TWI859454B - 混成氣凝膠及其製造方法、以及使用混成氣凝膠之斷熱材 - Google Patents

混成氣凝膠及其製造方法、以及使用混成氣凝膠之斷熱材 Download PDF

Info

Publication number
TWI859454B
TWI859454B TW110123474A TW110123474A TWI859454B TW I859454 B TWI859454 B TW I859454B TW 110123474 A TW110123474 A TW 110123474A TW 110123474 A TW110123474 A TW 110123474A TW I859454 B TWI859454 B TW I859454B
Authority
TW
Taiwan
Prior art keywords
aerogel
hollow particles
hollow
particles
weight
Prior art date
Application number
TW110123474A
Other languages
English (en)
Chinese (zh)
Other versions
TW202227361A (zh
Inventor
則慶 呉
李官益
雷蒙 V 里斐拉 維圖達佐
Original Assignee
國立研究開發法人物質 材料研究機構
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 國立研究開發法人物質 材料研究機構 filed Critical 國立研究開發法人物質 材料研究機構
Publication of TW202227361A publication Critical patent/TW202227361A/zh
Application granted granted Critical
Publication of TWI859454B publication Critical patent/TWI859454B/zh

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/157After-treatment of gels
    • C01B33/158Purification; Drying; Dehydrating
    • C01B33/1585Dehydration into aerogels
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/0091Preparation of aerogels, e.g. xerogels
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B30/00Compositions for artificial stone, not containing binders
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/0045Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by a process involving the formation of a sol or a gel, e.g. sol-gel or precipitation processes
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/30Particle morphology extending in three dimensions
    • C01P2004/32Spheres
    • C01P2004/34Spheres hollow
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/64Nanometer sized, i.e. from 1-100 nanometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/16Pore diameter
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16LPIPES; JOINTS OR FITTINGS FOR PIPES; SUPPORTS FOR PIPES, CABLES OR PROTECTIVE TUBING; MEANS FOR THERMAL INSULATION IN GENERAL
    • F16L59/00Thermal insulation in general
    • F16L59/06Arrangements using an air layer or vacuum

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Silicon Compounds (AREA)
  • Thermal Insulation (AREA)
TW110123474A 2020-07-14 2021-06-28 混成氣凝膠及其製造方法、以及使用混成氣凝膠之斷熱材 TWI859454B (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2020120921 2020-07-14
JP2020-120921 2020-07-14

Publications (2)

Publication Number Publication Date
TW202227361A TW202227361A (zh) 2022-07-16
TWI859454B true TWI859454B (zh) 2024-10-21

Family

ID=79555175

Family Applications (1)

Application Number Title Priority Date Filing Date
TW110123474A TWI859454B (zh) 2020-07-14 2021-06-28 混成氣凝膠及其製造方法、以及使用混成氣凝膠之斷熱材

Country Status (6)

Country Link
US (1) US20230150825A1 (https=)
EP (1) EP4183744A4 (https=)
JP (1) JP7477911B2 (https=)
CN (1) CN115997083A (https=)
TW (1) TWI859454B (https=)
WO (1) WO2022014194A1 (https=)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7603924B2 (ja) * 2020-11-20 2024-12-23 国立研究開発法人物質・材料研究機構 断熱配管
JP7607955B2 (ja) * 2020-11-20 2025-01-06 国立研究開発法人物質・材料研究機構 エアロゲル粉末の製造方法及びこれを用いた断熱材
CN113526912B (zh) * 2021-07-01 2023-02-17 中广核研究院有限公司 稀土基气凝胶复合材料及其制备方法和应用

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW201711962A (zh) * 2015-08-28 2017-04-01 Hitachi Chemical Co Ltd 氣凝膠複合體及絕熱材

