US2596875A - Method of handling waste sulfite liquor - Google Patents

Method of handling waste sulfite liquor Download PDF

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US2596875A
US2596875A US164356A US16435650A US2596875A US 2596875 A US2596875 A US 2596875A US 164356 A US164356 A US 164356A US 16435650 A US16435650 A US 16435650A US 2596875 A US2596875 A US 2596875A
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Thomas W Stewart
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Weyerhaeuser Timber Co
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    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C11/00—Regeneration of pulp liquors or effluent waste waters
    • D21C11/10—Concentrating spent liquor by evaporation

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  • This invention relates to improvements in the method of handling and burning waste sulphite liquor and particularly to the storage of the liquor prior to burning thereof to recover magnesium oxide and sulphur dioxide from the liquor.
  • Preheating is necessary in the usual methods of preparation of waste liquor for burning because of the lowering of the temperature of the waste liquor due to flashing.
  • Such iiashing occurs in the normal operation of a multiple effect evaporator when the most concentrated waste liquor is Withdrawn from the last eiiect and is transferred to a container which is at a lower pressure.
  • the sudden lowering of the pressure over the hot liquor which has been heated at superatmospheric pressure to a temperature above its boiling point at atmospheric pressure, causes the liquor to immediately vaporize or flash.
  • the pressure lin the last effect of a multiple effect evaporator is in the range of 15u-30 pounds gauge, so that the temperature of the liquor in the last effect is at the boiling point corresponding to that pressure.
  • This invention is directed to a method of burning concentrated waste liquor in which the liquor is concentrated by multiple effect evaporation at successively increasing pressures. It is then delivered from the last effect at the over-atmospheric pressure of the last effect to a storage container in which over-atmospheric pressure substantially equal to that in the last effect is maintained to conserve the heat of the concentrated liquor and to permit the delivery of the stored liquor to a burning zone at substantially the temperature maintained in the storage container. Conservation of heat in the liquor in the storage container will also depend upon the prevention of heat losses through radiation and conduction.
  • the preferred embodiments of the invention serve to compensate for losses of heat through radiation and conduction by raising the temperature of the liquor in the storage container whenever it falls below the temperature of the liquor in the last elect.
  • the invention depends upon the maintenance of the concentrated waste liquor at a substantial pressure during storage so that its temperature will not fall below that suitable for efficient ring.
  • the pressure on the liquor is held at 15 pounds per square inch gauge, or higher, the temperature ⁇ prevailing in the last effect of the evaporator, for example 250 F'., will .be maintained in the liquor in storage, and the liquor may be withdrawn as required and fired directly without further heating.
  • the liquor from the last effect of the evaporator is delivered to a storage tank of such construction that the liquor can be maintained at the pressure prevailing in the last effeet, for example 15 pounds per square inch gauge.
  • the liquor is then withdrawn as required from the storage tank and delivered to the ⁇ burners.
  • a tank 5 is provided for the unconcentrated waste liquor which is recovered from the digester and washers (not shown)
  • the unconcentrated liquor is Awithdrawn by a pump 6 and delivered through a pipe 'I to a cascade evaporator 8 in which partial concentration is effected.
  • the details of the cascade evaporator are Well known and require, therefore, no further description.
  • the liquor flows through a pipe 9 to a neutralizing tank I9 where acid constituents are neutralized by the addition of magnesium oxide to the liquor.
  • the liquor is Withdrawn through a pump II and delivered by a pipe I2 to the multiple eifect evaporator.
  • the multiple effect evaporator comprises a plurality of effects, in the present case six, I3, I4, I5, I6, l1 and I8. It is understood that the number of effects may be varied, depending upon the particular liquor to be evaporated.
  • Each effect comprises a vapor body I9, a heater 20, a circulating pump 2
  • the details of each of the effects are identical. rlJhey differ merely in the pressures maintained therein.
  • effects I3 and I4 may be operated at a pressure of fifteen pounds per square inch, gauge, effect I5 at a pressure of three to ive pounds per square inch, gauge, effect I6 at a six-inch vacuum, effect Il at an eighteen-inch vacuum, and effect I8 at a twenty-six to twenty-eight inch vacuum.
