US2922044A - Calutron - Google Patents

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US2922044A
US2922044A US270201A US27020152A US2922044A US 2922044 A US2922044 A US 2922044A US 270201 A US270201 A US 270201A US 27020152 A US27020152 A US 27020152A US 2922044 A US2922044 A US 2922044A
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arc
plates
block
calutron
ions
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US270201A
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Edward J Lofgren
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Priority claimed from US668112A external-priority patent/US2874296A/en
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J49/00Particle spectrometers or separator tubes
    • H01J49/26Mass spectrometers or separator tubes
    • H01J49/28Static spectrometers
    • H01J49/30Static spectrometers using magnetic analysers, e.g. Dempster spectrometer

Definitions

  • the practice is to pass a stream of vapor or gas to be ionized to or into the vicinity of an electric arc.
  • The are is customarily of columnar form struck between a filamentary cathode and an anode spaced apart in the direction of a magnetic field in which the entire structure functions. Ions are produced by collisions of the gas or vapor molecules with particles occurring in the arc and are removed from the are or its vicinity under the urgency of an electric accelerating field.
  • This field is established between the arc mechanism and one or more, usually two, accelerating electrodes spaced from the arc mechanism in the general direction of propagation of an ion beam constituted by the withdrawn ions.
  • an ion source of the described kind is accompanied by the production of large quantities of heat.
  • the resulting high temperatures have deleterious effects upon the materials of the arc mechanism and shorten the life of the arc structure to an uneconomic extent.
  • the various particles generated by the operation of the arc bombard or sputter upon the adjacent mechanical surfaces cause deterioration and erosion of an undesirable sort and quantity.
  • the ion stream flowing from the arc block tends to erode and vary the shape of the surfaces of the aperture or orifice through which the ions emerge. Since these surfaces are efiective to establish the contour of the electric field existing in the vicinity and since the contour of such field is instrumental in controlling the particular shape and focus of the ion beam, imperfect and improper action of the mechanism occurs after only a short initial operation.
  • An additional object of the invention is to provide means for insuring a protracted operation of the ionizing mechanism without substantial interference with the trajectory or pattern of the ion beam.
  • An additional object of the invention is in general to improve arc ionizing mechanisms.
  • a still further object of the invention is to improve calutrons in general.
  • Figure 1 is a diagrammatic showing of the'ion source portion of a calutron, the showing being in isometric perspective with portions of the structure being omitted for clarity.
  • Fig. 2 is a section on a horizontal plane of an ion source mechanism for a calutron in diagrammatic form.
  • an ion source mechanism incorporating a source block 6 preferably fabricated of metal having a good thermal conductivity such as copper and mechanically supported upon a mounting stem 7 also serving as an electrical conductor.
  • the source block 6 is formed with a normally covered charge cavity 8 within which material to be ionized is placed. Customarily, the material is in a separate container or charge bottle containing granular material that evolves gas or vapor when heated.
  • the charge block 6 is provided with a plurality of heaters 9 efiective to increase the charge temperature to the gasifying or vaporizing point.
  • Gas so evolved flows from the charge chamber 8 through a passage 11 into a normally covered gas distribution and arc chamber 12 likewise constituted by a cavity in the arc block 6.
  • a filamentary cathode 13 disposed in the end of a cathode stem 14 carrying appropriate electrical leads and maintained, by means of a filament supply 2 and an arc supply 3, at the proper potential with respect to the arc block 6 that the block also serves as an arc anode.
  • the position of the arc in the block is shown approximately by the stippled area 16 in Fig. 1.
  • Ions formed adjacent the are withdrawn from the arc block 6 through an opening 17 leading from the arc chamber 12 to the exterior of the block and being formed and defined by the facing edges of the forward coplanar walls 18 and 19 of the arc block.
  • the margins of the opening 17 are further defined by a pair of coplanar plates 21 and 22 defining a somewhat narrower slot 23 and preferably fabricated of a metal having a higher resistance to temperature efiects than the copper of the block 6 and thus being preferably made of molybdenum.
  • the plates 21 and 22 are held in intirnate contact with the walls 18 and 19 in order to facilitate thermal transfer from the plates to the block.
  • the further margins of the opening are defined by a supplementary pair of plates 24 and 26, respectively, having their facing edges 27 and 28 bevelled to define a dihedral angle.
  • the plates 24 and 26 are preferably formed of a metal such as copper having a high heat absorptive and transmitting property and are maintained in intimate thermal contact with the plates 21 and 22.
  • the narrowest portion 23 of the arc slit is defined by resistant plates 21 and 22. Overheating of these plates is prevented by the ability of the adjacent plates, for example, 19 and 26 to carry away rapidly the heat imposed upon the intermediate plate 22.
  • This laminated construction has been found in practice to increase the length of the arc aezaosa 51i! very materially, and. to resist erosion so that the original surfaces defining the arc slit are not interfered with by operation for a protracted period.
  • an ion source for a calutron comprising an arc block defining an arc chamber having an exit opening formed by bevelled edges of the arc block that converge in the outward direction from said are chamber, means for creating an electron stream in the arc chamber, means for supplying an ionizable charge to the arc chamber, and an ion accelerating electrode disposed near the arc block opposite the exit opening.

