TWI410520B - Chemical vapor deposition apparatus - Google Patents

Chemical vapor deposition apparatus Download PDF

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Publication number
TWI410520B
TWI410520B TW097142786A TW97142786A TWI410520B TW I410520 B TWI410520 B TW I410520B TW 097142786 A TW097142786 A TW 097142786A TW 97142786 A TW97142786 A TW 97142786A TW I410520 B TWI410520 B TW I410520B
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Taiwan
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gas
reaction
susceptor
chemical vapor
vapor deposition
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TW097142786A
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Chinese (zh)
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TW200930835A (en
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Changsung Sean Kim
Sang Duk Yoo
Jong Pa Hong
Ji Hye Shim
Won Shin Lee
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Samsung Electronics Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/455Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/02104Forming layers
    • H01L21/02365Forming inorganic semiconducting materials on a substrate
    • H01L21/02612Formation types
    • H01L21/02617Deposition types
    • H01L21/0262Reduction or decomposition of gaseous compounds, e.g. CVD
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/67Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere
    • H01L21/67005Apparatus not specifically provided for elsewhere
    • H01L21/67011Apparatus for manufacture or treatment
    • H01L21/67155Apparatus for manufacturing or treating in a plurality of work-stations
    • H01L21/67207Apparatus for manufacturing or treating in a plurality of work-stations comprising a chamber adapted to a particular process
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/67Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere
    • H01L21/683Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere for supporting or gripping
    • H01L21/687Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere for supporting or gripping using mechanical means, e.g. chucks, clamps or pinches
    • H01L21/68714Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere for supporting or gripping using mechanical means, e.g. chucks, clamps or pinches the wafers being placed on a susceptor, stage or support

Abstract

Provided is a chemical vapor deposition apparatus. The apparatus includes a reaction chamber, a gas introduction unit, and a gas exhaust unit. The reaction chamber includes a susceptor on which a wafer is loaded and a reaction furnace in which the wafer is processed by chemical vapor deposition. The gas introduction unit is disposed at an outer wall of the reaction chamber to supply reaction gas from an outside of the reaction furnace to a center portion of the reaction furnace. The gas exhaust unit is disposed at a center portion of the reaction chamber to discharge the reaction gas to an upper or lower outside of the reaction chamber after the reaction gas is used for a reaction in the reaction furnace. Therefore, the gas density inside the chamber can be kept at a substantially uniform state even when process pressure is increased for growing a high-temperature deposition layer.

Description

化學氣相沉積裝置Chemical vapor deposition device [相關申請案之交互參照][Reciprocal Reference of Related Applications]

本申請案主張於2007年12月26日向韓國智慧財產局提出之韓國專利申請案第10-2007--0137715號和於2008年9月30日提出之第10-2008-0096306號之優先權,該兩案皆併入於本案中作為參考。The present application claims priority to Korean Patent Application No. 10-2007--0137715 filed on Dec. 26, 2007 to the Korean Intellectual Property Office and No. 10-2008-0096306 filed on September 30, 2008. Both cases are incorporated in this case for reference.

本發明係關於化學氣相沉積裝置,用以藉由向內供應反應氣體而在晶圓的表面上均勻地並穩定地生長沉積層。The present invention relates to a chemical vapor deposition apparatus for uniformly and stably growing a deposited layer on a surface of a wafer by supplying a reaction gas inward.

一般而言,化學氣相沉積(Chemical Vapor Deposition;CVD)係用來於各種基板上生長各種結晶層之重要的方法。CVD較之液體沉積方法在生長高品質結晶層方面具有優勢;然而,相對較低的結晶生長率係CVD之缺點。欲克服此缺點,有多個層(layer)於各週期期間被同時生長在複數個基板上。In general, Chemical Vapor Deposition (CVD) is an important method for growing various crystal layers on various substrates. CVD has advantages over liquid deposition methods in growing high quality crystalline layers; however, relatively low crystal growth rates are disadvantages of CVD. To overcome this disadvantage, a plurality of layers are simultaneously grown on a plurality of substrates during each cycle.

然而,於多個層同時生長於複數個基板上之情況,該等基板應該保持於相同的溫度並暴露於相同的反應氣體流量中,以便維持生長於基板上的多個層之均勻品質。However, where multiple layers are simultaneously grown on a plurality of substrates, the substrates should be maintained at the same temperature and exposed to the same flow of reactant gases in order to maintain a uniform quality of the layers grown on the substrate.