  • Other pressures may be employed.
  • effects I3 and I4 may be operated at pressures ranging from ten to twenty-five pounds per square inch, gauge more or less, with consequent variation in the pressures maintained in the remaining effects of the evaporator.
  • the vapor from effect I8 is Withdrawn through a pipe 32 and discharged through a jet condenser 33. It Will be understood that in each ofthe effects the liquor is constantly circulated between the vapor body I9 and the heater 20 and that as the result of the heating the vapor is delivered from each vapor body in the manner indicated.
  • the liquor, partially concentrated in the cascade evaporator 8 is delivered to effect I6.
  • the liquor After being heated therein and partially evaporated, the liquor is delivered through a pipe 34 to the effect II operating at a lower pressure.
  • the further concentrated liquor is delivered through a pipe 35 to the effect I8 for further concentration.
  • the liquor is Withdrawn through a pipe 36 and delivered by a pump 3l through a pipe 38 to effect I5, Where it is heated by vapor from the effects I3 and I4.
  • the liquor is Withdrawn through ⁇ a pipe 39 and is transferred by a pump 40 through a pipe 4I to effect I4, where it is heated with steam.
  • the liquor From the effect I4 the liquor is Withdrawn through a pipe 43 and delivered by a pump 44 through a pipe 45 to effect I3, Where it is further concentrated by heating With steam.
  • the liquor is withdrawn through a pipe 46 and delivered by a pump 41 and pipe 48 to the storage container 49.
  • the latter is connected by a vent pipe 59 to the vapor body I9 of the effect I3 so that the pressure in the storage container 49 is identical with that in the vapor body I9 of effect I3.
  • the temperature of the liquor delivered to the storage container 49 should be in the neighborhood of 259 F., assuming that a pressure of fifteen pounds per square inch gauge is maintained in the vapor body I9 of effect I3. Because of the pressure maintained in the storage container 49, the liquid -Will remain ⁇ at substantially the same temperature which will be higher or lower, depending upon the pressure maintained in the vapor body I9 of effect I3.
  • the liquor at the high temperature maintained as a result of pressure in the storage container 49 isv in ⁇ thebest possible condition for ringwithout the necessity of employing steam for reheating the liquor before it is fired.V It is withdrawn frompthe storage container 45 through a pipe 5I and is delivered by a pump 52 through a pipe 53 vto the burner 54 of a furnace 55 having boiler tubes 53 wherein the heat developed by the Aburner 54 is utilized in producing steam for use in the plant.
  • the method as described avoids the difficulties which have beenmet heretofore in handling concentrated liquor When the latter has beenpermitted to become partially cooled before it isdelivered to the furnace for combustion.
  • 1.V The method of burning concentrated Waste liquor from the Vdigestion of Vligno-cellulose material which comprises concentrating the liquor by multiple effect evaporation With at least the last eect maintained at over-atmospheric pressure, delivering the liquor at the .over-atmospheric pressure therein to a storage containen'maintaining' the pressure in the storage container substantially at that of the last effect, thereby conserving thev heat in the concentrated liquor, and delivering'the heated liquor at substantially the temperature maintained in the storage container to the burning Zone.
  • the method of burning concentrated Waste liquor from the digestion of ligno-cellulose material which comprises concentrating the liquor rst by cascade evaporation and then by multiple effect evaporation with at least the last eifect maintained Vat over-atmospheric pressure, delivering the liquor at the over-atmospheric pressure therein to ⁇ a storage container, maintaining the pressure in the storage .container substantially at that of the last effect,
  • the last eiect operating at a pressure in the range of 10-25 pounds per square inch, delivering the liquor from the last effect to a storage container, maintaining substantially the same pressure in both the last effect and the storage container, thereby conserving the heat in the concentrated liquor, and delivering the heated liquor at substantially the temperature maintained in the storage container to the burning zone.
  • the method of burning concentrated Waste liquor from the digestion of ligno-cellulose material which comprises circulating the liquor rst by cascade evaporation and then by multiple eiect evaporation, the last effect operating at a pressure in the range of 10-25 pounds per square inch, delivering the liquor from the last effect to a storage container, maintaining substantially the same pressure in both the last eiect and the storage container, thereby conserving the heat in the concentrated liquor, and delivering the heated liquor at substantially the temperature maintained in the storage container to the burning zone.

