US281044A - Process of analyzing pig-iron - Google Patents

Process of analyzing pig-iron Download PDF

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US281044A
US281044A US281044DA US281044A US 281044 A US281044 A US 281044A US 281044D A US281044D A US 281044DA US 281044 A US281044 A US 281044A
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iron
analyzing
furnace
blast
metal
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/20Metals
    • G01N33/204Structure thereof, e.g. crystal structure

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  • My object is to make an immediate test practicable without delaying the transfer of the metal from the blast-furnace.
  • the invention consists, briefly, in taking a small quantity of the molten iron, and by pouring it into water granulating it, in which condition it is quite brittle, and then crushing and analyzing the granules. More fully, my invention is as follows: Usually the metal is transferred in a ladle set on trucks, and as the converting-works are generally some distance from the blast-furnace, it generally takes from twenty minutes to a half hour from the first tapping of the blast-furnace till the ladle is brought to the converter. As soon as the metal begins to run from the furnace, I catch or dip up a small quantity of it and let it drop sev eral feet into Water, preferably clean Water in a clean vessel.
  • the metal divides into small globules or pellets, which chill at once. These can be taken at once to the laboratory, and, being extremely brittle, they'can be very readily crushed in a steel mortar, and thus reduced to the condition required for analysis.
  • the analysis which is at this stage desired, requires but a few minutes to determine, the result is that I can have the report on the contents of the ladle ready by thetime the latter has arrived at the converting-works. There is therefore no delay caused in the proper carrying out of the direct process, and at the same time, the precise character of the metal being analytically determined, the reagents of conversion may be accurately regulated and the standard product maintained-a result which is unattainable in the present practice of making samples and boring them after slow cooling.
  • I claim as my invention The method of analyzing the runs of a blastfurnace, consisting in first granulating some of the molten metal by pouring into water and then crushing and analyzing the said granules, substantially as described.

Description

UNITED STAT-Es PATEIYLOEFICE- SAMUELA. FORD, or-rrrrsnune, PENNSYLVANIA.
PRocEssoF ANALYZINGPIGV- IRON .FROM "BLAST-FURNACES.
SPECIFICATION forming part of Letters Patent No. 281,044, dated July 10, 1883.
7 Application filed Januaryl'l, 188 3. (No specimens.)
new and useful Improvements in Processes 0fv Analyzing Pig-Iron from Blast-Furnaces; and I do hereby declare thatthe following is a full,
' clear,and exact description of the invention,
analysis cannot be had for several hours.
which will enable others skilled in the art to which it appertains to make and use the same.
In the manufacture of steel, whether Bessemer or openhearth, by the direct process, wherein the molten metal is taken directly from the blast-furnace to the converter or furnace, it is practically out of the question to obtain a running analysis of the charge in time to be of service. If the usual f sample be cast and allowed to cool in the ordinary way, the If the sample-piece he suddenly cooled in water, it chills, and cannot bereadily broken up or drilled for the test. Meanwhile the ladle of molten metal drawn from theblast-furnace cannot be held for' such a length of time; hence the character of the contents of the ladle must be to a certain extent guessed at, es-
pecially with reference to the contained sili-.
con.
My object is to make an immediate test practicable without delaying the transfer of the metal from the blast-furnace.
The invention consists, briefly, in taking a small quantity of the molten iron, and by pouring it into water granulating it, in which condition it is quite brittle, and then crushing and analyzing the granules. More fully, my invention is as follows: Usually the metal is transferred in a ladle set on trucks, and as the converting-works are generally some distance from the blast-furnace, it generally takes from twenty minutes to a half hour from the first tapping of the blast-furnace till the ladle is brought to the converter. As soon as the metal begins to run from the furnace, I catch or dip up a small quantity of it and let it drop sev eral feet into Water, preferably clean Water in a clean vessel. As soon as it strikes the water, the metal divides into small globules or pellets, which chill at once. These can be taken at once to the laboratory, and, being extremely brittle, they'can be very readily crushed in a steel mortar, and thus reduced to the condition required for analysis. As the analysis, which is at this stage desired, requires but a few minutes to determine, the result is that I can have the report on the contents of the ladle ready by thetime the latter has arrived at the converting-works. There is therefore no delay caused in the proper carrying out of the direct process, and at the same time, the precise character of the metal being analytically determined, the reagents of conversion may be accurately regulated and the standard product maintained-a result which is unattainable in the present practice of making samples and boring them after slow cooling.
I claim as my invention The method of analyzing the runs of a blastfurnace, consisting in first granulating some of the molten metal by pouring into water and then crushing and analyzing the said granules, substantially as described.
In testimony that I claim the foregoing as my own I have hereto affixed my signature in presence of two Witnesses.
SAMUEL A. FORD.
\Vitnesses XVM. I. Mann, '1. J. McTiei-in.
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