能夠用於上述目的之方法之例子包括:一種使用複數個噴射管(injection tube)創造沿著基板之均勻氣流(gas flow)的方法;繞著旋轉軸放射狀地配置複數個基板並旋轉在相同旋轉軸上之全部基板之方法(繞軌方法);以及個別地旋轉複數個基板之方法(個別旋轉法)。這些在相關領域 中習知之方法可合併或個別被使用。Examples of methods that can be used for the above purposes include: a method of creating a uniform gas flow along a substrate using a plurality of injection tubes; radially arranging a plurality of substrates around the axis of rotation and rotating at the same A method of rotating all the substrates on the shaft (railing method); and a method of individually rotating a plurality of substrates (individual rotation method). These are in related fields The methods known in the art can be combined or used individually.

本發明之態樣提供一種化學氣相沉積裝置,該裝置藉由維持室內之氣體密度於實質均勻狀態並防止甚至當製程壓力於生長高溫沉積層之製程狀況下增加時有密集的蒸汽反應,而得到高品質之氣相沉積。Aspects of the present invention provide a chemical vapor deposition apparatus which maintains a dense vapor reaction by maintaining a gas density in a chamber in a substantially uniform state and preventing an increase in process pressure even under process conditions in which a high temperature deposition layer is grown. High quality vapor deposition is obtained.

依照本發明之態樣,提供化學氣相沉積裝置,包含:反應室,其包含感受器(susceptor)以及反應爐(reaction furnace),該感受器上載放晶圓而該反應爐中係藉由化學氣相沉積進行該晶圓之加工;氣體引入單元,其係配置在該反應室之外壁用以將反應氣體由該反應爐的外側供應至該反應爐之中央部分;以及氣體排放單元,其係配置在該反應室之中央部分用以於該反應氣體被用於該反應爐中的反應之後將該反應氣體排放至該反應室之上方或下方外側。According to an aspect of the present invention, there is provided a chemical vapor deposition apparatus comprising: a reaction chamber comprising a susceptor and a reaction furnace, wherein the susceptor is loaded with a wafer and the reaction furnace is subjected to a chemical vapor phase Depositing processing of the wafer; a gas introduction unit disposed on an outer wall of the reaction chamber for supplying a reaction gas from a outside of the reaction furnace to a central portion of the reaction furnace; and a gas discharge unit configured to The central portion of the reaction chamber is used to discharge the reaction gas to the upper side or the lower side of the reaction chamber after the reaction gas is used in the reaction in the reaction furnace.

該化學氣相沉積裝置可復包含配置在該氣體引入單元和該氣體排放單元之間之流量控制單元,以便造成從該氣體引入單元至該氣體排放單元之均勻氣流。The chemical vapor deposition apparatus may further include a flow control unit disposed between the gas introduction unit and the gas discharge unit to cause a uniform gas flow from the gas introduction unit to the gas discharge unit.

該化學氣相沉積裝置可復包含驅動單元,該驅動單元提供旋轉動力以朝一個方向旋轉該感受器。The chemical vapor deposition apparatus may further include a driving unit that provides rotational power to rotate the susceptor in one direction.

該化學氣相沉積裝置可復包含配置靠近於該感受器之加熱單元用以提供熱至該感受器。The chemical vapor deposition apparatus can include a heating unit disposed adjacent to the susceptor for providing heat to the susceptor.

該流量控制單元可包含:阻障壁構件,其係配置於該 反應爐之外側用以界定該反應室中的反應爐,並將供應自該氣體引入單元之反應氣體引入至該反應爐中同時調整反應氣體之壓力;以及至少一個氣體室,其係配置於該反應室之外壁與該阻障壁構件之間用來儲存供應自該氣體引入單元之反應氣體並透過該阻障壁構件供應該反應氣體。The flow control unit may include: a barrier member disposed on the The outer side of the reaction furnace is used to define a reaction furnace in the reaction chamber, and a reaction gas supplied from the gas introduction unit is introduced into the reaction furnace while adjusting a pressure of the reaction gas; and at least one gas chamber is disposed at the A reaction gas supplied from the gas introduction unit is stored between the outer wall of the reaction chamber and the barrier wall member, and the reaction gas is supplied through the barrier wall member.

當裝設有複數個氣體室時,該化學氣相沉積裝置可復包含至少一個區分構件用以分離該複數個氣體室。When a plurality of gas chambers are installed, the chemical vapor deposition apparatus may further comprise at least one distinguishing member for separating the plurality of gas chambers.