Description

May 13, 1952 T. w. STEWART METHOD OF' HANDLING WASTE SULPHITE LIQUOR Filed May 26, 1950 lNvENToR Hamas ffzaar TTORNEYS Patented May 13, 1952 METHOD OF HANDLING WfASTE SULFITE LIQUOR Thomas W. Stewart, Longview, Wash., assignor to Weyerhaeuser Timber Company, Longview,
Wash., a corporation of Washington Application May 26, 1950,'Serial No. 164,356 4 Claims. (Cl. 159--47) This invention relates to improvements in the method of handling and burning waste sulphite liquor and particularly to the storage of the liquor prior to burning thereof to recover magnesium oxide and sulphur dioxide from the liquor.
The application of the invention will be understood by reference to the patent to Palmrose et al. No. '2,320,294 issued May 25, 1943. This patent describes the digestion of ligneous material in magnesium bisulphite cooking liquor and the subsequent concentration and burning of the waste liquor to recover its principal constituents for further use in the system. In the patented method, the concentrated waste liquor leaving the last effect of a multiple effect evaporator is' delivered through a pipe to the combustion furnace. In practical operation of such a method, it is necessary to have storage tanks for the concentrated liquor between the evaporator and the furnace. If the liquor is maintained at normal atmospheric pressure in such storage tanks, it loses its temperature rapidly and is no longer in the best condition for rapid firing. It is necessary, therefore, to install preheaters to bring the liquor back to ring temperature. This is both difficult and expensive because of the necessity for employing steam as a heating medium and particularly because the concentrated liquor has a strong scaling tendency and the heating surfaces are rapidly fouled and become inefficient.
Preheating is necessary in the usual methods of preparation of waste liquor for burning because of the lowering of the temperature of the waste liquor due to flashing. Such iiashing occurs in the normal operation of a multiple effect evaporator when the most concentrated waste liquor is Withdrawn from the last eiiect and is transferred to a container which is at a lower pressure. The sudden lowering of the pressure over the hot liquor, which has been heated at superatmospheric pressure to a temperature above its boiling point at atmospheric pressure, causes the liquor to immediately vaporize or flash. Normally, the pressure lin the last effect of a multiple effect evaporator is in the range of 15u-30 pounds gauge, so that the temperature of the liquor in the last effect is at the boiling point corresponding to that pressure. When, as in normal practice, the pressure of this liquor is relieved to atmospheric pressure, steam is flashed off until the temperature of the liquor is lowered to the boiling point of the liquor at atmospheric pressure. The present invention avoids loss of heat through ashing to atmospheric pressure and conserves heat in the liquor so that it may be burned Without reheating. l
This invention is directed to a method of burning concentrated waste liquor in which the liquor is concentrated by multiple effect evaporation at successively increasing pressures. It is then delivered from the last effect at the over-atmospheric pressure of the last effect to a storage container in which over-atmospheric pressure substantially equal to that in the last effect is maintained to conserve the heat of the concentrated liquor and to permit the delivery of the stored liquor to a burning zone at substantially the temperature maintained in the storage container. Conservation of heat in the liquor in the storage container will also depend upon the prevention of heat losses through radiation and conduction. Although this invention is not directed to the solution of these problems, which can be taken care of by well-known methods of insulation, the preferred embodiments of the invention serve to compensate for losses of heat through radiation and conduction by raising the temperature of the liquor in the storage container whenever it falls below the temperature of the liquor in the last elect.
Other objects and advantages of the invention will be apparent as it is better understood by reference to the following specification and the accompanying drawing, which illustrates diagrammatically the equipment required for concentrating, storing and burning the liquor.
