US3925243A - Apparatus for the manufacture of emulsions - Google Patents

Apparatus for the manufacture of emulsions Download PDF

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US3925243A
US3925243A US39115873A US3925243A US 3925243 A US3925243 A US 3925243A US 39115873 A US39115873 A US 39115873A US 3925243 A US3925243 A US 3925243A
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liquid
stator
stirring member
nozzle
draw
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Hans G Brogli
Werner F Brogli
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Hans G Brogli
Werner F Brogli
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Priority to CH815970A priority Critical patent/CH500756A/en
Priority to US14585371A priority
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Priority to US39115873 priority patent/US3925243A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING
    • B01F15/00Accessories for mixers ; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F15/00006Mixing heads comprising a driven stirrer
    • B01F15/00012Mixing heads comprising a driven stirrer the stirrer being provided with a surrounding stator
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING
    • B01F3/00Mixing, e.g. dispersing, emulsifying, according to the phases to be mixed
    • B01F3/08Mixing, e.g. dispersing, emulsifying, according to the phases to be mixed liquids with liquids; Emulsifying
    • B01F3/0807Emulsifying
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING
    • B01F3/00Mixing, e.g. dispersing, emulsifying, according to the phases to be mixed
    • B01F3/08Mixing, e.g. dispersing, emulsifying, according to the phases to be mixed liquids with liquids; Emulsifying
    • B01F3/0853Mixing liquids using driven stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING, DISPERSING
    • B01F7/00Mixers with rotary stirring devices in fixed receptacles, i.e. movement of the receptacle not being meant to effect the mixing; Kneaders

Abstract

The disclosure relates to apparatus for the manufacture of emulsions in which a first liquid is gradually introduced into a second liquid while stirring. Due of the two liquids, for example a fat or wax, may be heated, for example to melt it, and the other liquid may be relatively cold. In order to ensure good emulsifying in spite of such temperature differences, the apparatus comprises nozzle means arranged to introduce said first liquid in fine distribution into the draw in area of a rotating stirring member running in the second liquid, which stirring member is the rotor part of a mixing and homogenizing tool that also has a stator surrounding the rotor.

Description

United States Patent 11 1 Brogli et a]. Dec. 9, 1975 [5 1 APPARATUS FOR THE MANUFACTURE OF 2,142,344 1/1939 Bowen .1 259/23 EMULSIONS 2,502,778 4/1950 Collins et al 1. 252/359 D 2,673,075 3/l954 Borck; 252/359 C lnvemorsi Hans g Gotthelfslrasse 42, 3,415,650 l2/l968 Frame et al 259/23 x a Werner F. Brogli, 3,692,283 9/1972 Sauer et a1 259/24 E22: FOREIGN PATENTS OR APPLICATIONS [22] Filed: Aug- 23, 1973 340,82l l/l93l Unlled Kmgdom 259/96 [2l] Appl. No 391,158 Primary Examiner-Jack Sofer Related us. Application Dam Attorney, Agent, or Firm-Eyre, Mann & Lucas [63 Continuation-inart of Ser. No. I45, 53,

1 1971, Pat. No. 791,984. 8 May m [57] ABSTRACT The disclosure relates to apparatus for the manufac- [30] Foreign Application Priority Data ture of emulsions in which a first liquid is gradually in- June 1, 1970 Switzerland 859/70 troduced into a second liquid while stirring Due of the two liquids, for example a fat or wax, may be 52 us. (:1 252/359 c; 252/359 D; 259/23; heated, for example to melt n and the other liquid 25 9 may be relatively cold. In order to ensure good emulsi- [51] I t, CU B011? 7/16; B01 13 00; 3 5 fying in spite of such temperature differences, the ap- [58] Field of Search 252/359 C, 359 D, P compl'ises nozzle means arranged introduce 252/3()(,-3]3 NG; 259/23 9 30 said first liquid in fine distribution into the draw in area of a rotating stirring member running in the sec- [5 References Cited ond liquid, which stirring member is the rotor part of UNITED STATES PATENTS a mixing and homogenizing tool that also has a stator surrounding the rotor, l,727,l52 9/1929 Winkler 259/DIG. 30 1,757,065 5/1930 Warsop et al. 252/359 (3 3 Claims, 5 Drawing Figures STIRRER U.S. Patent Dec. 9, 1975 Sheet 1 of2 3,925,243

