US261175A - Gael eumpff - Google Patents
Gael eumpff Download PDFInfo
- Publication number
- US261175A US261175A US261175DA US261175A US 261175 A US261175 A US 261175A US 261175D A US261175D A US 261175DA US 261175 A US261175 A US 261175A
- Authority
- US
- United States
- Prior art keywords
- pounds
- eumpff
- gael
- stuff
- dye
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000975 dye Substances 0.000 description 14
- RUFPHBVGCFYCNW-UHFFFAOYSA-N 1-Naphthylamine Chemical compound C1=CC=C2C(N)=CC=CC2=C1 RUFPHBVGCFYCNW-UHFFFAOYSA-N 0.000 description 8
- 239000002253 acid Substances 0.000 description 8
- 239000000243 solution Substances 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- BVKZGUZCCUSVTD-UHFFFAOYSA-N Carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 6
- JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 description 6
- VWDWKYIASSYTQR-UHFFFAOYSA-N Sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 210000002268 Wool Anatomy 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 description 2
- 235000011167 hydrochloric acid Nutrition 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- UFWIBTONFRDIAS-UHFFFAOYSA-N naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 239000000344 soap Substances 0.000 description 2
- 235000010344 sodium nitrate Nutrition 0.000 description 2
- 239000004317 sodium nitrate Substances 0.000 description 2
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/24—Monoazo dyes prepared by diazotising and coupling from coupling components containing both hydroxyl and amino directing groups
- C09B29/28—Amino naphthols
- C09B29/30—Amino naphtholsulfonic acid
Definitions
- CARL RUMPFF OF APRATH, NEAR ELBERFELD, PRUSSIA, GERMANY.
- This invention relates to a brown dye-stuff or coloring-matter which is produced by the action of diazo-naphtalene sulphonate of soda upon naphthylamine in an acid solution.
- M y dye-stutf when dry, appears as a brown powder. It is solnblein hot water, and crystallizes when the solution gets cold. The aqueous solution becomes yellowish brown by addition ofalkalies. It becomes, however, bluish red by the addition of concentrated mineral acids,and the dye-stuff separates partially.
- the new dye-stuff dyes silk and wool in an acidulated bath, and is fast against soap and light.
- the new brown dye-stuff or coloring-matter which is produced by the action of diazo naphtalene sulphonate of soda upon naphthylamine in an acid solution.
Description
UNITED STATES PATENT ()FFICE.
CARL RUMPFF, OF APRATH, NEAR ELBERFELD, PRUSSIA, GERMANY.
MANUFACTURE OF COLORING-MATTER FROM NAPHTHYLAMINE.
SPECIFICATION forming part of Letters Patent No. 261,175, dated July 18, 1882. Application filed April 21, 1882. (Spetimens) To all whom it may concern.-
Be it known that I, CARL RUMPFF, residing at Aprath, near Elberfeld, in the Kingdom of Prussia and EmpireofGerniany, have invented a new and usefullmprovement in Manufacturing a new Brown Dye-Stuff, of which the following is a specification.
This invention relates to a brown dye-stuff or coloring-matter which is produced by the action of diazo-naphtalene sulphonate of soda upon naphthylamine in an acid solution.
In carrying out my invention I take fifty pounds of naphthylamine sulphonate of soda dissolvedin five hundred pounds of water, and cooled down with ice to 3 centigrade. To this solutionI add slowly seventy-five pounds of [111.1-
riat-ic acid, and thereafter eleven pounds sodium nitrate dissolved in forty pounds of water. After several hours rest the liquid is poured into a solution containing twenty-five pounds of naphthylamine, fifty pounds of muriatic acid, and five hundred pounds of water. The new brown dye-stuff separates instantly as a voluminous precipitate, which is filtered and dried.
M y dye-stutf, when dry, appears as a brown powder. It is solnblein hot water, and crystallizes when the solution gets cold. The aqueous solution becomes yellowish brown by addition ofalkalies. It becomes, however, bluish red by the addition of concentrated mineral acids,and the dye-stuff separates partially. The new dye-stuff dyes silk and wool in an acidulated bath, and is fast against soap and light.
What.- I claim as new, and desire to secure by Letters Patent, is-
The new brown dye-stuff or coloring-matter which is produced by the action of diazo naphtalene sulphonate of soda upon naphthylamine in an acid solution.
CARL BUMP]? F.
\Vitnesses:
J. FERD. KEDENBURG, A. SGHEELE.
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US261175A true US261175A (en) | 1882-07-18 |
Family
ID=2330452
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US261175D Expired - Lifetime US261175A (en) | Gael eumpff |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US261175A (en) |
-
0
- US US261175D patent/US261175A/en not_active Expired - Lifetime
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