Description

E. J. LOFGREN Jan. 19, 1960 CALUTRON Original Filed May 8, 1946 INVENTOR. EDWARD J. LOFGREN FILAMENT SUPPLY ARG SUPPLY AOGELERATING VOLTAGE SUPPLY 35 ATTORNEY.
CALUTRON Edward J. Lofgren, Albany, Ca1if., assignor to the United States of America as represented by the United States Atomic Energy Commission Original application May 8, 1946, Serial No. 668,112, new Patent No. 2,874,296, dated February 17, 1959. Divided and this application February 6, 1952, Serial No. 270,201
2 Claims. (Cl. 250-413) This invention relates to means for producing ions from an ionizable material, and especially to ionizing means employing an electric are as an ionizing agent. Devices of this character are particularly disclosed and explained in US. Patent No. 2,709,222, issued to Ernest 0. Lawrence, on May 24, 1955, and in which Figures 3 to 5 of the drawings and the accompanying description especially characterize a structure to which the present disclosure is most applicable. This is a divisional application of my copending application Serial No. 668,112, filed May 8, 1946, for Calutrons and issued February 17, 1959, as US. Patent 2,874,296.
In devices of this nature the practice is to pass a stream of vapor or gas to be ionized to or into the vicinity of an electric arc. The are is customarily of columnar form struck between a filamentary cathode and an anode spaced apart in the direction of a magnetic field in which the entire structure functions. Ions are produced by collisions of the gas or vapor molecules with particles occurring in the arc and are removed from the are or its vicinity under the urgency of an electric accelerating field. This field is established between the arc mechanism and one or more, usually two, accelerating electrodes spaced from the arc mechanism in the general direction of propagation of an ion beam constituted by the withdrawn ions.
The operation of an ion source of the described kind is accompanied by the production of large quantities of heat. The resulting high temperatures have deleterious effects upon the materials of the arc mechanism and shorten the life of the arc structure to an uneconomic extent. Also the various particles generated by the operation of the arc bombard or sputter upon the adjacent mechanical surfaces and cause deterioration and erosion of an undesirable sort and quantity. In addition the ion stream flowing from the arc block tends to erode and vary the shape of the surfaces of the aperture or orifice through which the ions emerge. Since these surfaces are efiective to establish the contour of the electric field existing in the vicinity and since the contour of such field is instrumental in controlling the particular shape and focus of the ion beam, imperfect and improper action of the mechanism occurs after only a short initial operation.
It is therefore an object of the invention to provide means for withstanding the ravages of the quantities of heat, erosion and deterioration concomitant with the operation of an ion source of the calutron type.
An additional object of the invention is to provide means for insuring a protracted operation of the ionizing mechanism without substantial interference with the trajectory or pattern of the ion beam.
An additional object of the invention is in general to improve arc ionizing mechanisms.
A still further object of the invention is to improve calutrons in general.
Other objects of the invention together with the foregoing are attained by the embodiments of the invention United rates Patent 0 M Patented Jan. 19, 1960 disclosed in the accompanying description and drawings in the latter of which:
Figure 1 is a diagrammatic showing of the'ion source portion of a calutron, the showing being in isometric perspective with portions of the structure being omitted for clarity.
Fig. 2 is a section on a horizontal plane of an ion source mechanism for a calutron in diagrammatic form.
Since the general construction of a calutron and the detailed arrangement of the portions constituting the environment of the present inventive embodiment are well disclosed in the identified patent to Lawrence, and play no immediate part in the present invention, reference is herein had only to a diagrammatic showing for simplicity in understanding and clarity of disclosure. It is understood that the entire mechanism operates in a magnetic field, is suppled with electricity in various appropriate circuits, and is, except for the parts referred to specifically herein, like the structure shown in the Lawrence patent.
There is provided an ion source mechanism incorporating a source block 6 preferably fabricated of metal having a good thermal conductivity such as copper and mechanically supported upon a mounting stem 7 also serving as an electrical conductor. The source block 6 is formed with a normally covered charge cavity 8 within which material to be ionized is placed. Customarily, the material is in a separate container or charge bottle containing granular material that evolves gas or vapor when heated.