L 0 TO BE ULSIFIED (LTBE) LIQUID BATH TO BE MIXED U.S. Patent Dec. 9, 1975 Sheet 2 of2 3,925,243

F7 3 Q/STIRRER .rSTIRREH 3 '-STIRRER APPARATUS FOR THE MANUFACTURE OF EMULSIONS CROSS-REFERENCE This application is a continuation-in-part of Ser. No. 145,853 which was filed May 21, 1971 now US. Pat. No. 3,791,984 issued Feb. 12, 1974.

BACKGROUND OF THE INVENTION This invention relates to the manufacture of an emulsion.

In the manufacture of emulsions it is usual to insert the media to be emulsified at temperatures which differ only a little, or as far as possible not at all, from one another.

If, for example, it is desired to produce an emulsion with fat or wax it is as a rule necessary to melt the fat or wax. Then an aqueous liquid can be allowed to run gradually whilst stirring into the melt, which is heated for example at about 80C, whereby experience has always shown that a satisfactory emulsion can only be obtained if the aqueous liquid supplied is likewise heated, for example to about 82C. From this experience there has resulted the procedural rule already mentioned.

On the other hand it can be noted that emulsions are as a rule stable against decomposition only at temperatures below a certain specific value. This value may, for example, according to the type and quantity of emulsifiers and other additions used, be at about to or C. If therefore according to known methods an emulsion has been produced from a fat or wax fusion and a likewise heated aqueous liquid then it is for the most part necessary to cool the emulsion with further stirring until below the stability limit in order to prevent a decomposition of the emulsion. This cooling may under certain circumstances require several hours whilst the actual emulsifying could frequently be carried out in a few minutes. The cooling thus makes the manufacture of the emulsion uneconomic because the emulsifying devices remain filled for a very long time and it also renders a continuous operation practically impossible. Attempts have been made to accelerate the cooling by means of cooling surfaces; this however has frequently the drawback that certain substances, for example wax, become deposited on the cooling surfaces and are thereby drawn out of the emulsion.

It has now been found that under certain circumstances and conditions the traditional procedure aforementioned can be disregarded with resultant advantages.

The parent application Ser. No. 145,853 thus claims a method for the manufacture of an emulsion in which.

a first liquid is gradually introduced while stirring into a second liquid which has been heated to a temperature which is above the limit temperature up to which the finished emulsion is stable and above the solidification temperature of this first liquid, which method is characterized in that the first liquid, at a temperature below the said limit temperature and/or solidification temperature, is introduced in fine distribution in the entry area of a stirring member which runs in the heated second liquid.

The first liquid may be suitably introduced at a temperature which is at least 25C preferably at least 50C below the temperature at which the second liquid, for example melted fat or wax, has been heated. In most cases the first liquid, for example an aqueous liquid,

may be practically cold, that is have room temperature or tap water temperature. In this way the mixture temperature of the finished emulsion after the total quantity provided of the first liquid has been introduced may be below the said limit temperature so that no more cooling with stirring is necessary.

It is also possible to heat the first liquid, for example when this is a fat or wax, and introduce it into a cold second liquid in the manner described above.

SUMMARY OF THE INVENTION The present application relates to apparatus suitable for carrying out the method for making emulsions described above. The apparatus comprises a mixing and homogenizing tool with an annular stator and a stirring member disposed in the stator which is rotatable in order to draw a medium from an inlet side of the stator to mix it thoroughly and thrust it out at an outlet side, and it is characterized in that at least one nozzle is dis posed at the inlet side of the stator with an opening directed towards the draw in area of the stirring member, which nozzle is connected to a supply pipe for the liquid which is to be introduced and emulsified.