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH587979A5 (https=) * 1976-02-06 1977-05-31 Sulzer Ag
GB2048847B (en) * 1978-08-28 1983-07-06 Torobin Leonard B Method and apparatus for producing hollow microspheres
AUPR554501A0 (en) * 2001-06-07 2001-07-12 Lehmann Pacific Solar Pty Limited Radiative cooling surface coatings
US20040077738A1 (en) 2002-05-15 2004-04-22 Cabot Corporation Aerogel and hollow particle binder composition, insulation composite, and method for preparing the same
CN1329333C (zh) * 2004-11-29 2007-08-01 北京科技大学 一种硅酸钙复合纳米孔超级绝热材料的制备方法
JP5615514B2 (ja) 2008-05-15 2014-10-29 ニチアス株式会社 断熱材、これを用いた断熱構造及び断熱材の製造方法
US9650500B2 (en) * 2010-11-15 2017-05-16 Dow Global Technologies Llc Nanoporous particles in a hollow latex matrix
US20140059971A1 (en) * 2011-03-18 2014-03-06 Bjørn Petter Jelle Thermal insulation materials
CN105110339A (zh) * 2015-06-23 2015-12-02 北京建工新型建材有限责任公司 一种低成本柔性二氧化硅气凝胶的制备方法
US10422573B2 (en) 2015-12-08 2019-09-24 Whirlpool Corporation Insulation structure for an appliance having a uniformly mixed multi-component insulation material, and a method for even distribution of material combinations therein
CN108778996A (zh) * 2016-03-25 2018-11-09 日立化成株式会社 溶胶组合物、气凝胶复合体、带有气凝胶复合体的支撑构件和绝热材
JP2018130933A (ja) 2017-02-17 2018-08-23 日立化成株式会社 積層複合体及び断熱材
JP6932572B2 (ja) 2017-07-13 2021-09-08 株式会社トクヤマ 球状シリカエアロゲル、その製造方法、及び、その用途
CN108689680A (zh) * 2018-05-30 2018-10-23 巩义市泛锐熠辉复合材料有限公司 一种高效隔热保温气凝胶毡的制备方法

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW201711962A (zh) * 2015-08-28 2017-04-01 Hitachi Chemical Co Ltd 氣凝膠複合體及絕熱材

Also Published As

Publication number Publication date
US20230150825A1 (en) 2023-05-18
CN115997083A (zh) 2023-04-21
JPWO2022014194A1 (https=) 2022-01-20
TW202227361A (zh) 2022-07-16
WO2022014194A1 (ja) 2022-01-20
EP4183744A4 (en) 2025-06-18
EP4183744A1 (en) 2023-05-24
JP7477911B2 (ja) 2024-05-02

Similar Documents

Publication Publication Date Title
TWI859454B (zh) 混成氣凝膠及其製造方法、以及使用混成氣凝膠之斷熱材
Li et al. Synthesis of stable hollow silica microspheres with mesoporous shell in nonionic W/O emulsion
TWI531534B (zh) 金屬氧化物粉末及其製造方法
CN113795472B (zh) 陶瓷泡沫、其制造方法及其用途
JP4994360B2 (ja) アルコキシシラン基で修飾したシリカ/ラテックスハイブリッドからなるモノリシックキセロゲル及びエーロゲルの臨界未満の条件下における製造方法。
CN104587922B (zh) 一种二氧化钛二氧化硅复合纳米多孔微球的制备方法
JP6405540B2 (ja) エアロゲルとその製造方法
US9663376B2 (en) Xerogel production method
JP7616081B2 (ja) 塗液の製造方法及び断熱材の製造方法
TWI871475B (zh) 氣凝膠粉末之製造方法及使用其之斷熱材
JP2010047710A (ja) 柔軟性、成形性を有する発泡ポリマー−シリカ複合体およびそれを用いた断熱材料
US10494265B2 (en) Method for producing silica aerogel and silica aerogel produced thereby
KR102656798B1 (ko) 코어-쉘 구조 에어로겔 함유 초단열성 도료조성물 및 그 제조방법
KR101889474B1 (ko) 실리카 기공 구조체 및 그 제조 방법
JP7259857B2 (ja) 塗液の製造方法、塗液及び塗膜
JP2003267719A (ja) 多孔体、多孔体膜を有する基体およびこれらの製造方法
CN117004267A (zh) 二氧化硅气凝胶接枝二氧化钛纳米点分散体及其制备方法和应用
JP4912190B2 (ja) 多孔質シリカゲル及びシリカガラスの製造方法
KR102025607B1 (ko) 소수성 구형 은나노 실리카 에어로겔 과립의 제조방법
CN115650245A (zh) 一种无表面活性剂微乳液体系硅气凝胶及其制备方法
KR102152214B1 (ko) 판상형 금속-실리카 복합 에어로겔의 제조방법 및 이에 의해 제조된 판상형 금속-실리카 복합 에어로겔
US20050095416A1 (en) Inorganic porous materials containing dispersed particles
WO2025087701A1 (en) Process for producing a porous silica material and its uses
Virtudazo et al. Development of Eco-Friendly Techniques for Preparation of Porous Nano-/Micro-Size Hollow Silicate Particles
Zhang et al. Sonochemical synthesis and liquid crystal assembly of PS-b-PEO–titania aggregates