US1064723A - Ore concentration. - Google Patents

Ore concentration. Download PDF

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Publication number
US1064723A
US1064723A US58762110A US1910587621A US1064723A US 1064723 A US1064723 A US 1064723A US 58762110 A US58762110 A US 58762110A US 1910587621 A US1910587621 A US 1910587621A US 1064723 A US1064723 A US 1064723A
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froth
ore
mixture
agitating
finely divided
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US58762110A
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Henry Howard Greenway
Henry Lavers
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Minerals Separation Ltd
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Minerals Separation Ltd
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
    • B03D1/00—Flotation
    • B03D1/001—Flotation agents
    • B03D1/004—Organic compounds
    • B03D1/012—Organic compounds containing sulfur
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S209/00—Classifying, separating, and assorting solids
    • Y10S209/901—Froth flotation; copper

Definitions

  • This invention relates to improvements in ore concentration and has for its object the separation of certain constituents of an ore, such as metallic sulfids -from other constituents such as gangue when the ore is suspended in a liquid such as water.
  • the crushed ore is introduced into water to which is added a very small quantity of an essential oil, and the mixture is thoroughly agitated.
  • the ore particles are thus or thereafter caused to come into contact with a gas such as air: the result is that metallic sulfid particles float to the surface in the form of a froth or scum and can thereafter be separated by any well known means.
  • the essential oils which we have found suitable for this purpose are the essential oils of eucalyptus, cinnamon, thyme, SflSSflfIfiS, pennyroyal, peppermint, cloves, lavender, sandalwood, Wintergreen and rosemary, or mixtures of these, but we do not confine our to these essential oils.
  • ⁇ Ve have hereinafter, in the broader claims, designated a suitable essential oil for this process as a froth producing essential oil.
  • lVater containing a small percent-age of sulfuric acid in solution, say from 0.1% to 0.5%, and containing also a small quantity say 0.4 lbsato 2.25 lbs. per ton of ore to be treated of an essential oil such as eucalyptus oil is with finely pulverized ore introduced into an agitating apparatus in the proportion of from three to five parts by weight of water to one part by weight of ore.
  • an essential oil such as eucalyptus oil
  • agitation is carried out in such a way as thoroughly to disseminate air through the' mixture which is thereafter discharged into a spitzkasten. It is found that a froth floats on the surface of the water in the spit-zkasten. This froth contains a large proportion of the metallic sulfids but is substantially free from gangue. Any well known means may be employed for collecting the froth.
  • the resulting tailings can be retreated by the same process with or without the addition of fresh quantities of the substances referred to.
  • the action may be in some instances be improved by heating the mixture and in some instances, as in the concentration of copper pyrites, the operation may be conducted without the addition of acid.
  • agitation vessels A are placed in series. These may conveniently be large vats separated by partitions A having openings A at the bottom so that the liquid may pass from one to another.
  • Each vessel is provided with a rotatable stirrer B which is conveniently of the formshown in the drawing. Each stirrer is carried on a spindle B rotated at a high speed by any convenient means. Crushed ore or similar finely divided mineral is fed into the first vessel A through any convenient ore-feeding device such as C, and water is also fed into the vessel A.
  • a small proportion of one or more essential oils which enable metallic sulfidsto be floated by air under the conditions specified may be-introduced from the feeding vessels D and The liquid containing ore in suspension is vigorously agitated in the agitation vessels and escapes at the outlet A highly charged with air.
  • a settling apparatus consisting of one or more spitzkasten F, is placed immediately at the outlet from the agitation apparatus.
  • the spitzkasten F has a launder G to receive the floating froth which passes away through the outlet G
  • the liquid and the sunken material pass out through the outlet H at the bottom of the spitzkasten.
  • the level of the liquid in the spitzkasten is slightly above the lip J.
  • an inclined baffle or guide plate K which may be made adjustable, extending upward from below the inlet A and arranged Y to direct the stream of ore particles and air-bubbles toward the surface of the liquid in the spitzkasten.

