US1715194A - Method of extracting candelilla wax - Google Patents

Method of extracting candelilla wax Download PDF

Info

Publication number
US1715194A
US1715194A US56507A US5650725A US1715194A US 1715194 A US1715194 A US 1715194A US 56507 A US56507 A US 56507A US 5650725 A US5650725 A US 5650725A US 1715194 A US1715194 A US 1715194A
Authority
US
United States
Prior art keywords
wax
rolls
candelilla wax
plant
matter
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US56507A
Inventor
Garcia Jose Trevino
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Application granted granted Critical
Publication of US1715194A publication Critical patent/US1715194A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B11/00—Recovery or refining of other fatty substances, e.g. lanolin or waxes

Definitions

  • This invention aimstoprovide a novel apparatus and method forextracting cande- 'lilla wax in'snch manner as to reduce. to a minimum the bulk of the material that must be carried through the processand yet be. highly etl'cetive in the recovery of the wax content from the plant.
  • a further object resides in the provision of a method and apparatus of this eharzwter which is reliable and etlicient in operation and adapted to be. carried out at a comparatively slight expense by means of iustrumentalities ordinarily available.
  • FIG. 1 is a dia rannnatic view partly in elevation and partly in section illustrating the method and the apparatus employed for carrying out the method
  • Figure 2 is a view in longitudinal section showing the decortieating machine employed as a unit of the apparatus, and
  • Figure 3 is a detail view of the adjustable bearing construction of the crusher mounted in the hopper of the decorticator.
  • each crusher comprises frame. members 2 in which a series of pairs of co-acting'crushing rolls are rotatably mounted, one pair of. rolls being designated at; 3 and the other pair of rolls being designated at 4.
  • the first pair of rolls, that is the rolls 3, are driven at a slow rate of speed, preferably at. the rate of one hundred and sixty revolutions per minute while the rolls 4 arepret'erably driven at a speed of four hundred revolutlons per minute.
  • the members of each pair of rolls have intermeshin g corrugations.
  • each pair of rolls is rotatably mounted in fixed bearings while the other member of each pair is rotatably mounted inslidable bearings urged by means of coil springs toward the fixed bearings so that the rolls are yieldably held in co-operatin'g relation.
  • the candelilla plant is passed through the rolls of the crusher and is thoroughly broken up so as to be prepared for the next step of the method which occurs in the decorticating machine, designated generally at 10.
  • the candelilla plant is passed through the rolls of the crusher and is thoroughly broken up so as to be prepared for the next step of the method which occurs in the decorticating machine, designated generally at 10.
  • decorticating machine comprises a suitable frame 11 on which a fixed conical casing 12 is mounted.
  • the casing 12 has an upperimperforate section 13 and a lower reticulated section constituted of wire mesh or the like.
  • a dust and wax receiving chamber 11 is positioned below the reticulated section of the casing.
  • An inner shell 16 of conical form and somewhat smaller than the outer shell is tixed on a shaft l'r'cxtending axially through the outer shell whereby the inner shell rotates within the outer shell.
  • a motor and suitable gearing is provided for driving the shaft. 17.
  • the inner and outer shells have co-acting dccorticating teeth 18 and 19, respectively, the teeth 18 projecting radially outward from the inner shell and'the teeth 19 projecting radially inward from the easing or outer shell.
  • the inaterial which has been crushed in the crusher is delivered from the hoppers 2-2 which enclose the crushers into the space between the co-acting shells of the derorticator.
  • the wax and dust are separated from the fiber of the plantdue to the tearing and beating action of the co-acting teeth. This action will be better appreciated when it is borne in mind thatthe inner shell rotatcs at a speed of from three hundred to four hundred revolutions per minute.
  • the wax and non-waxy matter in finely divided form are carried through the reticulated lower section l3 into the chamber 14 and the fiber is carried out through the discharge opening provided therefor at the large end of the machine.
  • the wax .and finely divided non-waxy matter are taken from the chamber 14. at suitable intervals and deposited in a vat 26 wherein the wax and finely divided non waxy matter are mixed with hot water and subjected to the action of steam in the well known manner for separating the waxy matter from the non-waxy matter.
  • the method of separating the waxy matter from the nonwaxy matter is well known in the art and since it forms no part of the present'invention, need not. he further explained. Since the melting point of the wax is between and 80 F. the heat; may approximate such a temperature or higher. WVhen' water is employed it is brought to the boiling point as is well known.
  • the chamber 14 is provided with suitable doors 30 to provide a closed chamber except when the finely divided non-waxy matter and wax taken therefrom and carried tothe we; 3
  • Oneofthe principal features of the invention resides in the manner in which the bulk of the plant is separated from'the wax-bearing content prior to the steps taken to recover the wax. In other words instead of carrying the whole bulk of the plant into'the vat and handling this bulk throughout the rebovery process the bulk is eliminated in the decortlcator andonly the wax and finely divided non-waxy matter remain to behandled.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Processing Of Solid Wastes (AREA)
  • Crushing And Grinding (AREA)

