US128234A - Improvement in apparatus for generating carbonic-acid gas - Google Patents
Improvement in apparatus for generating carbonic-acid gas Download PDFInfo
- Publication number
- US128234A US128234A US128234DA US128234A US 128234 A US128234 A US 128234A US 128234D A US128234D A US 128234DA US 128234 A US128234 A US 128234A
- Authority
- US
- United States
- Prior art keywords
- valve
- generator
- marble
- gas
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- CURLTUGMZLYLDI-UHFFFAOYSA-N carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 title 2
- 235000011089 carbon dioxide Nutrition 0.000 title 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 22
- 239000002253 acid Substances 0.000 description 20
- BVKZGUZCCUSVTD-UHFFFAOYSA-N Carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 16
- 239000004579 marble Substances 0.000 description 8
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate dianion Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 6
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 6
- 235000015450 Tilia cordata Nutrition 0.000 description 6
- 235000011941 Tilia x europaea Nutrition 0.000 description 6
- 239000004571 lime Substances 0.000 description 6
- 238000007599 discharging Methods 0.000 description 4
- 239000004615 ingredient Substances 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- 239000002699 waste material Substances 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 238000007664 blowing Methods 0.000 description 2
- 230000003467 diminishing Effects 0.000 description 2
- 239000000428 dust Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 235000011149 sulphuric acid Nutrition 0.000 description 2
- 239000001117 sulphuric acid Substances 0.000 description 2
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/002—Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
Definitions
- a vertical generator .with a stuffing-box on top that serves both for the agitator and a valve or valves, by which the marble dust is admitted to the generator in a gradual and showerlike manner at various points or places of distribution, over a column of liquid acid of suitable strength, through which it descends.
- the agitator and valve above referred to both being operated in commonthat, is, through or by the same stem or shaftnot only allows of the one stuffing-box sufficing, buta proper relative action of the agitator to the supply of marble-dust is kept up, and'a more thorough or intimate contact of the marble with the acid, as the former descends through the latter, is effected.
- the invention also embraces a perforated tubular step-bearingfor the agitator-shaft, in the bottom of the genera-tor, for-drawing off the residuum below.
- the invention likewise consists in a certain arrangement of handles for operating the valve that admits the marble-dust relatively to the openings in the valve or valve-seat and openings through which the marble-dust and other ingredients are introduced, whereby said handles also form guards to prevent the last-mentioned openings being exposed for the purpose of resupplying the generator when the valve is open, thus preventing-that is, by the closed position of the valve or closed condition of the valve-seat-waste and back action of the gas in the generator on the marble-dust, causing the latter to blow or fly into the eyes of the attendant or otherwise.
- the invention furthermore embraces a combination, with a washer or purifier and the water therein, of broken pieces or lumps of carbonate of lime or other material containing carbonic acid, whereby less water is required to efi'ect the washing of the gas as it passes from the generator, and consequently there is a reduced absorption of the carbonic acid; also the latter is made to pass more circuitously through the washer, and is, therefore, more thoroughly exposed; and the. carbonate of lime in the washer takes up any excess of sulphuric acid passing off in a free state; also adds to the carbonic acid.
- the invention likewise consists in a combination of a force-pump, as an integral part of the apparatus, with the generator thereof, for the purpose of expelling, by forcing in water, the carbonic acid at a high pressure from the generator, and clearing the latter of gas.
- a A represent the generator of the apparatus, the upper portion, A, being separated from the lower portion, A, by a disk or diaphragm, b, which has openings 0 c in it for introduction of the marble-dust and water to the lower andxmaiu portion A of the generator, and for the escape of the carbonic acid as evolved in the latter.
- These openings 0 c are controlled by a revolving valve, B, carried by an upright stem or shaft, 0, said valve being formed of arms or covering-surfacesof about or a little more than the area of the openings 0 a, so that as the valve is rotated it opens and closes said openings. Any other suitable form of valve may be used.
- the stem 0 is arranged to project through a stuffing-box, E, in the top of the generator, and extends downward to or near the bottom of the generator, where it works in a stepbearing, 13.