該化學氣相沉積裝置可復包含配置在該反應室中於面對該感受器的那側之旋渦防止單元,以便朝向該氣體引入單元漸漸減少該感受器與該反應室之間之距離。The chemical vapor deposition apparatus may further include a vortex prevention unit disposed in the reaction chamber on a side facing the susceptor to gradually reduce a distance between the susceptor and the reaction chamber toward the gas introduction unit.

該流量控制單元可包含:配置於該反應爐的外側之傾斜阻障壁,該阻障壁係用以界定該反應室內之反應爐,並將供應自該氣體引入單元之反應氣體引入至反應爐中,同時調整該反應氣體之壓力,該傾斜阻障壁係以預定的角度傾斜;以及複數個氣體室,其係配置於該反應室之外壁與該傾斜阻障壁之間,用來儲存供應自該氣體引入單元之反應氣體並透過該傾斜阻障壁供應該反應氣體;以及至少一個區分構件,其係用以分離該等氣體室。The flow control unit may include: a slope blocking barrier disposed on an outer side of the reaction furnace, the barrier wall is configured to define a reaction furnace in the reaction chamber, and introduce a reaction gas supplied from the gas introduction unit into the reaction furnace, Simultaneously adjusting the pressure of the reaction gas, the inclined barrier wall is inclined at a predetermined angle; and a plurality of gas chambers disposed between the outer wall of the reaction chamber and the inclined barrier wall for storing and supplying from the gas a reaction gas of the unit and supplying the reaction gas through the inclined barrier wall; and at least one distinguishing member for separating the gas chambers.

該化學氣相沉積裝置可復包含配置在該反應室中於面對該感受器的那側之旋渦防止單元,以便朝向該氣體引入單元漸漸減少該感受器與該反應室之間之距離。The chemical vapor deposition apparatus may further include a vortex prevention unit disposed in the reaction chamber on a side facing the susceptor to gradually reduce a distance between the susceptor and the reaction chamber toward the gas introduction unit.

該流量控制單元可包含:複數個配置於該反應室中之氣體室;至少一個區分構件,其係用以分離該等氣體室, 而使得該等氣體室具有不同的長度並成階梯狀;以及多個配置於該等氣體室之末端部份之區分阻障壁,該等區分阻障壁用以將供應自該氣體引入單元之反應氣體引入至該反應爐中,同時調整反應氣體之壓力;其中該等氣體室配置於該反應室之外壁與該等區分阻障壁之間用來儲存供應自該氣體引入單元之反應氣體並透過該等區分阻障壁供應該反應氣體。The flow control unit may include: a plurality of gas chambers disposed in the reaction chamber; at least one distinguishing member for separating the gas chambers, And the gas chambers have different lengths and are stepped; and a plurality of different barrier walls disposed at end portions of the gas chambers for separating the reaction gases supplied from the gas introduction unit Introduced into the reaction furnace while adjusting the pressure of the reaction gas; wherein the gas chambers are disposed between the outer wall of the reaction chamber and the different barrier walls for storing and passing the reaction gas supplied from the gas introduction unit The barrier wall is supplied to the reaction gas.

該化學氣相沉積裝置可復包含配置在該反應室中於面對該感受器的那側之旋渦防止單元,以便朝向該氣體引入單元漸漸減少該感受器與該反應室之間之距離。The chemical vapor deposition apparatus may further include a vortex prevention unit disposed in the reaction chamber on a side facing the susceptor to gradually reduce a distance between the susceptor and the reaction chamber toward the gas introduction unit.

該化學氣相沉積裝置可復包含複數個於實質水平方向上配置於該等區分阻障壁上之平行導引構件用來導引反應氣體之流動。The chemical vapor deposition apparatus may further include a plurality of parallel guiding members disposed on the different barrier walls in a substantially horizontal direction for guiding the flow of the reaction gas.

氣體引入單元可包含複數個與該等氣體室連通之氣體供應線用來將不同的氣體供應至該等氣體室。The gas introduction unit may include a plurality of gas supply lines in communication with the gas chambers for supplying different gases to the gas chambers.

該驅動單元可包含:形成在該感受器之外表面之從動齒輪;與該從動齒輪嚙合之主動齒輪;以及配置在旋轉該主動齒輪的驅動軸之末端之旋轉馬達以提供旋轉動力。The driving unit may include: a driven gear formed on an outer surface of the susceptor; a driving gear meshed with the driven gear; and a rotary motor disposed at an end of a driving shaft that rotates the driving gear to provide rotational power.

