US1566921A - Oil still - Google Patents

Oil still Download PDF

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Publication number
US1566921A
US1566921A US390088A US39008820A US1566921A US 1566921 A US1566921 A US 1566921A US 390088 A US390088 A US 390088A US 39008820 A US39008820 A US 39008820A US 1566921 A US1566921 A US 1566921A
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Prior art keywords
oil
bank
tubes
still
separator
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Expired - Lifetime
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US390088A
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Primrose John
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POWER SPECIALTY Co
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POWER SPECIALTY CO
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Publication date
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Priority to US390088A priority Critical patent/US1566921A/en
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Publication of US1566921A publication Critical patent/US1566921A/en
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G9/00Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C10G9/06Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils by pressure distillation
    • C10G9/08Apparatus therefor
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G7/00Distillation of hydrocarbon oils

Definitions

  • Iriy present improvement consists in providing a return passage for unvolatilized oil from the separator to the said second bank of tubes, and providing means for forcing oil to flow through said bank a second time, whereby the unvolatilized parts thereof will be driven off by such second or repeated heating and a lar r output of vapor thus obtained.
  • the heating chamber 1 of the still is of the usual character, and is, in the present i11- stance, divided by a vertical wall 2 into a forward and a rear compartment.
  • a vertical wall 2 In the latter is a bank of oil tubes or pipes 3 connected in any proper and known manner for causing the oil from the source of supply 4 to flow upward through the tubes of the bank or in a direction counter to the How of the hot gases which pass downward in this compartment on their way to the flue.
  • a second and smaller bank 5 of'oil tubes In the forward compartment is a second and smaller bank 5 of'oil tubes, the lowermost row of which is connected with the uppermost row in the first bank, and such smaller bank is connected by a pipe 6 to any suitable form of separator 7.
  • the flow of oil in the second bank is not, and need not be,

Description

Dec. 22, 1925- J. PRIMROSE OIL STILL Filed June 19 1920 v- W ATTOR 5V8 8) [WW 1 I 7% Patented Dec. 22, 1925.
UNITED STATES 1,566,921 PATENT OFFICE.
JOHN PRIMROSE, OF NEW YORK, N. Y., ASSIGNOR TO' POWER SPECIALTY COMPANY,
OF YORK, N- Y-, A CORPORATION OF NEW YORK.
OIL s'rILL.
Application filed June 19, 1920., Serial No. 390,088.
To all whom it may concern:
Be it known that I, Join: PRIMROSE, a citizen of the United States, residing at New York, in the county and State of New York, have invented certain new and useful Im-- provements in ()il Stills, of which the following is a full, clear, and exact description.
.by a vertical bridge wall into two compartments. In that which is the more remote from the fire the heatabsorbing tubes or pipes carrying the oil are arranged in one main group, over which the hot gases flow downwardly, While the oil, introduced cold at the bottom of the bank, flows counter to the current of hot gases. After passing through this bank of tubes the hot oil is carried over to-the bottom of a smaller bank of tubes in the compartment over the fire, and the top of such bank is connected to the usual se arator for taking off the vapors set free by the 'heat and delivering the unvaporized oil to a suitable receptacle.
This form of still is described merely as typical of all stills to which my imprpvement is applicable, and in such stills it has been found that the oil in the final heat absorption stage, or in the second bank of coils where it is exposed to the highest temperature, does not give off all of the vapors which it should, but-thatka certain proportion of its volatile constituents goes over to the separator w'th the oil.
It is to reme y this objection and to increase the yield of the volatile constituents of the oil that Iriy present improvement was devised, and it consists in providing a return passage for unvolatilized oil from the separator to the said second bank of tubes, and providing means for forcing oil to flow through said bank a second time, whereby the unvolatilized parts thereof will be driven off by such second or repeated heating and a lar r output of vapor thus obtained.
'ggecifically considered, the construction of the still is not of the essence of the invention, provided the condition herein described obtains, and the invention is not therefore limited in its scope, but consists broadly in the combination with the hottest elemcnts of the heating surface of means for returning and forcing through the same the uuvaporizcd oil or any desired portion of the same which has already passed through them.
The invention is illustrated in the accompanying drawing, which is a view largely diagrammatic of a still of the kind described with my invention applied thereto.
The heating chamber 1 of the still is of the usual character, and is, in the present i11- stance, divided by a vertical wall 2 into a forward and a rear compartment. In the latter is a bank of oil tubes or pipes 3 connected in any proper and known manner for causing the oil from the source of supply 4 to flow upward through the tubes of the bank or in a direction counter to the How of the hot gases which pass downward in this compartment on their way to the flue.
In the forward compartment is a second and smaller bank 5 of'oil tubes, the lowermost row of which is connected with the uppermost row in the first bank, and such smaller bank is connected by a pipe 6 to any suitable form of separator 7. The flow of oil in the second bank is not, and need not be,
counter to the flow of gases, as the oil has reached a temperature when it enters the second bank that makes this unnecessary for good results.
From the separator the vapors are taken off, as by means of a pipe 8, and the unvolatilized oil by a pipe 9 at the bottom, but by means of apipe 10 any proportion of this oil that may be desired or found necessary is led to a pump 11, by which it is forced back to the connection 12 between the first and second banks of tubes, and hence caused to flow again through the hottest tubes, or those of the smaller second bank.
By this means it has been found that much Va or that is not given off by the first run of Oll is set free on its subsequent travel through the second hot bank.
Manifest-1y the construction of the still as a whole is largely immaterial. As is usual in practice, it will be provided with the proper controlling valves, with means for indicating the temperature of the oil and other known accessories.
- What I claim is:
1. The combination with an oil still hav" ing banks or groups of tubes exposed to the passed through the still, for the purpose set v forth.
2. The combination with'an oil still, of a furnace comprising two compartments, a
bank of tubes in that compartment more remote from the fire, a bank of tubes in the compartment nearer the fire connected in series with the first, and means including an oil supplying connection intermediate the first and second banks for forcing oil that has passed through and issued from the second bank back to and through said bank, for the purpose set forth.
3. The combination with an oil still hav ing two banks of tubes and means for causing-the oil to flow counter to the hot gases in the bank which is the more remote from the fire, of a separator connected with the bank which is nearer the fire, a connection for oil from the separator back to the second bank and a pump therein for causing oil after having passed through said second bank and separator to reflow through the second bank, for the purpose set forth.
at. The combination with an oil still having two banks of tubes, one near the fire and the other more remote therefrom, means for causing the oil to flow counter to hot gases in the latter bank and in the direction of the passage of the hot gases in the former bank, a separator connected with the outlet of the bank nearest the fire, and means for causing oil to flow back from the separator to the inlet of said former bank, said means being independent of the oil supplying means for the said latter bank.
in testimony whereof I hereto affix my signature.
JOHN PRIMROSE.
US390088A 1920-06-19 1920-06-19 Oil still Expired - Lifetime US1566921A (en)

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US390088A US1566921A (en) 1920-06-19 1920-06-19 Oil still

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US390088A US1566921A (en) 1920-06-19 1920-06-19 Oil still

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US1566921A true US1566921A (en) 1925-12-22

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