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Description

H. H. GREBNWAY 8: H. LAVERS,
ORE CONCENTRATION.
APPLICATION FILED OCT. 17, 1910.
. 1,064,723, Patented June 17, 1913.
HEN s'rn HENRY HOWARD GREENWAY, OF MELBOURNE, VICTORIA, AND HENRY LAVERS, OF
BROKEN HILL, NEW SOUTH WALES. AUSTRALIA, ASSIGNORS TO MINERALS SEPA- RATION LIMITED, OF LONDON, ENGLAND.
ORE CONCENTRATION.
Specification of Letters Patent.
Patented June 17, 1913.
Application filed October 17, 1910. Serial No. 587,621.
Commonwealth of Australia, have invented new and useful Improvements in Ore Concentration, of which the following is a specification.
This invention relates to improvements in ore concentration and has for its object the separation of certain constituents of an ore, such as metallic sulfids -from other constituents such as gangue when the ore is suspended in a liquid such as water.
According to this invention the crushed ore is introduced into water to which is added a very small quantity of an essential oil, and the mixture is thoroughly agitated. The ore particles are thus or thereafter caused to come into contact with a gas such as air: the result is that metallic sulfid particles float to the surface in the form of a froth or scum and can thereafter be separated by any well known means. Among the essential oils, which we have found suitable for this purpose are the essential oils of eucalyptus, cinnamon, thyme, SflSSflfIfiS, pennyroyal, peppermint, cloves, lavender, sandalwood, Wintergreen and rosemary, or mixtures of these, but we do not confine ourselves to these essential oils.
\Ve have hereinafter, in the broader claims, designated a suitable essential oil for this process as a froth producing essential oil.
The following is an example of one method of carrying this invention into eifect:
lVatercontaining a small percent-age of sulfuric acid in solution, say from 0.1% to 0.5%, and containing also a small quantity say 0.4 lbsato 2.25 lbs. per ton of ore to be treated of an essential oil such as eucalyptus oil is with finely pulverized ore introduced into an agitating apparatus in the proportion of from three to five parts by weight of water to one part by weight of ore. The
agitation is carried out in such a way as thoroughly to disseminate air through the' mixture which is thereafter discharged into a spitzkasten. It is found that a froth floats on the surface of the water in the spit-zkasten. This froth contains a large proportion of the metallic sulfids but is substantially free from gangue. Any well known means may be employed for collecting the froth.
If desired the resulting tailings can be retreated by the same process with or without the addition of fresh quantities of the substances referred to.
The action may be in some instances be improved by heating the mixture and in some instances, as in the concentration of copper pyrites, the operation may be conducted without the addition of acid.
To graphically illustrate one way of practicing the present invention, there has been shown in the accompanying drawings a perspective view of one form of apparatus, parts being broken away to disclose the interior construction.
Several agitation vessels A are placed in series. These may conveniently be large vats separated by partitions A having openings A at the bottom so that the liquid may pass from one to another. Each vessel is provided with a rotatable stirrer B which is conveniently of the formshown in the drawing. Each stirrer is carried on a spindle B rotated at a high speed by any convenient means. Crushed ore or similar finely divided mineral is fed into the first vessel A through any convenient ore-feeding device such as C, and water is also fed into the vessel A. A small proportion of one or more essential oils which enable metallic sulfidsto be floated by air under the conditions specified may be-introduced from the feeding vessels D and The liquid containing ore in suspension is vigorously agitated in the agitation vessels and escapes at the outlet A highly charged with air.
A settling apparatus consisting of one or more spitzkasten F, is placed immediately at the outlet from the agitation apparatus. As shown in the drawing, the spitzkasten F has a launder G to receive the floating froth which passes away through the outlet G The liquid and the sunken material pass out through the outlet H at the bottom of the spitzkasten. The level of the liquid in the spitzkasten is slightly above the lip J. Within the spitzkasten is placed an inclined baffle or guide plate K, which may be made adjustable, extending upward from below the inlet A and arranged Y to direct the stream of ore particles and air-bubbles toward the surface of the liquid in the spitzkasten.
We claim:
1. The herein described process of concenr trating ores, which consists in mixing finely divided ore with water containing a frothproducing essential oil, agitating the mixture to form a froth, and separating the froth.
2. The herein described process of concentrating ores, which consists in mixing finely divided ore with water containing a small quantity of a froth-producing essential oil, agitating the mixture to form a froth, and separating the froth.
3. The herein described process of concentrating ores which consists in mixing finely divided ores with Water containing a frothproducing essential oil, heating the mixture, agitating the heated mixture to form a froth, and separating the froth.
4. The herein described process of concentrating ores, which consists in mixing finely divided ores with water containing eucalyptus oil, agitating the mixture to form a froth, and separating the froth.
5. The herein described process of concentrating ores, which consists in mixing finely divided ores with water containing a small quantity of eucalyptus oil, agitating the mixture to form a froth, and separating the froth.
6. The'herein described process of concentrating ores, which consists in mixing finely divided ore with water containing eucalyptus oil, heating the mixture, agitating the heated mixture to form a froth, and separating the froth.
7. The herein-described process of concentrating ores, which consists in mixing the ore in a finely divided condition with water and a froth-producing essential oil, the latter in the proportion of less than one-fifth of one per centum of the ore, agitating the mixture to form a froth and separating the froth. 1
8. The herein-described process of concentrating ores, which consists in mixing the ore in a finely divided condition with water and eucalyptus oil, the latter in the proportion of from 02% to .1% of the ore, agitating the mixture to form a froth and separating the froth.
In testimony whereof we have signed our names to this specification. in the presence of two subscribing Witnesses.
HENRY HOWARD GREENVVAY.
\Vitnesses CHARLES NICHOLAS CoLLisoN, VV. H. CUBLEY.
HENRY LAVERS.
Witnesses:
THOS. RoUNswELL, EDW. PovEY.-
US58762110A 1910-10-17 1910-10-17 Ore concentration. Expired - Lifetime US1064723A (en)