The nozzle must be arranged close to the stirring member, in a region where the medium flow rate is high, in such a manner that the entire amount of liquid supplied by it in fine distribution is at once drawn into the homogenizing tool and completely emulsified, and the temperature equalization between this liquid and the medium occurs substantially only in the homogenizing tool.

The nozzle may, for example, have a fine annular gap surrounding the draw in area of the stirring member. Instead of this there could also be arranged around the draw in area a ring of nozzles in order to obtain the required fine distribution of the first liquid.

In a particularly suitable construction the nozzle having an annular gap may be fonned by two annular plates which are fixed to the inlet side of the stator. The annular space bounded by these plates may be divided in the peripheral direction into two or more partial spaces which are each connected to a separate supply pipe so that several components of the first liquid or several first liquids can be introduced separately into the draw in area of the stirring tool. Furthermore the annular gap of the nozzle may be arranged surrounding the draw in area of the stirring member such that the medium drawn in by the stirring member and flowing past the gap produces a low pressure in the nozzle in order to draw in the first liquid through the supply pipe so that the use of a pumping device specifically for the first liquid can be dispensed with. In order to achieve an improved thorough mixing of the medium in the stirring tool a third annular plate may be suitably disposed on the stator which bounds a second nozzle space likewise leading into an annular gap which is directly adjacent the mixing chamber in the mixing tool and is connected to this via openings in the uppermost plate. Thereby a portion of the medium is turned around in the mixing chamber and fed again to the stirring member through the said openings and the additional annular nozzle.

The necessary fine distribution of the liquid introduced into the draw in area of the stirring member can be attained suitably also with a rotatable nozzle wheel which is disposed on the inlet side of the stator and connected to a supply pipe.

DESCRIPTION OF PREFERRED EMBODIMENTS Embodiments of the apparatus according to the invention are explained by way of example in the following description with reference to the drawings. In the drawings:

FIG. 1 shows diagrammatically a vertical section through a stirring tool with a ring nozzle on the inlet side,

FIG. 2 shows diagrammatically a horizontal section through a particular embodiment of the ring nozzle according to FIG. I and FIGS. 3, 4 and 5 show diagrammatic sections through stirring tools with nozzles arranged differently on the inlet side.

The stirring and homogenizing tool shown in FIG. 1 has an annular stator I which is carried via vertical bars 2 on a stand not shown and is immersed, from above, into a medium in a vessel likewise not shown. In the stator l a rotor or stirring member 3 is disposed which may be rotated by means of a shaft 4 around its vertical axis and then sucks, mixes and thrusts upwards medium from below as indicated by the arrows.

On the underside of the stator 1 three annular plates 5, 6 and 7 are fixed, spaced apart from one another, and enclosing between them annular chambers 8 and 9. These annular chambers are' closed on the outer periphery but open inside towards the draw in area of the stirring member 3 via annular nozzle gaps 8a and 9a. The upper annular chamber 8 is in communication,.via openings in the plate 5, with the mixing chamber in the stator 1 so that material to be mixed is supplied to this annular chamber. The lower annular chamber 9 is connected to a supply pipe 10 for a liquid to be emulsified which is fed in fine distribution through the corresponding annular gap 9a to the material to be mixed, which is sucked in by the stirring member 3. The annular gap may have a height of about 0.5 mm to a few mm, for example 3 mm, according to the dimensions of the stirring tool.

In the example shown the annular gaps 8a and 9a are so arranged, and the plates 5, 6 and 7 are so formed on their inner edges, that the medium sucked by the stirring member flowing past the annular gaps produces in these a low pressure in the manner of a jet pump. This has the advantage that the liquid to be emulsified is sucked automatically through the pipe 10. It would of course also be possible to convey the liquid through the pipe 10 with pressure or maintain a vacuum above the material to be mixed, with the use of a closed vessel.

According to FIG. 2 if desired the annular space 9 above the plate 7 may be divided by means of radial partitions 9b into several sector like areas and these separate areas may be connected to separate supply pipes 10, 10 and 10". In this way several different liquids to be emulsified can then be fed separately simultaneously. The arrangement shown is intended for three different liquids in mutual quantity ratios 50 percent; 30 percent; percent (through the pipes 10 and 10 and 10 respectively).