該化學氣相沉積裝置可復包含配置在該感受器之中央部分用來旋轉該感受器之軸,該軸包含位於該軸中之氣體排放單元,其中該驅動單元包含:配置在該感受器之從動齒輪;與該從動齒輪嚙合之主動齒輪;以及配置在旋轉該主動齒輪之驅動軸之末端之旋轉馬達。The chemical vapor deposition apparatus may further include a shaft disposed at a central portion of the susceptor for rotating the susceptor, the shaft including a gas discharge unit located in the shaft, wherein the drive unit includes: a driven gear disposed on the susceptor a driving gear meshed with the driven gear; and a rotary motor disposed at an end of the driving shaft that rotates the driving gear.

氣體排放單元可包含:形成於該反應室之內頂部或該感受器之中央部分之排氣孔;以及與該排氣孔連通之排氣線。The gas discharge unit may include: a vent hole formed at a top portion of the reaction chamber or a central portion of the susceptor; and an exhaust line communicating with the vent hole.

現將參照所附圖式詳細說明本發明之示範實施例。Exemplary embodiments of the present invention will now be described in detail with reference to the accompanying drawings.

本發明之化學氣相沉積裝置可應用於任何用以利用化學反應來沉積薄層(膜)於目標物(如晶圓)上之化學氣相沉積裝置。The chemical vapor deposition apparatus of the present invention can be applied to any chemical vapor deposition apparatus for depositing a thin layer (film) on a target (e.g., a wafer) by a chemical reaction.

第1圖為顯示依照本發明之實施例的化學氣相沉積裝置之透示圖,而第2圖為顯示第1圖之化學氣相沉積裝置之側剖面圖。1 is a perspective view showing a chemical vapor deposition apparatus according to an embodiment of the present invention, and FIG. 2 is a side sectional view showing a chemical vapor deposition apparatus of FIG. 1.

如第1和2圖中所顯示,現行實施例之化學氣相沉積裝置包含反應室10、驅動單元20、加熱單元30、氣體引入單元40、氣體排放單元50以及流量控制單元60。As shown in FIGS. 1 and 2, the chemical vapor deposition apparatus of the present embodiment includes a reaction chamber 10, a driving unit 20, a heating unit 30, a gas introduction unit 40, a gas discharge unit 50, and a flow rate control unit 60.

反應室10包含具有如反應爐1的預定尺寸之內部空間,於此反應爐1中化學氣相反應發生於所引入之反應氣體與沉積目標物(如晶圓)之間,而絕緣材料可以配置在反應爐1之內部用來保護反應爐1免於熱空氣的傷害。The reaction chamber 10 includes an internal space having a predetermined size as the reaction furnace 1, in which a chemical vapor reaction occurs between the introduced reaction gas and a deposition target (such as a wafer), and the insulating material can be configured. The inside of the reaction furnace 1 is used to protect the reaction furnace 1 from the damage of hot air.

感受器14配置在反應室10之內部,有複數個容裝器(pocket)15形成於感受器14中用來容裝複數個晶圓2。也就是說,感受器14配置在反應爐1中。The susceptor 14 is disposed inside the reaction chamber 10, and a plurality of pockets 15 are formed in the susceptor 14 for accommodating a plurality of wafers 2. That is, the susceptor 14 is disposed in the reaction furnace 1.

如第2圖中所示,感受器14具有小於反應室10之外徑之外徑。感受器14係由如石墨之材料所形成,並具有碟 形。耦接至反應室10之中央部分之軸16可由具有排氣孔51之中空管構件所形成。排氣孔51形成氣體排放通道(gas exhaust passage)。As shown in FIG. 2, the susceptor 14 has an outer diameter smaller than the outer diameter of the reaction chamber 10. The susceptor 14 is formed of a material such as graphite and has a dish shape. The shaft 16 coupled to the central portion of the reaction chamber 10 may be formed of a hollow tubular member having a venting opening 51. The vent hole 51 forms a gas exhaust passage.

驅動單元20提供旋轉動力,而使得裝載有複數個晶圓2於其上之感受器14能夠朝一個方向上持續地旋轉。The drive unit 20 provides rotational power such that the susceptor 14 on which the plurality of wafers 2 are loaded can be continuously rotated in one direction.

如第2圖中所示,驅動單元20包含:從動齒輪21,其係位於感受器14之外底表面如同整體部分或分離結構;以及與該從動齒輪21嚙合之主動齒輪22。該主動齒輪22耦接至旋轉馬達24之驅動軸23之末端,該旋轉馬達24反應於所施加的電力而產生旋轉力。As shown in FIG. 2, the drive unit 20 includes a driven gear 21 which is located on the outer surface of the susceptor 14 as an integral part or a separate structure; and a drive gear 22 that meshes with the driven gear 21. The drive gear 22 is coupled to the end of the drive shaft 23 of the rotary motor 24, which generates a rotational force in response to the applied electric power.