To produce the desired effect the charge block 6 is provided with a plurality of heaters 9 efiective to increase the charge temperature to the gasifying or vaporizing point. Gas so evolved flows from the charge chamber 8 through a passage 11 into a normally covered gas distribution and arc chamber 12 likewise constituted by a cavity in the arc block 6. To strike an appropriate are there is arranged above the arc block 6 a filamentary cathode 13 disposed in the end of a cathode stem 14 carrying appropriate electrical leads and maintained, by means of a filament supply 2 and an arc supply 3, at the proper potential with respect to the arc block 6 that the block also serves as an arc anode. The position of the arc in the block is shown approximately by the stippled area 16 in Fig. 1.
Ions formed adjacent the are are withdrawn from the arc block 6 through an opening 17 leading from the arc chamber 12 to the exterior of the block and being formed and defined by the facing edges of the forward coplanar walls 18 and 19 of the arc block. The margins of the opening 17 are further defined by a pair of coplanar plates 21 and 22 defining a somewhat narrower slot 23 and preferably fabricated of a metal having a higher resistance to temperature efiects than the copper of the block 6 and thus being preferably made of molybdenum. The plates 21 and 22 are held in intirnate contact with the walls 18 and 19 in order to facilitate thermal transfer from the plates to the block. Additionally, the further margins of the opening are defined by a supplementary pair of plates 24 and 26, respectively, having their facing edges 27 and 28 bevelled to define a dihedral angle. The plates 24 and 26 are preferably formed of a metal such as copper having a high heat absorptive and transmitting property and are maintained in intimate thermal contact with the plates 21 and 22.
By the provision of this arrangement the narrowest portion 23 of the arc slit is defined by resistant plates 21 and 22. Overheating of these plates is prevented by the ability of the adjacent plates, for example, 19 and 26 to carry away rapidly the heat imposed upon the intermediate plate 22. This laminated construction has been found in practice to increase the length of the arc aezaosa 51i! very materially, and. to resist erosion so that the original surfaces defining the arc slit are not interfered with by operation for a protracted period.
:are attained in the modified ltembodiment disclosed in Fig. 2 wherein for the most part the structure is identical except that the are shown by the stippled 'portion fil is related to a pair of arc slit defining plates 32 and 33 in vsuch a fashion that many of the ions withdrawn by accelerating electrodes 34 and 36, suitably supplied by accelerating voltage supply 35, do not directly impinge upon the plates 32 and 33. r
This is efiectuated by providing the plates with bevelled faces 37 and 38 respectively defining a dihedral angle :that converges in the direction of efiiuX of the ions. Thus the contour of the arc plasma, represented by the heavy line 39, is in part behind the arc slit plates 32 and 33 -and the portions 41 and 42 of the plasma that principal- 1y tend to release ions away from the central portion 44 of the ion stream are well masked from the electric field established by the arc slit plates 32 and 33 and the accelerating electrodes 34 and 36. In this fashion most of the ions leaving the vicinity of the are 31 pass through the arc slit between the adjacent edges of the plates 32 .and 33 without impinging thereon. As a result, the edges of the plates 32 and 33 which form the arc slit are not excessively eroded and are maintained in satisfactory op erating condition for a substantial time.
In both modifications of the invention disclosed herein there is aiforded a mechanism eifective to improve in general the operation vof an ion producing mechanism and calutrons in general.
What is claimed is:
1. In an ion source for a calutron, the combination comprising an arc block defining an arc chamber having an exit opening formed by bevelled edges of the arc block that converge in the outward direction from said are chamber, means for creating an electron stream in the arc chamber, means for supplying an ionizable charge to the arc chamber, and an ion accelerating electrode disposed near the arc block opposite the exit opening.
2. The combination of claim 1 wherein the arc slit opening is defined by marginal edges bevelled to define a dihedral angle.
References Cited in the file of this patent
US270201A 1946-05-08 1952-02-06 Calutron Expired - Lifetime US2922044A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
US270201A US2922044A (en) 1946-05-08 1952-02-06 Calutron

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US668112A US2874296A (en) 1946-05-08 1946-05-08 Calutron ion source
US270201A US2922044A (en) 1946-05-08 1952-02-06 Calutron

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2745017A (en) * 1945-11-28 1956-05-08 Frank F Oppenheimer Ion producing mechanism
US2850636A (en) * 1945-08-29 1958-09-02 John G Backus Ion producing mechanism

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2850636A (en) * 1945-08-29 1958-09-02 John G Backus Ion producing mechanism
US2745017A (en) * 1945-11-28 1956-05-08 Frank F Oppenheimer Ion producing mechanism

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