If desired the liquid could be fed from the supply pipe also via an annularly arranged rim of individual nozzles instead of through the nozzle ring gap 9a. It is merely essential for the liquid to be emulsified to be introduced in as fine a distribution as possible directly into the draw in area of the stirring member.

Other different possible arrangements of nozzles are shown diagrammatically, by way of example, in FIGS.

3, 4 and 5. Here also the nozzles are arranged on the inlet side of a stirring and homogenizing tool which, like that shown in FIG. 1, has a stator l and a rotor or stirring member 3. The nozzle openings are directed towards the draw in area of the stirring member 3 in order to introduce the second liquid to be emulsified in fine distribution in this draw in area.

According to FIG. 3 several separate single nozzles 16 are peripherally disposed on the inlet side of the stator 1, connected to individual supply pipes 20.

According to FIG. 4 an annular nozzle 26 is disposed below the stator 1. An annular chamber 29 in this nozzle 26 is connected to a supply pipe 30. The chamber 29 is in communication with the draw in area of the stirring member 3 via a plurality of nozzle openings 29a on the inside of the ring nozzle body.

According to FIG. 5 there is used, for the supply of the liquid to be emulsified in the draw in area of the stirring member 3, a rotatable and drivable nozzle wheel 36 which is disposed under the stirring member 3 and approximately coaxially with this and to which the liquid is fed via a supply pipe 40. The nozzles of this nozzle wheel are directed upwardly towards the stirring member 3.

Emulsions can be made as follows with the apparatus described.

There is placed in a vessel, in which the stirring tool is immersed, a liquid which for any reason, for example because it would be congealed at room temperature, is heated to a temperature which is above the limit temperature up to which the emulsion to be made is stable and above the coagulation temperature or solidification temperature of the liquid. This liquid may, for example, be a melted fat or wax at a temperature of about C. The stirring tool is then allowed to run so that the liquid is whirled or rolled around. Another liquid, which is to be emulsified, for example an aqueous solution, is now supplied via the supply pipe. This other liquid has a temperature below the said limit temperature and/or below the coagulation temperature or solidification temperature of the liquid in the vessel. One may also, for example, with an arrangement according to FIG. 2 or with single nozzles according to FIG. 3 supply several liquids simultaneously; in this case at least one and preferably all of the liquids supplied should then have a temperature below the said value. As a rule the liquid to be emulsified may be introduced cold, that is at about room temperature or tap water temperture. In the manner stated immediately with the commencement of the introduction of the liquid to be emulsified, so long as the liquid in the vessel is still hot, a good parent emulsion can be obtained. With increasing quantity of liquid introduced the temperature of course dops gradually. Surprisingly however it is nevertheless possible without difficulties to emulsify further quantities of cold liquid after the parent emulsion" is formed, although as a rule small quantities of suitable emulsifier must be added.

It is also possible to interchange the heated liquid and the relatively cold liquid, i.e. the cold liquid may be placed in the vessel and the heated liquid, such as fat or wax, may be gradually introduced via the supply pipe and nozzle. If it is intended to carry out this mode of operation, heating means may be provided for heating the supply pipe.

It is possible in the manner described to emulsify a liquid in almost any desired quantity into the liquid in the vessel. One may, for example, produce an emulsion from fat and an aqueous solution in which the constituent parts are present in the weight ratio of 3 l to l 3 and which is solid at room temperature in that the fat forms the outer phase. One may however also increase the quantity of the aqueous liquid up to a weight ratio of 2 8 to l 9. The emulsion then changes, that is, the fat forms the inner phase so that the finished emulsion is liquid at room temperature.

One liquid is thus always used at a temperature which is substantially lower than the temperature of the heated other liquid, for example, by at least 25C preferably at least 50C lower. In most cases the cold liquid may be suitably used at room temperature or tap water temperature In the manner described an emulsion may as a rule be produced in a few minutes. After completion of the introduction of the second liquid the emulsion is ready and no longer requires cooling whilst stirring in contradistinction to the cooling times of several hours which were frequently heretofore necessary in the manufacture of emulsions in accordance with known methods and in known apparatus which did not permit the use of liquids at substantially different temperatures.