- This step-bearin g is formed of a tube arranged to screw or project up into the generator at its lowest point, and perforated, as at (Z (1, below its support of the stem or shaft 0, whereby all the residuum in the generator may be drawn off from time to time, as required, and which a lateral arrangement of said tube as a mere discharging device would not effect.
- a discharge-pipe is connected with this perforated tubular step-bearing outside of the generator, and the same fitted with a valve, 6, for opening and closing the discharge, as required.
- the stem or shaft 0 is provided below with an agitator, G, so that the same stem, 0, working through the one stufiing-box, IE, not only operates the valve to supply the lower and gas-evolving portion A of the generator with marble-dust, but to simultaneously set in motion the agitator to stir up the diluted acid and marble-dust descending therethrough, and this in proper relation with the admission of the marble, the agitator stopping, when the valve B is at rest, over the openings 0 c, and increasing or diminishing its action with the more rapid or slower rotation of the valve.
- Said agitator may be variously shaped or constructed.
- the marbledust is admitted to the upper portion or chamber A of the generator by an inlet, H, and, as the valve B is rotated, is distributed, at various points and in broken showers, through the openings 00, descending through the column of diluted acid in the lower part of the generator, and the whole contents being thoroughly stirred by the agitator during such descent of the dust, thus bringing the marble into intimate contact with the acid, and expediting the evolution of the gas.
- the liquid acid Prior to the introduction of the marbledust the liquid acid is admitted, as by a tube or inlet, I, arranged to project through the upper portion, A, of the generator and diaphragm or disk b, and the water to dilute the acid is introduced, by an inlet or pipe, J, to the chamber A, at or near its top, passing down through the valve, and washing out any remaining marble-dust in said chamber.
- a tube or inlet, I arranged to project through the upper portion, A, of the generator and diaphragm or disk b
- the water to dilute the acid is introduced, by an inlet or pipe, J, to the chamber A, at or near its top, passing down through the valve, and washing out any remaining marble-dust in said chamber.
- the water may be forced in by a pump, K, that forms an integral portion of the apparatus, and which is more especially designed to expel, by forcing in water, the gas from the generator at a high pressure after the evolution of fresh gas has ceased.
- Said pump may be variously constructed, but is here shown as operated by'a brake, f, and
- L is the outlet or pipe which conducts the gas as made to the washer and purifier M, from which it passes off by an outlet, 70.
- This washer in addition to being charged with water, is also supplied with lumps, x .r, of car bonate of lime or other material containing m m, and these are so set, in relation with the valve B and the different openings through which the ingredients are admitted to the generator, that they act as guards to check or prevent the opening of said inlets when the valve B is open or apertures c c uncovered by it, thereby avoiding waste of gas from the generator and blowing or flying of the mar ble-dust by the pressure of the gas at or vthrough the inlet when attempting to admit it.
- the handles m m are set so that they lie over the inlets H I J and outlet L, or certain of them, when the valve B is open, or openings '0 c not covered by'it, thus making it inconvenient to get at said inlets; but when the valve B is closed, then the handles m m occupy an intermediate position to the inlets, especially to the inlets H and I, as represented in Figs. 2 and 4, thereby giving ready access to said inlets, or indicating, by the position of the handles, that the valve B is closed, and that it will be safe to admit of a fresh supply of marble-dust, or otherwise establish communication with the exterior of the generator.
- valve B and agitator G with the stem or shaft 0 and single stuffing-box E on top of the generator, substantially as and for the purposes herein set forth.
Description
2 Sheets--Sheet1.
JOHN MATTH EWS.
Improvement in Apparatus for Generating Carbonic Acid Gas.
Patented June 25,1872.
2 Sh t sh "2'. JOHN MATTHEWS.
in Apparatus for Generating Carbonic Acid Gas.
Improvement Patented June 25, 1872.
UNITED STATES PATENT OFFICE;
JOHN MATTHEWS, OF NEW YORK, N. Y.
IMPROVEMENT-IN APPARATUS FOR GENERATING CARBONlC-ACID GAS.
