US301174A - Territory - Google Patents

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US301174A
US301174A US301174DA US301174A US 301174 A US301174 A US 301174A US 301174D A US301174D A US 301174DA US 301174 A US301174 A US 301174A
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Prior art keywords
cylinder
alum
coating
spencer
interior
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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00Compounds of aluminium
    • C01F7/68Aluminium compounds containing sulfur
    • C01F7/74Sulfates

Definitions

  • Fig. 1 is an end elevation.
  • Fig. 2 is a vertical longitudinal section.
  • Fig. 3 is a detail.
  • Fig. 4 is a vertical cross-section.
  • Fig. 5 is a top view of two of the rollers.
  • My process consists in placing the alum to be desiccated in a revolving cylinder, which is to be subjected to a heat sufficient to melt the alum, which will flow evenly over the in- 3 5 terior surface of the cylinder, forming a coat ing thereon, which may be about one-half an inch thick, and which can be easily detached from the cylinder and removed therefrom when sufficiently dry.
  • A represents a revolving cylinder, which may be made of cast iron, about one inch thick. As shown,this cylinder is supposed to be eight feet long and four feet in diameter. The cylinder is surrounded with brick-work 13.
  • O is a furnace located at one side of the cylinder.
  • D is a passage for smoke and heat, which passes nearly around the cylinder.
  • E is a smoke-pipe.
  • a b are flanges upon the opposite ends of the cylinder.
  • F is a head upon one end of the cylinder, bolted to the flange a.
  • c is a hollow cylindrical part or journal, extending out from thehcad F, and preferably cast therewith.
  • d is a removable cover upon the outer end of the part c, which,'when in place, may be held in any suitable manner.
  • G is a head at the opposite end of the cylinder, and is bolted to the flange b. This head is also provided with a hollow cylindrical journal or part c.
  • f are friction-rollers arranged in the brick- 6 work, upon which the parts 0 0 rest and rotate.
  • H is a gear-wheel, permanently attached to the part c, which extends out beyond the brickwork.
  • I is a pipe, supported in any suitable manc nor, the inner end, 9, of which enters the part a, but is not connected therewith.
  • J is a coating of alum on the interior of the cylinder.
  • a quantity of So alum is to be placed in the cylinder when at rest, which can be done by removing the cover d, the alum being thrown in through the hollow part c, after which the cover is to be replaced and secured in position.
  • the cylinder is to be rotated in any suitable manner, which may be done by means of a gear-wheel, which is not shown, engaging with the bevel-wheel H.
  • a suitable fire being provided in the furnace, the alum in the cylinder will be melted, 0 and will be evenly distributed upon, and will adhere to the interior surface of the cylinder, forming a coating thereon, the thickness of which will of course depend upon the quantity of alum in the cylinder.
  • the alum After the alum has been first melted, and during the earlier stages of the drying process, its consistency is such that it will drip more or less from the upper part of the cylinder, and the inclined projections i 70 serve the office of directing the drippings a little inward from the extreme ends of the cylinder.
  • the coating upon the interior of the cylinder is continuous, and it is evident that if it be, say, half an inch thick there will be a self-supporting tendency in addition to the adhesion to the surface of the cylinder; but this selfsupporting tendency will only continue so long as the alum remains unbroken. I am thus able, rapidly and efficientl y, to desiccate alum, all parts being thoroughly dried without any danger of burning.