What is claimed is:

1. Apparatus for the manufacture of an emulsion from a first bath liquid and a second feed liquid immiscible with said first liquid, one of said liquids being heated and the other liquid being relatively cool, said apparatus comprising:

a mixing and homogenizing tool immersed in said first liquid comprising an annular stator and a stirring member disposed in said stator, the stator having an inlet side and an outlet side, and said stirring member being rotatable to form a draw in area for drawing said first liquid from said inlet side into said mixing and homogenizing tool,

and at least one nozzle disposed at said inlet side of said stator and having a nozzle opening of shape and position to introduce said second liquid in fine distribution in the draw in area of said stirring member so that said second liquid is drawn into said mixing and homogenizing tool together with said first liquid and thoroughly mixed therewith in said tool before said liquids are thrust out at said outlet side,

said nozzle having an annular gap which is formed by the inner peropheries of coaxial annular plates which are fixed to said inlet side of said stator, said nozzle gap being divided in the peripheral direction into at least two sector-like chambers each of which is connected to a separate supply pipe for different liquids.

2. Apparatus for the manufacture of an emulsion from a first bath liquid and a second feed liquid immiscible with said first liquid, one of said liquids being heated and the other liquid being relatively cool, said apparatus comprising:

a mixing and homogenizing tool immersed in said first liquid comprising an annular stator and a stirring member disposed in said stator, the stator having an inlet side and an outlet side, sand said stirring member being rotatable to form a draw in area for drawing said first liquid from said inlet side into said mixing and homogenizing tool,

and at least one nozzle disposed at said inlet side of said stator and having a nozzle opening of shape and position to introduce said second liquid in fine distribution in the draw in area of said stirring member so that said second liquid is drawn into said mixing and homogenizing tool together with said first liquid and thoroughly mixed therewith in said tool before said liquids are thrust out at said outlet side,

said nozzle having an annular gap which is formed by the inner peripheries of coaxial annular plates which are fixed to said inlet side of said stator, said annular gap being disposed surrounding said draw in area of said stirring member in such manner that said first liquid sucked by the stirring member and flowing past the annular gap produces a low pressure in the noule in order to suck in said second liquid through a supply pipe connected to said nozzle.

3. Apparatus for the manufacture of an emulsion from a first bath liquid and a second feed liquid immiscible with said first liquid, one of said liquids being heated and the other liquid being relatively cool, said apparatus comprising:

a mixing and homogenizing tool immersed in said first liquid comprising an annular stator and a stirring member disposed in said stator, the stator having an inlet side and an outlet side, and said stirring member being rotatable to form a draw in area for drawing said first liquid from said inlet side into said mixing and homogenizing tool,

and a ring of separate nozzles disposed annularly around said draw in area of said stirring member,

said nozzles having nozzle openings of shape and position to introduce said second liquid in fine distribution in the draw in area of said stirring member so that said second liquid is drawn into said mixing and homogenizing tool together with said first liquid and thoroughly mixed therewith in said tool before said liquids are thrust out at said outlet side.

I I l i

Claims (3)

