US273679A - Leeoy s - Google Patents

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US273679A
US273679A US273679DA US273679A US 273679 A US273679 A US 273679A US 273679D A US273679D A US 273679DA US 273679 A US273679 A US 273679A
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chamber
tube
gas
gasoline
inner case
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/06—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of inorganic compounds containing electro-positively bound hydrogen, e.g. water, acids, bases, ammonia, with inorganic reducing agents
    • C01B3/10—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of inorganic compounds containing electro-positively bound hydrogen, e.g. water, acids, bases, ammonia, with inorganic reducing agents by reaction of water vapour with metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
    • B01J8/0085—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction promoting uninterrupted fluid flow, e.g. by filtering out particles in front of the catalyst layer
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/36—Hydrogen production from non-carbon containing sources, e.g. by water electrolysis

Definitions

  • Figure 1 is a vertical sectional view of my improved apparatus.
  • Fig. 2 is a plan view of the inner case, its cones, tubes, and pipes.
  • Fig. 3 is a cross-sectional view of the inner case; and
  • Figs. 4 and 5 are detail views.
  • This invention has relation to apparatus for making gas; and it consists in the construction and novel arrangement of devices, as hereinafter set forth, and particularly pointed out in the appended claims.
  • the object of the invention is to provide a simple self-regulating apparatus for making gas, whiclrwill be easily managed, inoffensive, and perfectly safe.
  • the letter A desig- 3o nates the outside case, barrel, or tank, having a suitable lining and a hinged lined cover or lid, which is designed to hold the acidulated water, and is provided with a waste-cock at a.
  • B designates an inner chamber, which con- 5 tains the generating-chamber, the gas-chamber, and the gasoline-chamber, and which is provided with suitable pipes, valves, and a feed-tube, as will be hereinafter explained.
  • This inner case, B is made bottomless, in or- 0 der that the basket E, which holds the iron or zinc filings or chips, may be readily inserted and detachably connected therewith.
  • D D represent sills or supports, which rest on the bottom of the outer case, A, and serve 5 to hold the inner case above said bottom.
  • a receiver or basket, E On these sills or supports, within the inner case and at the lower portion thereof, is located a receiver or basket, E, in which iron filings are placed; or clippings of zinc may be used in the basket.
  • the basketE consists of a perforated rim or short casing, k, having an internal bead or ledge about midway of its height, upon which rests a perforated diaphragm, h, which divides the basket into two compartments,l and m, the upper one being for the filings or chips.
  • the lower edge of the inner case, B is wired and provided with sheaths on its outer side for the reception of the shanks of the removable spring-catchess,forholdingthebasket E in place.
  • the upper end of the inner case is closed by the top I), and the gas-chamber F within said case is connected to the gasolinechamber by means of a bent tube, G, which extends from the top of the case B through the top of the compartment 0 and nearly to the bottom of the latter.
  • This tube is provided with a check-valve at c.
  • the gas-chamber F is also provided with an outlet-pipe, H, extending upward and provided with a checkvalve, d. 7
  • the filling-tube Kand the outlet-tube L Extending through the top of the gasolinecompartment are the filling-tube Kand the outlet-tube L, the latter extending to the burner, and being provided with a check-valve, e.
  • the filling-tube is provided with a valve at g. 7
  • Catches or fastenings Z are connected to the inner wall of the outer case,'A, and are designed to be attached to the inner case, B, or to engage the same when placed in the outer case, so as to hold itin position.
  • the various 8o tubes which extend through the top b of the inner case, B, are strengthened by means of conical braces P, of metal.
  • a chamber, 1 Within this conical brace-wall, around the tube G, is formed a chamber, 1;, which communicates with the tube G through a number of perforations made therein, and through perforations made in the base of said chamber 1) with the gas-chamber F of theinner case.
  • the chamber 1 within the cone-brace of the outlet- 0 tube L of the gasoline-chamber is made to communicate with the gasoline-chamber and with the interior of the tube.
  • These perforations provide many passages for the gas, and are designed to prevent obstructions from clogging 5 the main conducting-tubes G and L.
  • a quantity of zinc or iron clippings is first to be placed in the upper chamber of the basket E.
  • the basket is then placed within the lower portion of the inroo ner case, B, and fastened thereto by means of the catches s.
  • the vent or outlet tube L of the gasoline-compartment is then opened and the chamberG filled with gasoline of about 87, test, a little pure water having first been poured into the chamber.
  • the check-valves 0, 01,0, and g are closed, and theinverted case B, with the attached basket of clippings, is placed within the outer tank, A,in sucha manner that it shall rest on the sills or cleat-supports D.
  • the inner case having been fastened to the tank by means of the catches Z the tank-outlet a is closed, and water acidulated by the addition of sulphuric acid. at the rate of one pound of the acid to each gallon of water is poured into the tank until the top bof the inner case is covered.
  • the vent-cock H is now opened, and as the air escapes from the chamber F the acidulated water rises in said chamber from below, and, reaching the chamberl of the basket E, acts upon the zinc or iron therein, generating hydrogen gas.
  • the vent-cock H is now closed and the hydrogen gas fills the chamber F.
  • the hydrogen gas passes over and is conducted by the tube G to the lower portion of the gasoline-chamber, whence it rises through the water and gasoline and becomes carbureted and forms a rich illuminating-gas.
  • the valve e of the perforated outlet pipe L is opened, allowing the gas to pass to the burner.
  • the apparatus is self-regulating.
  • the valve 0 ot'the outlet-pipe L is closed, the hydrogen-gas chamber F, becoming filled with the gas, displaces the acidulated water, forcing it downward in the inner case, B, until it is below the iron or zinc clippingsin the basket E. In this manner action upon the zinc or iron is prevented and the apparatus ceases to make gas.
  • the water in the tank can be discharged and. the tank replenished without removing the inner case. So, also, the gasoline-chamber can be refilled through its feed-tube K'without disturbing any other portion of the apparatus,
  • the apparatus is safe, as the inner case is surrounded by acidulated water of the character hereinbefore described, which is a powerful extinguisher of fire.
  • the gas generating and carbnreting apparatus consisting ot'the tank A for acidulated water, the inner case, 13, within said tank, having in its upper portion the gasoline compartment U, and in its lower portion the raised basket E for iron or zinc, the valved bent tube Gr, extending from the interior of the case to near the bottom of the gasoline-chamber, the valved feed-tube K, and the valved outlet-tube L, and tube H, substantially as specified.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Filling Or Discharging Of Gas Storage Vessels (AREA)