於第4圖中所示之另一實施例中,驅動單元20可以包含:耦接至軸16作為整體部分或分離結構之從動齒輪21a;以及與該從動齒輪21a嚙合之主動齒輪22a。該軸16可以於垂直方向上從感受器14之底部向下延伸。主動齒輪22a可以耦接至旋轉馬達24a之驅動軸23a之末端,該旋轉馬達24a反應於所施加的電力而產生旋轉力。In another embodiment shown in FIG. 4, the driving unit 20 may include: a driven gear 21a coupled to the shaft 16 as an integral portion or a separate structure; and a driving gear 22a meshing with the driven gear 21a. The shaft 16 can extend downward from the bottom of the susceptor 14 in a vertical direction. The drive gear 22a may be coupled to the end of the drive shaft 23a of the rotary motor 24a, which generates a rotational force in response to the applied electric power.

由於此結構,當旋轉馬達24或24a運作時,裝載有晶圓2於其上之感受器14能夠藉由嚙合之主動齒輪22(22a)以及從動齒輪21(21a)以大約5rpm至大約50rpm之固定速度朝一個方向旋轉。Due to this configuration, when the rotary motor 24 or 24a is operated, the susceptor 14 on which the wafer 2 is loaded can be driven by the driving gear 22 (22a) and the driven gear 21 (21a) by about 5 rpm to about 50 rpm. The fixed speed rotates in one direction.

加熱單元30配置靠近於加熱元件14之底部,該加熱元件14上裝載有晶圓2並且朝向感受器14輻射熱能用來間接加熱晶圓2。The heating unit 30 is disposed adjacent to the bottom of the heating element 14, which is loaded with the wafer 2 and radiates thermal energy toward the susceptor 14 for indirectly heating the wafer 2.

加熱單元30可以是電子加熱器、高頻感應加熱器、紅外線輻射加熱器以及雷射加熱器其中一種。The heating unit 30 may be one of an electronic heater, a high frequency induction heater, an infrared radiant heater, and a laser heater.

溫度感測器(未顯示)可以配置在反應室10內部接近感受器14的外表面或加熱單元30的位置以偵測反應室10之內部溫度用來調整加熱溫度。A temperature sensor (not shown) may be disposed within the reaction chamber 10 proximate the outer surface of the susceptor 14 or the location of the heating unit 30 to detect the internal temperature of the reaction chamber 10 for adjusting the heating temperature.

氣體引入單元40配置在反應室10之外壁18以將氣體供應至反應室10用來產生自反應室10之外壁流向反應室10之內部中央的氣流。The gas introduction unit 40 is disposed at the outer wall 18 of the reaction chamber 10 to supply gas to the reaction chamber 10 for generating a gas flow from the outer wall of the reaction chamber 10 to the inner center of the reaction chamber 10.

氣體引入單元40包含第一至第三氣體引入單元41、42以及43用來供應不同的氣體。例如,第一反應氣體可以透過第一氣體引入單元41被供應,而第二反應氣體可以透過第二和第三氣體引入單元42和43被供應。The gas introduction unit 40 includes first to third gas introduction units 41, 42 and 43 for supplying different gases. For example, the first reaction gas may be supplied through the first gas introduction unit 41, and the second reaction gas may be supplied through the second and third gas introduction units 42 and 43.

第一和第二反應氣體可為不同或者具有共同的成分。或者,相同的氣體可透過第一至第三氣體引入單元41、42以及43被供應,又或者三種氣體皆可分別透過第一至第三氣體引入單元41、42以及43被供應。各種反應氣體皆可根據待形成於目標物上之沉積層而改變。The first and second reactive gases may be different or have a common composition. Alternatively, the same gas may be supplied through the first to third gas introduction units 41, 42 and 43, or three gases may be supplied through the first to third gas introduction units 41, 42 and 43, respectively. Various reaction gases may vary depending on the deposited layer to be formed on the target.

氣體排放單元50配置在反應室10之中央部分用以在氣體用於在晶圓2之表面上生長層之後將氣體(廢氣)排放至反應室10之上方或下方外側,同時從外側將氣體供應至反應爐1的內部中央。The gas discharge unit 50 is disposed at a central portion of the reaction chamber 10 for discharging a gas (exhaust gas) to the outside or below the reaction chamber 10 after the gas is used to grow a layer on the surface of the wafer 2, while supplying gas from the outside. It is to the center of the inside of the reaction furnace 1.