Description

(No Model.) 3 Sheets-Sheet 1.
,A. E. SPENCER.
1 DESIGGATING ALUM. I -'W1,174. Patented July 1, 1884.
may 8.91966 ajllegn-t f PETERS, Pmmumu mr, WashingImL o c.
3 Sheets-Sheet 3.
(No Model.)
' A. E. SPENCER.
DESIGGATING ALUM.
Patented July 1, 1884.
$44M aaww.
lharrniu df'ra'rns Fa'rnti'r tries.
AROHELAUS E. SPENCER, OF CHICAGO, ILLINOIS, ASSIGNOR TO D'ERAEJTUS II. SPENCER, JR., OF CORINN E, UTAH TERRITORY.
DESICCATING ALUM.
SPECIFICATION forming part of Letters Patent No. 301,174, dated July 1, 1884:.
Application filed October 26, 1853. (No model.)
To all whom it ntay concern.-
Be it known that I, ARGIIELAUS E. Srnnonn, resi ding at Chicago, in the county of Cook and State of Illinois, and a citizen of the United States, have invented new and useful Improvements in Desiccating Alum, of which the following is a full description, reference being had to the accompanying drawings, in which-- Figure 1 is an end elevation. Fig. 2 is a vertical longitudinal section. Fig. 3 is a detail. Fig. 4 is a vertical cross-section. Fig. 5 is a top view of two of the rollers.
In Fig. ,4 I have shown a coating of alum on the interior of the cylinder, which coating T 5 is not shown in Fig. 2. Commercial alum usually contains about forty-seven per cent. of
Water of crystallization, and for some uses it.
is desirable and customary to expel the greater portion of such moisture, which has heretofore been done by placing the alum in shallow pans and exposing the same to heat in an oven. In such case the central portion of the alum in each pan does not dry as rapidly as other parts, and if the process be continued long 2 5 enough to dry the center thoroughly there is danger of burning portions of the alum. I have discovered a much more efficient method of desiccating alum than any heretofore used, and have also made some improvements in machinery for that purpose.
My process consists in placing the alum to be desiccated in a revolving cylinder, which is to be subjected to a heat sufficient to melt the alum, which will flow evenly over the in- 3 5 terior surface of the cylinder, forming a coat ing thereon, which may be about one-half an inch thick, and which can be easily detached from the cylinder and removed therefrom when sufficiently dry.
I11 the drawings, A represents a revolving cylinder, which may be made of cast iron, about one inch thick. As shown,this cylinder is supposed to be eight feet long and four feet in diameter. The cylinder is surrounded with brick-work 13.
O is a furnace located at one side of the cylinder.
D is a passage for smoke and heat, which passes nearly around the cylinder.
E is a smoke-pipe.
a b are flanges upon the opposite ends of the cylinder.
F is a head upon one end of the cylinder, bolted to the flange a.
c is a hollow cylindrical part or journal, extending out from thehcad F, and preferably cast therewith.
d is a removable cover upon the outer end of the part c, which,'when in place, may be held in any suitable manner.
G is a head at the opposite end of the cylinder, and is bolted to the flange b. This head is also provided with a hollow cylindrical journal or part c.
f are friction-rollers arranged in the brick- 6 work, upon which the parts 0 0 rest and rotate.
H is a gear-wheel, permanently attached to the part c, which extends out beyond the brickwork.
I is a pipe, supported in any suitable manc nor, the inner end, 9, of which enters the part a, but is not connected therewith.
h is a damper in the pipe I.
Upon the inside of the head F there is, as shown, an inwardlydnclined projection, t, and upon the other head there is a similar projection, It. V
J is a coating of alum on the interior of the cylinder.
The operation is as follows: A quantity of So alum is to be placed in the cylinder when at rest, which can be done by removing the cover d, the alum being thrown in through the hollow part c, after which the cover is to be replaced and secured in position. The cylinder is to be rotated in any suitable manner, which may be done by means of a gear-wheel, which is not shown, engaging with the bevel-wheel H. A suitable fire being provided in the furnace, the alum in the cylinder will be melted, 0 and will be evenly distributed upon, and will adhere to the interior surface of the cylinder, forming a coating thereon, the thickness of which will of course depend upon the quantity of alum in the cylinder. Inacylinder of .thesize 5 shown I place about one hundred pounds of alum to be dried, and that quantity will form a coating upon the interior of the cylinder about one-half an inch thick. \Vith a hot fire the quantity of alum mentioned will be IOO thoroughly desiccated in one hour. The eX- pelled moisture will pass off through c and the tube I. When the alum is sufficiently dry, I stop the cylinder and remove the cover d. The alum does not adhere very tenaciously to the cylinder, and can be readily detached therefrom by means of a scraper, and can be readily removed from the cylinder through the hollow part 0. After the alum has been first melted, and during the earlier stages of the drying process, its consistency is such that it will drip more or less from the upper part of the cylinder, and the inclined projections i 70 serve the office of directing the drippings a little inward from the extreme ends of the cylinder. The coating upon the interior of the cylinder is continuous, and it is evident that if it be, say, half an inch thick there will be a self-supporting tendency in addition to the adhesion to the surface of the cylinder; but this selfsupporting tendency will only continue so long as the alum remains unbroken. I am thus able, rapidly and efficientl y, to desiccate alum, all parts being thoroughly dried without any danger of burning.
WVhat I claim as new, and desire to secure by Letters Patent, is as follows:
The within-described process of desiccating alum, consisting in introducing the alum into a cylinder, then melting the same by heat applied to the outside of the cylinder, and then distributing the melted alum over the interior surface of the cylinder by. rotation of the cyls.
inder to dry the alum, substantially as described.
ARGHELAUS E. SPENCER. \Vitnesses:
ALBERT I-I. ADAMS, 0. WV. Bonn.
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2441022A (en) * 1943-07-12 1948-05-04 Phelps Dodge Corp Drying alum

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2441022A (en) * 1943-07-12 1948-05-04 Phelps Dodge Corp Drying alum

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