Specification forming part of Letters Patent No. 128,234, dated June 25, 1872; antedated June 7, 1872.
To all whom it may concern:
Be it known that I, JOHN MATTHEWS, of the city, county, and State of New York, have invented certain new and useful Improvements in Apparatus for Evolving Carbonic Acid; of which the following is a full, clear, and exact description, reference being had to p the accompanying drawing forming part of this ures.
My invention in apparatus for evolving carbonic acid, applicable to the manufacture ofsoda-water and other purposes, embraces a vertical generator, .with a stuffing-box on top that serves both for the agitator and a valve or valves, by which the marble dust is admitted to the generator in a gradual and showerlike manner at various points or places of distribution, over a column of liquid acid of suitable strength, through which it descends. By thus admitting the marble-dust to the diluted acid the former is more thoroughly actednpon by the latter, and a uniform strength of acid is preserved. When, as previously practiced, the marble is first introduced, it is necessary to admit the water before letting on the acid,
which latter is accordingly at first or for a While too much diluted. Furthermore, the agitator and valve above referred to, both being operated in commonthat, is, through or by the same stem or shaftnot only allows of the one stuffing-box sufficing, buta proper relative action of the agitator to the supply of marble-dust is kept up, and'a more thorough or intimate contact of the marble with the acid, as the former descends through the latter, is effected. The invention also embraces a perforated tubular step-bearingfor the agitator-shaft, in the bottom of the genera-tor, for-drawing off the residuum below.
The invention likewise consists in a certain arrangement of handles for operating the valve that admits the marble-dust relatively to the openings in the valve or valve-seat and openings through which the marble-dust and other ingredients are introduced, whereby said handles also form guards to prevent the last-mentioned openings being exposed for the purpose of resupplying the generator when the valve is open, thus preventing-that is, by the closed position of the valve or closed condition of the valve-seat-waste and back action of the gas in the generator on the marble-dust, causing the latter to blow or fly into the eyes of the attendant or otherwise. The invention furthermore embraces a combination, with a washer or purifier and the water therein, of broken pieces or lumps of carbonate of lime or other material containing carbonic acid, whereby less water is required to efi'ect the washing of the gas as it passes from the generator, and consequently there is a reduced absorption of the carbonic acid; also the latter is made to pass more circuitously through the washer, and is, therefore, more thoroughly exposed; and the. carbonate of lime in the washer takes up any excess of sulphuric acid passing off in a free state; also adds to the carbonic acid. The invention likewise consists in a combination of a force-pump, as an integral part of the apparatus, with the generator thereof, for the purpose of expelling, by forcing in water, the carbonic acid at a high pressure from the generator, and clearing the latter of gas.
Referring to the accompanying drawing, A A represent the generator of the apparatus, the upper portion, A, being separated from the lower portion, A, by a disk or diaphragm, b, which has openings 0 c in it for introduction of the marble-dust and water to the lower andxmaiu portion A of the generator, and for the escape of the carbonic acid as evolved in the latter. These openings 0 c are controlled by a revolving valve, B, carried by an upright stem or shaft, 0, said valve being formed of arms or covering-surfacesof about or a little more than the area of the openings 0 a, so that as the valve is rotated it opens and closes said openings. Any other suitable form of valve may be used.
The stem 0 is arranged to project through a stuffing-box, E, in the top of the generator, and extends downward to or near the bottom of the generator, where it works in a stepbearing, 13. This step-bearin g is formed of a tube arranged to screw or project up into the generator at its lowest point, and perforated, as at (Z (1, below its support of the stem or shaft 0, whereby all the residuum in the generator may be drawn off from time to time, as required, and which a lateral arrangement of said tube as a mere discharging device would not effect. A discharge-pipe is connected with this perforated tubular step-bearing outside of the generator, and the same fitted with a valve, 6, for opening and closing the discharge, as required.