Description

(No Model.)
L. S. GROVES.
APPARATUS FOR GENERATING AND GAEBUEETING HYDROGEN GAS.
Patented Ma.1*.6,1883.
A Fig.1.
WITNESSES v ATTORNEYS N. PETERS. Phnloiithugmpher. Washmglnn. D. c
a TATES ATENT FFICE.
LEROY S. GROVES, OF AFTON, IOWA, ASSIGNOR OF ONE-HALF TO JOHN W. i SHUTE, OF SAME PLACE.
APPARATUS FOR GENERATING A ND CARBURETING HYDROGEN GAS.
SPECIFICATION forming part of Letters Patent No. 273,679, dated March 6, 1883.
Application filed November 23, 1882. (No model.)
T all whom it may concern:
Be it known that I, LEROY S. GROVES, a citizen of the United States, residing at Afton, in the county of Union and State oflowa, have invented certain new and useful Iin provements in Apparatus for Generating and Oarbureting Hydrogen Gas; and I do declare the following to be a full, clear, and exact description of the invention, such as will enable others skilled m in the art to which it appertains to make and use the same, reference being had to the accom panying drawings, and to letters or figures of reference marked thereon, which form a part of this specification.
1 Figure 1 is a vertical sectional view of my improved apparatus. Fig. 2 is a plan view of the inner case, its cones, tubes, and pipes. Fig. 3 is a cross-sectional view of the inner case; and Figs. 4 and 5 are detail views.
This invention has relation to apparatus for making gas; and it consists in the construction and novel arrangement of devices, as hereinafter set forth, and particularly pointed out in the appended claims.
The object of the invention is to provide a simple self-regulating apparatus for making gas, whiclrwill be easily managed, inoffensive, and perfectly safe.
In the annexed drawings, the letter A desig- 3o nates the outside case, barrel, or tank, having a suitable lining and a hinged lined cover or lid, which is designed to hold the acidulated water, and is provided with a waste-cock at a.
B designates an inner chamber, which con- 5 tains the generating-chamber, the gas-chamber, and the gasoline-chamber, and which is provided with suitable pipes, valves, and a feed-tube, as will be hereinafter explained. This inner case, B,is made bottomless, in or- 0 der that the basket E, which holds the iron or zinc filings or chips, may be readily inserted and detachably connected therewith.
D D represent sills or supports, which rest on the bottom of the outer case, A, and serve 5 to hold the inner case above said bottom. On these sills or supports, within the inner case and at the lower portion thereof, is located a receiver or basket, E, in which iron filings are placed; or clippings of zinc may be used in the basket. The basketE consists of a perforated rim or short casing, k, having an internal bead or ledge about midway of its height, upon which rests a perforated diaphragm, h, which divides the basket into two compartments,l and m, the upper one being for the filings or chips. The lower edge of the inner case, B, is wired and provided with sheaths on its outer side for the reception of the shanks of the removable spring-catchess,forholdingthebasket E in place. The upper end of the inner case is closed by the top I), and the gas-chamber F within said case is connected to the gasolinechamber by means of a bent tube, G, which extends from the top of the case B through the top of the compartment 0 and nearly to the bottom of the latter. This tube is provided with a check-valve at c. The gas-chamber F is also provided with an outlet-pipe, H, extending upward and provided with a checkvalve, d. 7
Extending through the top of the gasolinecompartment are the filling-tube Kand the outlet-tube L, the latter extending to the burner, and being provided with a check-valve, e. The filling-tube is provided with a valve at g. 7
Catches or fastenings Z are connected to the inner wall of the outer case,'A, and are designed to be attached to the inner case, B, or to engage the same when placed in the outer case, so as to hold itin position. The various 8o tubes which extend through the top b of the inner case, B, are strengthened by means of conical braces P, of metal. Within this conical brace-wall, around the tube G, is formed a chamber, 1;, which communicates with the tube G through a number of perforations made therein, and through perforations made in the base of said chamber 1) with the gas-chamber F of theinner case. In a similar manner the chamber 1; within the cone-brace of the outlet- 0 tube L of the gasoline-chamber is made to communicate with the gasoline-chamber and with the interior of the tube. These perforations provide many passages for the gas, and are designed to prevent obstructions from clogging 5 the main conducting-tubes G and L.