Description

May 28, 1929.
J. T. GARCIA METHOD OF EXTRACTING CANDELILLA WAX Filed Sept. 15. 1925 xNvE NToR 6421M 31/! ATTORNEYS Patented May 28, 1929.
PATENtioFFicE.
This invention aimstoprovide a novel apparatus and method forextracting cande- 'lilla wax in'snch manner as to reduce. to a minimum the bulk of the material that must be carried through the processand yet be. highly etl'cetive in the recovery of the wax content from the plant.
A further object resides in the provision of a method and apparatus of this eharzwter which is reliable and etlicient in operation and adapted to be. carried out at a comparatively slight expense by means of iustrumentalities ordinarily available.
Other objects and ad vantages reside in certain novel features which will be hereinafter more fully described and particularly pointed outin the appended claim forming a part of this specification, and in which Figure. 1 is a dia rannnatic view partly in elevation and partly in section illustrating the method and the apparatus employed for carrying out the method,
Figure 2 is a view in longitudinal section showing the decortieating machine employed as a unit of the apparatus, and
Figure 3 is a detail view of the adjustable bearing construction of the crusher mounted in the hopper of the decorticator.
Referring to the drawings, the numeral 1 designates the crushers mounted in the hoppers of the dccorticator and in which the first step of the method is carried out. Each crusher comprises frame. members 2 in which a series of pairs of co-acting'crushing rolls are rotatably mounted, one pair of. rolls being designated at; 3 and the other pair of rolls being designated at 4. The first pair of rolls, that is the rolls 3, are driven at a slow rate of speed, preferably at. the rate of one hundred and sixty revolutions per minute while the rolls 4 arepret'erably driven at a speed of four hundred revolutlons per minute. The members of each pair of rolls have intermeshin g corrugations. One member of each pair of rolls is rotatably mounted in fixed bearings while the other member of each pair is rotatably mounted inslidable bearings urged by means of coil springs toward the fixed bearings so that the rolls are yieldably held in co-operatin'g relation.
The candelilla plant is passed through the rolls of the crusher and is thoroughly broken up so as to be prepared for the next step of the method which occurs in the decorticating machine, designated generally at 10. The
-- JosEcTREvmo GARCIA, or raana's, MEXICO. airman 6F. E x'rRAcTINs CAND LIL'LA WAX. j
itch- .iizt. ltpp lication filcd.September- 15,1925, S cria1 1 Io 56,507, and in Mexico October 30, 1924.
decorticating machine comprises a suitable frame 11 on which a fixed conical casing 12 is mounted. The casing 12 has an upperimperforate section 13 and a lower reticulated section constituted of wire mesh or the like. A dust and wax receiving chamber 11 is positioned below the reticulated section of the casing. An inner shell 16 of conical form and somewhat smaller than the outer shell is tixed on a shaft l'r'cxtending axially through the outer shell whereby the inner shell rotates within the outer shell. A motor and suitable gearing is provided for driving the shaft. 17. The inner and outer shells have co-acting dccorticating teeth 18 and 19, respectively, the teeth 18 projecting radially outward from the inner shell and'the teeth 19 projecting radially inward from the easing or outer shell. The inaterial which has been crushed in the crusher is delivered from the hoppers 2-2 which enclose the crushers into the space between the co-acting shells of the derorticator. In the decorticator the wax and dust are separated from the fiber of the plantdue to the tearing and beating action of the co-acting teeth. This action will be better appreciated when it is borne in mind thatthe inner shell rotatcs at a speed of from three hundred to four hundred revolutions per minute. The wax and non-waxy matter in finely divided form are carried through the reticulated lower section l3 into the chamber 14 and the fiber is carried out through the discharge opening provided therefor at the large end of the machine.
The wax .and finely divided non-waxy matter are taken from the chamber 14. at suitable intervals and deposited in a vat 26 wherein the wax and finely divided non waxy matter are mixed with hot water and subjected to the action of steam in the well known manner for separating the waxy matter from the non-waxy matter. The method of separating the waxy matter from the nonwaxy matter is well known in the art and since it forms no part of the present'invention, need not. he further explained. Since the melting point of the wax is between and 80 F. the heat; may approximate such a temperature or higher. WVhen' water is employed it is brought to the boiling point as is well known.
The chamber 14 is provided with suitable doors 30 to provide a closed chamber except when the finely divided non-waxy matter and wax taken therefrom and carried tothe we; 3
' Oneofthe principal features of the invention resides in the manner in which the bulk of the plant is separated from'the wax-bearing content prior to the steps taken to recover the wax. In other words instead of carrying the whole bulk of the plant into'the vat and handling this bulk throughout the rebovery process the bulk is eliminated in the decortlcator andonly the wax and finely divided non-waxy matter remain to behandled.
I claim In the pre-treatment of the candelilla plant preparatory to the extraction of wax there- 15 from, the steps which comprise crushing said plant end'thereafter subjecting'the crushed plant to a. tearing and beating action .wherebyj wax and non-Waxy matter in finely divided form are separated from the fibers of the 20 plant, and screening the finely divided wax and non -wzixy matter from the fibers.
JOSE TREVINQ GARCIA.
US56507A 1924-10-30 1925-09-15 Method of extracting candelilla wax Expired - Lifetime US1715194A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
MX1715194X 1924-10-30