The stem or shaft 0 is provided below with an agitator, G, so that the same stem, 0, working through the one stufiing-box, IE, not only operates the valve to supply the lower and gas-evolving portion A of the generator with marble-dust, but to simultaneously set in motion the agitator to stir up the diluted acid and marble-dust descending therethrough, and this in proper relation with the admission of the marble, the agitator stopping, when the valve B is at rest, over the openings 0 c, and increasing or diminishing its action with the more rapid or slower rotation of the valve. Said agitator may be variously shaped or constructed.
The marbledust is admitted to the upper portion or chamber A of the generator by an inlet, H, and, as the valve B is rotated, is distributed, at various points and in broken showers, through the openings 00, descending through the column of diluted acid in the lower part of the generator, and the whole contents being thoroughly stirred by the agitator during such descent of the dust, thus bringing the marble into intimate contact with the acid, and expediting the evolution of the gas.
Prior to the introduction of the marbledust the liquid acid is admitted, as by a tube or inlet, I, arranged to project through the upper portion, A, of the generator and diaphragm or disk b, and the water to dilute the acid is introduced, by an inlet or pipe, J, to the chamber A, at or near its top, passing down through the valve, and washing out any remaining marble-dust in said chamber.
The water may be forced in by a pump, K, that forms an integral portion of the apparatus, and which is more especially designed to expel, by forcing in water, the gas from the generator at a high pressure after the evolution of fresh gas has ceased. Said pump may be variously constructed, but is here shown as operated by'a brake, f, and
as drawingin water'up one column, g, and discharging it down another column, h, to the pipe J, the valves of the pump being at i and j.
L is the outlet or pipe which conducts the gas as made to the washer and purifier M, from which it passes off by an outlet, 70. This washer, in addition to being charged with water, is also supplied with lumps, x .r, of car bonate of lime or other material containing m m, and these are so set, in relation with the valve B and the different openings through which the ingredients are admitted to the generator, that they act as guards to check or prevent the opening of said inlets when the valve B is open or apertures c c uncovered by it, thereby avoiding waste of gas from the generator and blowing or flying of the mar ble-dust by the pressure of the gas at or vthrough the inlet when attempting to admit it. Thus the handles m m are set so that they lie over the inlets H I J and outlet L, or certain of them, when the valve B is open, or openings '0 c not covered by'it, thus making it inconvenient to get at said inlets; but when the valve B is closed, then the handles m m occupy an intermediate position to the inlets, especially to the inlets H and I, as represented in Figs. 2 and 4, thereby giving ready access to said inlets, or indicating, by the position of the handles, that the valve B is closed, and that it will be safe to admit of a fresh supply of marble-dust, or otherwise establish communication with the exterior of the generator.
What is here claimed, and desired to be secured by Letters Patent, is-
1. The combination of the valve B and agitator G with the stem or shaft 0 and single stuffing-box E on top of the generator, substantially as and for the purposes herein set forth.
2. The combination of the perforated tubular step or bearing F with the stem 0 and generator or lower portion A thereof, essentially as described.
3. The combination of the handles m m with the valve-stem 0, when arranged in relation with the valve or openings 0 c in the valve seat, and inlets and outlets, or certain of them, by which communication is established with the exterior of the generator, whereby said handles are made to form guards to check or evolving carbonic acid, of a force-pump, arranged to connect with the generator at or near its top, and forming an integral portion of said apparatus, to efl'ect the expulsion of the gas, essentially as herein described.
JOHN MATTHEWS.
Witnesses:
Trmo. M. TUTHILL, R1031). W. MOTT.
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US128234A true US128234A (en) | 1872-06-25 |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20030216996A1 (en) * | 2002-05-14 | 2003-11-20 | Capital One Financial Corporation | Methods and systems for providing financial payment services |
US8469583B1 (en) * | 2012-02-13 | 2013-06-25 | U.S. Department Of Energy | Radial flow pulse jet mixer |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20030216996A1 (en) * | 2002-05-14 | 2003-11-20 | Capital One Financial Corporation | Methods and systems for providing financial payment services |
US8469583B1 (en) * | 2012-02-13 | 2013-06-25 | U.S. Department Of Energy | Radial flow pulse jet mixer |
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