US3374172A - Oil additives - Google Patents

Oil additives Download PDF

Info

Publication number
US3374172A
US3374172A US540824A US54082466A US3374172A US 3374172 A US3374172 A US 3374172A US 540824 A US540824 A US 540824A US 54082466 A US54082466 A US 54082466A US 3374172 A US3374172 A US 3374172A
Authority
US
United States
Prior art keywords
additive
oil
extreme pressure
salt
lubricating oil
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US540824A
Other languages
English (en)
Inventor
Roberts Kenneth Charles
White Albert William
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anchor Chemical Co Ltd
Original Assignee
Anchor Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anchor Chemical Co Ltd filed Critical Anchor Chemical Co Ltd
Application granted granted Critical
Publication of US3374172A publication Critical patent/US3374172A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M1/00Liquid compositions essentially based on mineral lubricating oils or fatty oils; Their use as lubricants
    • C10M1/08Liquid compositions essentially based on mineral lubricating oils or fatty oils; Their use as lubricants with additives
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10Carboxylix acids; Neutral salts thereof
    • C10M2207/12Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10Carboxylix acids; Neutral salts thereof
    • C10M2207/12Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/129Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of thirty or more carbon atoms
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10Carboxylix acids; Neutral salts thereof
    • C10M2207/16Naphthenic acids
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2211/00Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2211/02Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions containing carbon, hydrogen and halogen only
    • C10M2211/022Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions containing carbon, hydrogen and halogen only aliphatic
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2211/00Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2211/04Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions containing carbon, hydrogen, halogen, and oxygen
    • C10M2211/044Acids; Salts or esters thereof
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2211/00Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2211/06Perfluorinated compounds
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2213/00Organic macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2213/02Organic macromolecular compounds containing halogen as ingredients in lubricant compositions obtained from monomers containing carbon, hydrogen and halogen only
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2213/00Organic macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2213/06Perfluoro polymers
    • C10M2213/062Polytetrafluoroethylene [PTFE]
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/02Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
    • C10M2219/024Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds of esters, e.g. fats
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00Metal present as such or in compounds
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00Metal present as such or in compounds
    • C10N2010/04Groups 2 or 12
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00Specified use or application for which the lubricating composition is intended
    • C10N2040/20Metal working
    • C10N2040/22Metal working with essential removal of material, e.g. cutting, grinding or drilling

Definitions

  • An object of the present invention is to reduce or inhibit the staining and corrosion described above.
  • an extreme pressure oil additive for lubricating oils and cutting fluids comprising a liquid chlorinated or sulphochlorinated compound and an organic salt of a Group II metal which salt is soluble in the chlorinated or sulphochlorinated compound and in the lubricating oil or cutting fluid.
  • Suitable metal salts are the calcium, barium and zinc salts of naphthenic acids, though other metals of Group II, for example cadmium, and other organic acids, especially aliphatic carboxylic acids, both saturated and unsaturated for example 2-ethyl hexoic, lauric and stearic, oleic and linoleic acids, may be used, provided that the requirement of adequate solubility in mineral oil is met.
  • Effective amounts of the Group II organic salt lie in the range 1.0 to 60.0 parts by Weight 100 parts of chlorinated additive, and it may be applied either in the form of the pure salt, or, preferably, as a commercially available concentrate.
  • the extreme pressure oil additive may also contain an amount of lubricating oil or cutting fluid to facilitate dispersal of the additive when applied.
  • Group II metals have the secondary advantage of low toxicity--a valuable feature, particularly in cutting fluids.
  • Chlorinated additives in which the invention is of outstanding value are sulpho-ehlorinated fatty oils (the reaction product of a fatty oil and sulphur mono-chloride) 3,374,172 Patented Mar. 19, 1968 but the scope of the invention is not limited to use of the stabiliser in additives of this type.
  • Example I A blend of mineral oil 92 parts by weight, sulphochlorinated sperm oil 8 parts by weight and an oil-soluble organic salt of a Group II metal 0.7 part by weight was spread as a film on a standard steel plate (a Beeny plate) in presence of standard steel chippings, and the whole was stored in a closed air space over water for 48 hours. The following results were observed:
  • Example II A liquid chlorinated propylene tetramer containing 40% by weight of chlorine was tested, as a 10% solution in a reference mineral oil, on a Beeny plate under the same conditions as above, both with and without additives according to the invention.
  • the additive-free solution stained the plate, whereas solutions containing respectively 1% by weight of calcium naphthenate, barium laurate and calcium stearate produced no evidence of stains.
  • Example III Under similar conditions a chlorinated sperm oil containing 30% by weight of chlorine stained the plate slightly while solutions containing 1% of calcium naphthenate and barium laurate were non-staining.
  • Example IV A sulpho-chlorinated methyl fatty ester under the above conditions stained the plate but in the presence of 1% calcium naphthenate no trace of staining was evident.
  • An extreme pressure oil additive for lubricating oils and cutting fluids comprising (a) a liquid reaction product of sulphur monochloride and a fatty ester, in an amount suflicient to impart extreme pressure properties when the additive is incorporated in a lubricating oil or cutting fluid, and
  • a salt soluble in the sulpho-chlorinated product and in the lubricating oil or cutting fluid, of a Group II metal and an acid selected from the group consisting of naphthenic acids and aliphatic carboxylic acids, said salt being present in an amount sufficient to prevent stain when the additive is incorporated in a lubricating oil or cutting fluids.
  • An extreme pressure lubricating oil or cutting fluid containing an additive as claimed in claim 1.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)
US540824A 1965-04-09 1966-04-07 Oil additives Expired - Lifetime US3374172A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB15300/65A GB1088759A (en) 1965-04-09 1965-04-09 Improvements relating to oil additives