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2769538A (en) * 1952-10-30 1956-11-06 Reerink Wilhelm Process for froth flotation dressing
WO2000009268A1 (en) * 1998-08-11 2000-02-24 Versitech, Inc. Flotation of sulfide mineral species with oils
US6526675B1 (en) 1999-06-07 2003-03-04 Roe-Hoan Yoon Methods of using natural products as dewatering aids for fine particles
US20030146134A1 (en) * 2000-05-16 2003-08-07 Roe-Hoan Yoon Methodsof increasing flotation rate
US6827220B1 (en) 1998-08-11 2004-12-07 Versitech, Inc. Flotation of sulfide mineral species with oils
US6855260B1 (en) 1999-06-07 2005-02-15 Roe-Hoan Yoon Methods of enhancing fine particle dewatering
US20060251566A1 (en) * 2005-02-04 2006-11-09 Yoon Roe H Separation of diamond from gangue minerals

Cited By (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2769538A (en) * 1952-10-30 1956-11-06 Reerink Wilhelm Process for froth flotation dressing
US20060000753A1 (en) * 1998-08-11 2006-01-05 Young Tom L Flotation of sulfide mineral species with oils
WO2000009268A1 (en) * 1998-08-11 2000-02-24 Versitech, Inc. Flotation of sulfide mineral species with oils
AU761765B2 (en) * 1998-08-11 2003-06-12 Versitech, Inc. Flotation of sulfide mineral species with oils
US7461745B2 (en) 1998-08-11 2008-12-09 Nalco Company Flotation of sulfide mineral species with oils
US6827220B1 (en) 1998-08-11 2004-12-07 Versitech, Inc. Flotation of sulfide mineral species with oils
US6526675B1 (en) 1999-06-07 2003-03-04 Roe-Hoan Yoon Methods of using natural products as dewatering aids for fine particles
US7820058B2 (en) 1999-06-07 2010-10-26 Mineral And Coal Technologies, Inc. Methods of enhancing fine particle dewatering
US6855260B1 (en) 1999-06-07 2005-02-15 Roe-Hoan Yoon Methods of enhancing fine particle dewatering
US20050139551A1 (en) * 1999-06-07 2005-06-30 Roe-Hoan Yoon Methods of enhancing fine particle dewatering
US20080053914A1 (en) * 1999-06-07 2008-03-06 Yoon Roe H Methods of Enhancing Fine Particle Dewatering
US6871743B2 (en) 2000-05-16 2005-03-29 Mineral And Coal Technologies, Inc. Methods of increasing flotation rate
US20050167340A1 (en) * 2000-05-16 2005-08-04 Roe-Hoan Yoon Methods of increasing flotation rate
US6799682B1 (en) 2000-05-16 2004-10-05 Roe-Hoan Yoon Method of increasing flotation rate
US20030146134A1 (en) * 2000-05-16 2003-08-07 Roe-Hoan Yoon Methodsof increasing flotation rate
US20060251566A1 (en) * 2005-02-04 2006-11-09 Yoon Roe H Separation of diamond from gangue minerals
US8007754B2 (en) 2005-02-04 2011-08-30 Mineral And Coal Technologies, Inc. Separation of diamond from gangue minerals

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