The invention depends upon the maintenance of the concentrated waste liquor at a substantial pressure during storage so that its temperature will not fall below that suitable for efficient ring. Thus, if the pressure on the liquor is held at 15 pounds per square inch gauge, or higher, the temperature `prevailing in the last effect of the evaporator, for example 250 F'., will .be maintained in the liquor in storage, and the liquor may be withdrawn as required and fired directly without further heating. In carrying out the invention, therefore, the liquor from the last effect of the evaporator is delivered to a storage tank of such construction that the liquor can be maintained at the pressure prevailing in the last effeet, for example 15 pounds per square inch gauge. The liquor is then withdrawn as required from the storage tank and delivered to the` burners.
Referring to the drawing, a tank 5 is provided for the unconcentrated waste liquor which is recovered from the digester and washers (not shown) The unconcentrated liquor is Awithdrawn by a pump 6 and delivered through a pipe 'I to a cascade evaporator 8 in which partial concentration is effected. The details of the cascade evaporator are Well known and require, therefore, no further description. From the cascade evaporator, the liquor flows through a pipe 9 to a neutralizing tank I9 where acid constituents are neutralized by the addition of magnesium oxide to the liquor. From the neutralizing tank, the liquor is Withdrawn through a pump II and delivered by a pipe I2 to the multiple eifect evaporator.
The multiple effect evaporator comprises a plurality of effects, in the present case six, I3, I4, I5, I6, l1 and I8. It is understood that the number of effects may be varied, depending upon the particular liquor to be evaporated. Each effect comprises a vapor body I9, a heater 20, a circulating pump 2| and pipes 22, 23 and 24 to permit circulation of the liquor. The details of each of the effects are identical. rlJhey differ merely in the pressures maintained therein. For example, effects I3 and I4 may be operated at a pressure of fifteen pounds per square inch, gauge, effect I5 at a pressure of three to ive pounds per square inch, gauge, effect I6 at a six-inch vacuum, effect Il at an eighteen-inch vacuum, and effect I8 at a twenty-six to twenty-eight inch vacuum. Other pressures may be employed. Thus, effects I3 and I4 may be operated at pressures ranging from ten to twenty-five pounds per square inch, gauge more or less, with consequent variation in the pressures maintained in the remaining effects of the evaporator.
To effect evaporation, steam is supplied from a steam line 25 through branches 26 and 2l' to the heaters 29 of effects I3 and I4. The vapor from the effects I3 and I4 is withdrawn through a vapor line 23 connected to each of the vapor bodies I9. The vapor from effects I3 and I4 is thus conveyed to the heater 29 of effect I5. The vapor from the effect I5 is withdrawn' from the vapor body I9 of that effect through a pipe 29 and delivered to the heater 20 of effect I6. The vapor from effect IS is Withdrawn through pipe 39 and delivered tothe heater 2li of eifect I1. The vapor from effect I'I is withdrawn through a pipe 3I and delivered to the heater 20 of effect I8. The vapor from effect I8 is Withdrawn through a pipe 32 and discharged through a jet condenser 33. It Will be understood that in each ofthe effects the liquor is constantly circulated between the vapor body I9 and the heater 20 and that as the result of the heating the vapor is delivered from each vapor body in the manner indicated.
In the present instance, the liquor, partially concentrated in the cascade evaporator 8, is delivered to effect I6. After being heated therein and partially evaporated, the liquor is delivered through a pipe 34 to the effect II operating at a lower pressure. After heating in the effect I'I, the further concentrated liquor is delivered through a pipe 35 to the effect I8 for further concentration. From the effect I8, the liquor is Withdrawn through a pipe 36 and delivered by a pump 3l through a pipe 38 to effect I5, Where it is heated by vapor from the effects I3 and I4. From the effect I5 the liquor is Withdrawn through `a pipe 39 and is transferred by a pump 40 through a pipe 4I to effect I4, where it is heated with steam. From the effect I4 the liquor is Withdrawn through a pipe 43 and delivered by a pump 44 through a pipe 45 to effect I3, Where it is further concentrated by heating With steam.