Publications (1)

Publication Number Publication Date
US3374172A true US3374172A (en) 1968-03-19

Family

ID=10056632

Family Applications (1)

Application Number Title Priority Date Filing Date
US540824A Expired - Lifetime US3374172A (en) 1965-04-09 1966-04-07 Oil additives

Country Status (5)

Country Link
US (1) US3374172A (enrdf_load_stackoverflow)
BE (1) BE679332A (enrdf_load_stackoverflow)
DE (1) DE1594333A1 (enrdf_load_stackoverflow)
GB (1) GB1088759A (enrdf_load_stackoverflow)
NL (1) NL6604733A (enrdf_load_stackoverflow)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NZ186808A (en) * 1977-04-06 1979-10-25 Rocol Ltd Lubricant composition containing group ii-a metal carbonate and halogenated organic lubricant

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2276341A (en) * 1938-12-21 1942-03-17 Lubri Zol Dev Corp Lubricating composition
US2360905A (en) * 1942-09-25 1944-10-24 Gulf Oil Corp Manufacture of sulpho-halogenated aliphatic monoesters
US2433853A (en) * 1944-11-23 1948-01-06 Lubri Zol Dev Corp Sulfurized oils
US2995516A (en) * 1955-03-08 1961-08-08 Standard Oil Co Cutting oil containing calcium stearate
US3017361A (en) * 1956-09-05 1962-01-16 Texaco Inc Non-squawking automatic transmission fluid

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2276341A (en) * 1938-12-21 1942-03-17 Lubri Zol Dev Corp Lubricating composition
US2360905A (en) * 1942-09-25 1944-10-24 Gulf Oil Corp Manufacture of sulpho-halogenated aliphatic monoesters
US2433853A (en) * 1944-11-23 1948-01-06 Lubri Zol Dev Corp Sulfurized oils
US2995516A (en) * 1955-03-08 1961-08-08 Standard Oil Co Cutting oil containing calcium stearate
US3017361A (en) * 1956-09-05 1962-01-16 Texaco Inc Non-squawking automatic transmission fluid

Also Published As

Publication number Publication date
BE679332A (enrdf_load_stackoverflow) 1966-09-16
GB1088759A (en) 1967-10-25
NL6604733A (enrdf_load_stackoverflow) 1966-10-10
DE1594333A1 (de) 1970-07-23

Similar Documents

Publication Publication Date Title
US3310489A (en) Lubricant composition
EP0227182B1 (en) Crease composition
US2897152A (en) Lubricating oils
US4274973A (en) Aqueous water-soluble soap lubricant concentrates and aqueous lubricants containing same
GB1009197A (en) Stable water-in-oil emulsion
GB782879A (en) Anti-corrosion compositions
GB906208A (en) Highly basic magnesium-containing additive agents and their use
US3769214A (en) Aqueous lubricant compositions containing alkanolamine salts of carboxylic acids
US2383033A (en) Lubricants
US3256187A (en) Cutting fluid
JPH0665589A (ja) 水溶性切削油組成物
US3544609A (en) Zinc complexes
US3374172A (en) Oil additives
US3050465A (en) Water-in-oil emulsion hydraulic fluids
US2951808A (en) Lubricant compositions containing metal salts of aromatic hydroxy carboxylic acids as antioxidants
US3776847A (en) Lubricating oil composition
GB1179374A (en) Anticorrosive for Lubricants
US2516838A (en) Soluble oil base
US4501677A (en) Heterocyclic nitrogen compounds--organometallic salt complexes as corrosion inhibitors in lubricating oils
US2298636A (en) Lubricating composition
US3184409A (en) Hydrocarbon compositions containing iodine as an antifriction agent
US3359202A (en) Lubricating compositions
US3278432A (en) Extreme pressure lubricants containing sulfur
US2371854A (en) Mineral oil composition
US3493507A (en) Grease compositions