Publications (1)

Publication Number Publication Date
US1715194A true US1715194A (en) 1929-05-28

Family

ID=19746155

Family Applications (1)

Application Number Title Priority Date Filing Date
US56507A Expired - Lifetime US1715194A (en) 1924-10-30 1925-09-15 Method of extracting candelilla wax

Country Status (1)

Country Link
US (1) US1715194A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2015185685A1 (en) * 2014-06-04 2015-12-10 Jena Trading Aps Separation of wax and fibers from plants
US10723972B2 (en) 2014-06-04 2020-07-28 Jena Trading Aps Method and plant for separation of wax and fibers from plants
US12448730B2 (en) 2019-01-22 2025-10-21 Jena Trading Aps Preparation of cellulose fibers
US12553008B2 (en) 2019-04-30 2026-02-17 Jena Trading Aps Extracting and refining plant cuticular waxes from aqueous dispersion using temperature and pH adjustment

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2015185685A1 (en) * 2014-06-04 2015-12-10 Jena Trading Aps Separation of wax and fibers from plants
CN107075409A (en) * 2014-06-04 2017-08-18 耶拿贸易有限公司 Wax and fiber are separated from plant
US20170253831A1 (en) * 2014-06-04 2017-09-07 Jena Trading Aps Separation of wax and fibers from plants
US10723972B2 (en) 2014-06-04 2020-07-28 Jena Trading Aps Method and plant for separation of wax and fibers from plants
US11407961B2 (en) 2014-06-04 2022-08-09 Jena Trading Aps Method and plant for separation of wax and fibers from plants
US12448730B2 (en) 2019-01-22 2025-10-21 Jena Trading Aps Preparation of cellulose fibers
US12553008B2 (en) 2019-04-30 2026-02-17 Jena Trading Aps Extracting and refining plant cuticular waxes from aqueous dispersion using temperature and pH adjustment

Similar Documents

Publication Publication Date Title
DE69210467T2 (en) Process for the production of vegetable pulp for the production of juice and puree and a device for carrying out the process
CN205380908U (en) Soybean oil production is with rolling embryo machine with crude oil separation work ability
DE4041994B4 (en) Method and device for peeling fresh rapeseed
US4028222A (en) Method for extracting oil from oil shale
US2650176A (en) Methods of separating sugar juice, pith, and fiber from stalks
US2267048A (en) Centrifugal extractor and method of extraction
US1972666A (en) Method and machine for the treatment of grain
US731736A (en) Method of expressing oil from seeds.
US1956615A (en) Method of producing tomato juice
CN207025486U (en) A kind of multistage tea oil cold press device
US3135021A (en) Rotary rib cotton gin
US523116A (en) Witsch gelinck
US1374657A (en) Method of separating fruit-pits and their kernels
US2158427A (en) Process for extracting oil or fat containing substances and the like
DE553710C (en) Schlagwerkmuehle for breaking down coal into its petrographic components
US3632051A (en) Method for treating maize seeds
CN107307436A (en) A kind of rubber fruit is peeled off packing device
US1928241A (en) Process of conditioning oil bearing materials
US1364222A (en) Apparatus for separating tip ends of bean-pods
US1099299A (en) Boll-cotton gin.
US1399891A (en) Process of isolating fiber from bagasse
US732040A (en) Cider-press.
US1335619A (en) Machine fob treating vegetable waste
US2618643A (en) Method of recovering oil from castor beans or the like
US658876A (en) Treatment of cotton-seed.