Having attained its maximum concentration in effect I3, the liquor is withdrawn through a pipe 46 and delivered by a pump 41 and pipe 48 to the storage container 49. The latter is connected by a vent pipe 59 to the vapor body I9 of the effect I3 so that the pressure in the storage container 49 is identical with that in the vapor body I9 of effect I3. As the result thereof, the temperature of the liquor delivered to the storage container 49 should be in the neighborhood of 259 F., assuming that a pressure of fifteen pounds per square inch gauge is maintained in the vapor body I9 of effect I3. Because of the pressure maintained in the storage container 49, the liquid -Will remain `at substantially the same temperature which will be higher or lower, depending upon the pressure maintained in the vapor body I9 of effect I3.
The liquor at the high temperature maintained as a result of pressure in the storage container 49 isv in` thebest possible condition for ringwithout the necessity of employing steam for reheating the liquor before it is fired.V It is withdrawn frompthe storage container 45 through a pipe 5I and is delivered by a pump 52 through a pipe 53 vto the burner 54 of a furnace 55 having boiler tubes 53 wherein the heat developed by the Aburner 54 is utilized in producing steam for use in the plant. The method as described avoids the difficulties which have beenmet heretofore in handling concentrated liquor When the latter has beenpermitted to become partially cooled before it isdelivered to the furnace for combustion. Such cooling, as indicated, necessitates reheating because the combustion does not occur eiciently if the liquid is supplied attoo low a temperature. When it is held at a temperature approaching 250 F., the liquor burns readily, and no reheating is required in accordance with the present invention. v
Various changes may be made in the details of the operation as described Without departing from the inventionor sacrificingv the advantages thereof.
I claim:
1.V The method of burning concentrated Waste liquor from the Vdigestion of Vligno-cellulose material which comprises concentrating the liquor by multiple effect evaporation With at least the last eect maintained at over-atmospheric pressure, delivering the liquor at the .over-atmospheric pressure therein to a storage containen'maintaining' the pressure in the storage container substantially at that of the last effect, thereby conserving thev heat in the concentrated liquor, and delivering'the heated liquor at substantially the temperature maintained in the storage container to the burning Zone.
2. The method of burning concentrated Waste liquor from the digestion of ligno-cellulose material which comprises concentrating the liquor rst by cascade evaporation and then by multiple effect evaporation with at least the last eifect maintained Vat over-atmospheric pressure, delivering the liquor at the over-atmospheric pressure therein to `a storage container, maintaining the pressure in the storage .container substantially at that of the last effect,
' thereby conserving the heat in the concentrated liquor by multiple effect evaporation, the last eiect operating at a pressure in the range of 10-25 pounds per square inch, delivering the liquor from the last effect to a storage container, maintaining substantially the same pressure in both the last effect and the storage container, thereby conserving the heat in the concentrated liquor, and delivering the heated liquor at substantially the temperature maintained in the storage container to the burning zone.
4. The method of burning concentrated Waste liquor from the digestion of ligno-cellulose material which comprises circulating the liquor rst by cascade evaporation and then by multiple eiect evaporation, the last effect operating at a pressure in the range of 10-25 pounds per square inch, delivering the liquor from the last effect to a storage container, maintaining substantially the same pressure in both the last eiect and the storage container, thereby conserving the heat in the concentrated liquor, and delivering the heated liquor at substantially the temperature maintained in the storage container to the burning zone.
THOMAS W. STEWART.
REFERENCES CITED The following references are of record in the ie of this patent:
UNITED STATES PATENTS

