufacture of White Lead, (for which the said HONMAN has obtained Letters Patent in Victoria, dated September 24, 1889, No. '7,127,and in Western Australia, dated April 29, 1891, No. 273,) of which the following is a full, clear, and exact description.
This invention relates to a method of manufacturing white lead in which the roasted ore is primarily subjected to the action of lead acetate, the clear solution from which subsequently having a stream of carbonic acid gas passed through it, and the object of the present invention is to'more completely treat the impoverished or residuum ore resulting from the above referred to operation.
In the companion case filed by us,on the 28th day ofMay, 1891, No. 394,452, we havedescribed the treatment of the reduced and roasted galena by subjecting it to acetate of lead and conveying the resultant liquid to a settling tank and from thence to a vat for subjecting the material to carbonic acid. This process need not be more particularly describedin this case as in carrying out the present invention we take the residuum of this treatment which contains the sulphate of lead and first dissolve it by a solution of caustic soda, caustic potash or ammonium acetate. This solution we subject to heat in a suitable vessel, maintaining it at a temperature of about 60 centigrade in order that finer crystals may be produced than would otherwise be the case, and then precipitate the White lead by carbonate or bi-carbouate of sodium potassium or ammonium. The white lead thus produced is then thoroughly washed and then dried.
Having now particularly described and ascertained the nature of our said invention and in what manner the same is to be performed, what we claim is-" The hereinbefore described process; consisting in dissolving sulphate of lead in a solution of caustic soda or potash or ammonium acetate, subjecting the solution to heat, precipitating the white lead by an alkaline carbonate and finally drying the resultant product, substantially as described.
ANDREW HONMAN. VICTOR VULLIEZ.
Witnesses:
HENRY STOKES, EDWARD BELL.
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US495490A true US495490A (en) | 1893-04-18 |
Family
ID=2564328
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US495490D Expired - Lifetime US495490A (en) | Andrew honman and victor vulliez |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US495490A (en) |
-
0
- US US495490D patent/US495490A/en not_active Expired - Lifetime
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