如第1和2圖中所顯示,氣體排放單元50係組構以透過反應室10之底部中央部分排放反應氣體。因此,氣體排 放單元50可以包含:排氣孔51,其形成於耦接至感受器14之旋轉中央的軸16中;以及配置在排氣孔51之下方末端的排氣線52。As shown in FIGS. 1 and 2, the gas discharge unit 50 is configured to discharge the reaction gas through the central portion of the bottom of the reaction chamber 10. Therefore, the gas row The discharge unit 50 may include an exhaust hole 51 formed in the shaft 16 coupled to the center of rotation of the susceptor 14 and an exhaust line 52 disposed at a lower end of the vent hole 51.

於第3和4圖中所示之另一實施例中,氣體排放單元50可以包含:穿過反應室10之頂部中央部分而形成之排氣孔51a以及連接至排氣孔51a之排氣線52a。In another embodiment shown in FIGS. 3 and 4, the gas discharge unit 50 may include: a vent hole 51a formed through a central portion of the top of the reaction chamber 10, and a vent line connected to the vent hole 51a. 52a.

因此,當自反應爐1的外側供應(亦即,經由外壁18供應)之反應氣體流向反應室10之中央時,反應氣體與晶圓2之上表面(沉積表面)進行反應以生長層於晶圓2之表面上。其後,反應氣體(廢氣)經由配置於感受器14之底側之軸16之排氣孔51排放至反應室10之下方外側,或經由配置在反應室10之頂側之排氣孔51a排放至反應室10之上方外側。Therefore, when the reaction gas supplied from the outside of the reaction furnace 1 (that is, supplied via the outer wall 18) flows toward the center of the reaction chamber 10, the reaction gas reacts with the upper surface (deposition surface) of the wafer 2 to grow a layer on the crystal. On the surface of the circle 2. Thereafter, the reaction gas (exhaust gas) is discharged to the outside of the lower side of the reaction chamber 10 via the exhaust hole 51 of the shaft 16 disposed on the bottom side of the susceptor 14, or discharged to the exhaust hole 51a disposed on the top side of the reaction chamber 10 to the lower side. The outer side of the reaction chamber 10 is above.

流量控制單元60係用來產生從氣體引入單元40流至氣體排放單元50之均勻氣流。如第2圖和第4圖中所顯示,流量控制單元60包含氣體室和阻障壁構件61。The flow control unit 60 is for generating a uniform gas flow from the gas introduction unit 40 to the gas discharge unit 50. As shown in FIGS. 2 and 4, the flow control unit 60 includes a gas chamber and a barrier member 61.

氣體室具有預定的尺寸並形成在反應室10之外壁18和阻障壁構件61之間。氣體室與氣體引入單元40連通以暫時儲存反應氣體並經由阻障壁構件61將反應氣體供應至反應爐1。The gas chamber has a predetermined size and is formed between the outer wall 18 of the reaction chamber 10 and the barrier member 61. The gas chamber is in communication with the gas introduction unit 40 to temporarily store the reaction gas and supply the reaction gas to the reaction furnace 1 via the barrier wall member 61.

如第2圖和第4圖中所示,可以裝設一個氣體室或複數個氣體室。As shown in Figures 2 and 4, a gas chamber or a plurality of gas chambers may be provided.

如第2和4圖中所示,化學氣相沉積裝置可以包含第 一氣體室11、第二氣體室12以及第三氣體室13,其中第一氣體室11、第二氣體室12以及第三氣體室13分別與第一氣體引入單元41、第二氣體引入單元42以及第三氣體引入單元43連通。As shown in Figures 2 and 4, the chemical vapor deposition apparatus may comprise a gas chamber 11, a second gas chamber 12, and a third gas chamber 13, wherein the first gas chamber 11, the second gas chamber 12, and the third gas chamber 13 are respectively coupled to the first gas introduction unit 41 and the second gas introduction unit 42 And the third gas introduction unit 43 is in communication.

阻障壁構件61係朝向該反應室10之中央被垂直地配置並與反應室10之外壁18(最外側)間隔(spaced from)一段預定距離。因此,阻障壁構件61係由多個圓柱狀構件所組構而成,該等圓柱狀構件係持續沿著反應室10之外壁18之周圍並且以一段遠離該外壁18之預定距離被配置。The barrier member 61 is vertically disposed toward the center of the reaction chamber 10 and spaced apart from the outer wall 18 (outermost side) of the reaction chamber 10 by a predetermined distance. Accordingly, the barrier member 61 is constructed from a plurality of cylindrical members that are continuously disposed around the outer wall 18 of the reaction chamber 10 and are disposed at a predetermined distance away from the outer wall 18.