In using the apparatus a quantity of zinc or iron clippings is first to be placed in the upper chamber of the basket E. The basket is then placed within the lower portion of the inroo ner case, B, and fastened thereto by means of the catches s. The vent or outlet tube L of the gasoline-compartment is then opened and the chamberG filled with gasoline of about 87, test, a little pure water having first been poured into the chamber. Then the check-valves 0, 01,0, and g are closed, and theinverted case B, with the attached basket of clippings, is placed within the outer tank, A,in sucha manner that it shall rest on the sills or cleat-supports D. The inner case having been fastened to the tank by means of the catches Z the tank-outlet a is closed, and water acidulated by the addition of sulphuric acid. at the rate of one pound of the acid to each gallon of water is poured into the tank until the top bof the inner case is covered. The vent-cock H is now opened, and as the air escapes from the chamber F the acidulated water rises in said chamber from below, and, reaching the chamberl of the basket E, acts upon the zinc or iron therein, generating hydrogen gas. The vent-cock H is now closed and the hydrogen gas fills the chamber F. Upon opening the valve 0 of the tube G the hydrogen gas passes over and is conducted by the tube G to the lower portion of the gasoline-chamber, whence it rises through the water and gasoline and becomes carbureted and forms a rich illuminating-gas. When desired for usethe valve e of the perforated outlet pipe L is opened, allowing the gas to pass to the burner.
' The apparatus is self-regulating. When the valve 0 ot'the outlet-pipe L is closed, the hydrogen-gas chamber F, becoming filled with the gas, displaces the acidulated water, forcing it downward in the inner case, B, until it is below the iron or zinc clippingsin the basket E. In this manner action upon the zinc or iron is prevented and the apparatus ceases to make gas.
If care is used in managing this apparatus, the offensive odor of the gasoline will not be perceptible as the gasoline-compartment is, with the exception of the outlet-tube, perfectly inclosed. There is no waste of material. The
water in the tank can be discharged and. the tank replenished without removing the inner case. So, also, the gasoline-chamber can be refilled through its feed-tube K'without disturbing any other portion of the apparatus,
the valve of the bent tube Gr being closed, however, while filling, to prevent the movement of the hydrogen gas into the gasoline-chamber at this time. 7
The apparatus is safe, as the inner case is surrounded by acidulated water of the character hereinbefore described, which is a powerful extinguisher of fire.
Having described this invention, What 1 claim, and desire to secure by Letters Patent,
1. The gas generating and carbnreting apparatus, consisting ot'the tank A for acidulated water, the inner case, 13, within said tank, having in its upper portion the gasoline compartment U, and in its lower portion the raised basket E for iron or zinc, the valved bent tube Gr, extending from the interior of the case to near the bottom of the gasoline-chamber, the valved feed-tube K, and the valved outlet-tube L, and tube H, substantially as specified.
2. The combination, with the tank A, of the inner case, B, its gasoline-compartment C, bent conducting-tube G and valve 0, valved feeding-tube K and valved outlets L and H, the sill-supports D, raised basket E, and the fastenings or catches s, substantially as specified.
3. The combination, with the gas-chamber F and the gasoline-chamber G, of the perforated gas-conducting tubes G and L, and their cone supports or braces P, forming chambers v and '0 around said tubes, the cones having perforated bottoms, substantially as specified.
In testimony whereof I at'fix my signature in presence of two witnesses.
LEROY S. GROVES. Witnesses J. E. OHENY, A. W. ENOCH.
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