Claims (1)

1. THE METHOD OF BURNING CONCENTRATED WASTE LIQUOR FROM THE DIGESTION OF LIGNO-CELLULOSE MATERIAL WHICH COMPRISES CONCENTRATION THE LIQUOR BY MULTIPLE EFFECT EVAPORATION WITH AT LEAST THE LAST EFFECT MAINTAINED AT OVER-ATMOSPHERIC PRESSURE, DELIVERING THE LIQUOR AST THE OVER-ATMOSPHERIC PRESSURE THEREIN TO A STORAGE CONTAINER, MAINTAINING THE PRESSURE IN THE STORAGE CONTAINER SUBSTANTIALLY AT THAT OF THE LAST EFFECT, THEREBY CONSERVING THE HEAT IN THE CONCENTRATED LIQUOR, AND DELIVERING THE HEATED LIQUOR AT SUBSTANTIALLY THE TEMPERATURE MAINTAINED IN THE STORAGE CONTAINER TO THE BURNING ZONE.
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2744571A (en) * 1953-09-28 1956-05-08 Goslin Birmingham Mfg Company Evaporating process
US2754897A (en) * 1951-01-22 1956-07-17 Ramen Torsten Processes for concentrating liquids containing incrustation-forming substances
US2884050A (en) * 1954-03-23 1959-04-28 Lloyd E Brownell Centrifugal evaporator
US3959067A (en) * 1974-12-06 1976-05-25 The A.P.V. Company Limited Concentration of volatiles-bearing products

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US780612A (en) * 1903-11-30 1905-01-24 Frederick Meyer Evaporating apparatus.
US1137780A (en) * 1913-08-14 1915-05-04 Hugh K Moore Method and means for treatment of waste liquors.
US2078288A (en) * 1935-07-24 1937-04-27 Socony Vacuum Oil Co Inc Method and apparatus for heating and deaerating boiler feed water
US2196498A (en) * 1936-12-23 1940-04-09 Monarch Governor Company Governor
US2303811A (en) * 1940-01-09 1942-12-01 Day And Zimmermann Inc Chemical recovery system for pulp mills
US2320294A (en) * 1940-04-23 1943-05-25 Weyerhacuser Timber Company Sulphite process
US2354175A (en) * 1940-07-27 1944-07-18 Babcock & Wilcox Co Apparatus for the recovery of heat and chemicals from waste liquor

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2403211A (en) * 1942-11-21 1946-07-02 Cash Charles Richard Percival Agitator for cascade evaporators

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US780612A (en) * 1903-11-30 1905-01-24 Frederick Meyer Evaporating apparatus.
US1137780A (en) * 1913-08-14 1915-05-04 Hugh K Moore Method and means for treatment of waste liquors.
US2078288A (en) * 1935-07-24 1937-04-27 Socony Vacuum Oil Co Inc Method and apparatus for heating and deaerating boiler feed water
US2196498A (en) * 1936-12-23 1940-04-09 Monarch Governor Company Governor
US2303811A (en) * 1940-01-09 1942-12-01 Day And Zimmermann Inc Chemical recovery system for pulp mills
US2320294A (en) * 1940-04-23 1943-05-25 Weyerhacuser Timber Company Sulphite process
US2354175A (en) * 1940-07-27 1944-07-18 Babcock & Wilcox Co Apparatus for the recovery of heat and chemicals from waste liquor

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2754897A (en) * 1951-01-22 1956-07-17 Ramen Torsten Processes for concentrating liquids containing incrustation-forming substances
US2744571A (en) * 1953-09-28 1956-05-08 Goslin Birmingham Mfg Company Evaporating process
US2884050A (en) * 1954-03-23 1959-04-28 Lloyd E Brownell Centrifugal evaporator
US3959067A (en) * 1974-12-06 1976-05-25 The A.P.V. Company Limited Concentration of volatiles-bearing products

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