阻障壁構件61可以由多孔主體(porous body)所形成,其中供應自氣體引入單元40之反應氣體可自由地流經該多孔主體。The barrier rib member 61 may be formed of a porous body in which a reaction gas supplied from the gas introduction unit 40 is free to flow through the porous body.

複數個氣體室11、12以及13可以藉由區分構件64a、64b被分離。The plurality of gas chambers 11, 12, and 13 can be separated by the distinguishing members 64a, 64b.

如第5圖中所示,當反應氣體從外側流至反應室10之內部中央時,能夠於反應室10之周圍側觀察到非均勻氣流,該反應氣體透過該反應室10而被引入。As shown in Fig. 5, when the reaction gas flows from the outside to the inner center of the reaction chamber 10, a non-uniform gas flow can be observed on the peripheral side of the reaction chamber 10, and the reaction gas is introduced through the reaction chamber 10.

當感受器14裝載晶圓2並且藉由加熱單元30被加熱至高溫時,非均勻氣流可能由感受器14之頂部表面與反應室10之天花板之間之熱對流所引起。When the susceptor 14 is loaded with the wafer 2 and heated to a high temperature by the heating unit 30, the non-uniform gas flow may be caused by thermal convection between the top surface of the susceptor 14 and the ceiling of the reaction chamber 10.

由於熱對流,反應氣體的氣流會受到向上之浮力,而因此反應氣流之速度從反應室10之外側向中央漸漸增加。也就是說,反應氣體之速度於反應室10之周圍側較反 應室10之中央為慢,而因此產生如旋渦之不均勻氣流,進而在晶圓2之沉積表面造成不穩定之反應以及生長在晶圓2上之不穩定之層。Due to the heat convection, the flow of the reaction gas is subjected to upward buoyancy, and thus the velocity of the reaction gas flow gradually increases from the outer side to the center of the reaction chamber 10. That is, the velocity of the reaction gas is relatively reversed on the peripheral side of the reaction chamber 10. The center of the chamber 10 is slow, thereby producing an uneven flow of air such as a vortex, which in turn causes an unstable reaction on the deposition surface of the wafer 2 and an unstable layer grown on the wafer 2.

因此,為使旋渦之產生降至最小或甚至去除產生旋渦之可能性,旋渦防止單元70可以藉由朝向氣體引入單元40漸漸減少感受器14與反應室10之間的距離之方式來配置在反應室10中於面對感受器14之表面,如第6和7圖中所示。Therefore, in order to minimize the occurrence of vortices or even to remove the possibility of generating vortices, the vortex prevention unit 70 can be disposed in the reaction chamber by gradually reducing the distance between the susceptor 14 and the reaction chamber 10 toward the gas introduction unit 40. 10 is in the surface facing the susceptor 14, as shown in Figures 6 and 7.

旋渦防止單元70可以藉由朝向感受器14突出反應室10之內天花板,或者藉由以可拆卸之方式將具有低熱傳導係數之材料(如石英)附接至反應室10之內天花板而形成。The vortex prevention unit 70 may be formed by projecting the ceiling inside the reaction chamber 10 toward the susceptor 14, or by attaching a material having a low heat transfer coefficient such as quartz to the ceiling inside the reaction chamber 10 in a detachable manner.

如第6圖中所示,面對感受器14之旋渦防止單元70之外表面可以包含與感受器14之頂部表面平行之水平表面71,以及與感受器14之頂部表面呈預定角度之傾斜表面72。於第7圖中所示之另一實施例中,旋渦防止單元70可以包含具有預定曲率(curvature)之曲面(curved surface)73。As shown in Fig. 6, the outer surface of the vortex prevention unit 70 facing the susceptor 14 may include a horizontal surface 71 parallel to the top surface of the susceptor 14, and an inclined surface 72 at a predetermined angle to the top surface of the susceptor 14. In another embodiment shown in FIG. 7, the vortex prevention unit 70 may include a curved surface 73 having a predetermined curvature.