1. Apparatus for the manufacture of an emulsion from a first bath liquid and a second feed liquid immiscible with said first liquid, one of said liquids being heated and the other liquid being relatively cool, said apparatus comprising: a mixing and homogenizing tool immersed in said first liquid comprising an annular stator and a stirring member disposed in said stator, the stator having an inlet side and an outlet side, and said stirring member being rotatable to form a draw in area for drawing said first liquid from said inlet side into said mixing and homogenizing tool, and at least one nozzle disposed at said inlet side of said stator and having a nozzle opening of shape and position to introduce said second liquid in fine distribution in the draw in area of said stirring member so that said second liquid is drawn into said mixing and homogenizing tool together with said first liquid and thoroughly mixed therewith in said tool before said liquids are thrust out at said outlet side, said nozzle having an annular gap which is formed by the inner peropheries of coaxial annular plates which are fixed to said inlet side of said stator, said nozzle gap being divided in the peripheral direction into at least two sector-like chambers each of which is connected to a separate supply pipe for different liquids.
2. APPARATUS FOR THE MANUFACTURE OF AN EMULSION FROM A FIRST BATH LIQUID AND A SECOND FEED LIQUID IMMISCIBLE WITH SAID FIRST LIQUID, ONE OF SAID LIQUIDS BEING HEATED AND THE OTHER LIQUID BEING RELATIVELY COOL, SAID APPARATUS COMPRISING: A MIXING AND HOMOGENIZING TOOL IMMERSED IN SAID FIRST LIQUID COMPRISING AN ANNULAR STATOR AND A STIRRING MEMBER DISPOSED IN SAID STATOR, THE STATOR HAVING AN INLET SIDE AND AN OUTLET SIDE, SAND SAID STIRRING MEMBER BEING ROTATABLE TO FORM A DRAW IN AREA FOR DRAWING SAID FIRST LIQUID FROM SAID INLET SIDE INTO SAID MIXING AND HOMOGENIZING TOOL, AND AT LEAST ONE NOZZLE DISPOSED AT SAID INLET SIDE OF SAID STATOR AND HAVING A NOZZLE OPENING OF SHAPE AND POSITION TO INTRODUCE SAID SECOND LIQUID IN FINE DISTRIBUTION IN THE DRAW IN AREA OF SAID STIRRING MEMBER SO THAT SAID SECOND LIQUID IS DRAWN INTO SAID MIXING AND HOMOGENIZING TOOL TOGETHER WITH SAID FIRST LIQUID AND THOROUGHLY MIXED THEREEITH IN SAID TOOL BEFORE SAID LIQUIDS ARE THRUST OUT AT SAID OUTLET SIDE, SAID NOZZLE HAVING AN ANNULAR GAP WHICH IS FORMED BY THE INNER PERIPHERIES OF COAXIAL ANNULAR PLATES WHICH ARE FIXED TO SAID INLET SIDE OF SAID STATOR, SAID ANNULAR GAP BEING DISPOSED SURROUNDING SAID DRAW IN AREA OF SAID STIRRING MEMBER IN SUCH MANNER THAT SAID FIRST LIQUID SUCKED BY THE STIRRING MEMBER AND FLOWING PAST THE ANNULAR GAP PRODUCES A LOW PRESSURE IN THE NOZZLE IN ORDER TO SUCK IN SAID SECOND LIQUID THROUGH A SUPPLY PIPE CONNECTED TO SAID NOZZLE.
3. Apparatus for the manufacture of an emulsion from a first bath liquid and a second feed liquid immiscible with said first liquid, one of said liquids being heated and the other liquid being relatively cool, said apparatus comprising: a mixing and homogenizing tool immersed in said first liquid comprising an annular stator and a stirring member disposed in said stator, the stator having an inlet side and an outlet side, and said stirring member being rotatable to form a draw in area for drawing said first liquid from said inlet side into said mixing and homogenizing tool, and a ring of separate nozzles disposed annularly around said draw in area Of said stirring member, said nozzles having nozzle openings of shape and position to introduce said second liquid in fine distribution in the draw in area of said stirring member so that said second liquid is drawn into said mixing and homogenizing tool together with said first liquid and thoroughly mixed therewith in said tool before said liquids are thrust out at said outlet side.
US39115873 1970-06-01 1973-08-23 Apparatus for the manufacture of emulsions Expired - Lifetime US3925243A (en)

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CH815970A CH500756A (en) 1970-06-01 1970-06-01 A process for the preparation of an emulsion
US14585371A true 1971-05-21 1971-05-21
US39115873 US3925243A (en) 1970-06-01 1973-08-23 Apparatus for the manufacture of emulsions

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US5241992A (en) * 1992-07-14 1993-09-07 Eastman Kodak Company Apparatus and method for distributing fluids
US5358329A (en) * 1993-02-12 1994-10-25 Fluid Dynamics, Inc. Apparatus for mixing plural flowable materials
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