於第6圖和第7圖中,參考編號44表示第一氣體引入單元41之氣體引入孔(參照第1圖);參考編號45表示第二氣體引入單元42之氣體引入孔(參照第1圖);和參考編號46表示第三氣體引入單元43之氣體引入孔(參照第1圖)。In FIGS. 6 and 7, reference numeral 44 denotes a gas introduction hole of the first gas introduction unit 41 (refer to FIG. 1); reference numeral 45 denotes a gas introduction hole of the second gas introduction unit 42 (refer to FIG. 1). And reference numeral 46 denotes a gas introduction hole of the third gas introduction unit 43 (refer to Fig. 1).

以相同之方式將氣體引入孔44、45以及46應用到如 第8圖至第11圖中所示之實施例。The gas introduction holes 44, 45, and 46 are applied to the same in the same manner as The embodiment shown in Figures 8 through 11 is shown.

如第8圖和第9圖中所示,流量控制單元60可以包含以預定角度傾斜之傾斜阻障壁62以及區分構件65a與65b,該等區分構件65a、65b被組構以將界定於傾斜阻障壁62與外壁18之間的氣體室區分成為第一至第三氣體室11、12以及13。於此種方式中,流量控制單元60可以具有傾斜的結構。As shown in FIGS. 8 and 9, the flow control unit 60 may include a sloped barrier wall 62 that is inclined at a predetermined angle and distinguishing members 65a, 65b that are configured to be defined by the tilting resistance The gas chamber between the barrier rib 62 and the outer wall 18 is divided into first to third gas chambers 11, 12, and 13. In this manner, the flow control unit 60 can have a slanted configuration.

傾斜阻障壁62向反應室10之中央傾斜並與反應室10之外壁18間隔一段預定的距離。因此,傾斜阻障壁62可以藉由圓柱狀構件所組構而成,該等圓柱狀構件係持續沿著反應室10之外壁18之周圍並且以一段遠離該外壁18之預定距離被配置。The inclined barrier wall 62 is inclined toward the center of the reaction chamber 10 and spaced apart from the outer wall 18 of the reaction chamber 10 by a predetermined distance. Accordingly, the inclined barrier walls 62 may be formed by a cylindrical member that continues along the periphery of the outer wall 18 of the reaction chamber 10 and is disposed at a predetermined distance away from the outer wall 18.

相似於阻障壁構件61,傾斜阻障壁62可以由多孔主體所形成,其中供應自氣體引入單元40之反應氣體能夠自由地流經該多孔主體。Similar to the barrier member 61, the inclined barrier rib 62 may be formed of a porous body through which the reaction gas supplied from the gas introduction unit 40 can freely flow.

由於流量控制單元60包含傾斜阻障壁62以及區分構件65a與65b,所以上方氣體室(例如:氣體室11)較下方氣體室(例如:氣體室13)為長。因此,於反應爐1中,冷反應氣體在反應爐1之上方側中相較於在反應爐1之下方側中能夠進一步流動,於是,能夠抑制熱對流而氣流可被穩定並維持均勻。Since the flow control unit 60 includes the inclined barrier wall 62 and the partition members 65a and 65b, the upper gas chamber (for example, the gas chamber 11) is longer than the lower gas chamber (for example, the gas chamber 13). Therefore, in the reaction furnace 1, the cold reaction gas can flow further in the upper side of the reaction furnace 1 than in the lower side of the reaction furnace 1, so that the heat convection can be suppressed and the gas flow can be stabilized and maintained uniform.

第9圖顯示依照本發明實施例之化學氣相沉積裝置,該裝置包含:如第8圖中所示之傾斜阻障壁62、區分構件 65a與65b以及氣體室11、12以及13;以及如第7圖中所示之旋渦防止單元70。Figure 9 shows a chemical vapor deposition apparatus according to an embodiment of the present invention, the apparatus comprising: a tilt barrier 62 as shown in Fig. 8, a distinguishing member 65a and 65b and gas chambers 11, 12 and 13; and vortex prevention unit 70 as shown in Fig. 7.

藉由以此方式結合流量控制單元60和旋渦防止單元70,反應氣體能夠於反應爐1中更均勻地流動。By combining the flow control unit 60 and the vortex prevention unit 70 in this manner, the reaction gas can flow more uniformly in the reaction furnace 1.

於第10圖和第11圖中所示之另一實施例中,複數個氣體室11、12以及13可以階梯之方式形成於反應爐1之周圍側,而區分阻障壁63a、63b以及63c可以被配置於氣體室11、12以及13之末端以便形成多階的流量控制單元(multi-stepped flow control unit)60。In another embodiment shown in FIGS. 10 and 11, a plurality of gas chambers 11, 12, and 13 may be formed in a stepwise manner on the peripheral side of the reaction furnace 1, and the barrier walls 63a, 63b, and 63c may be different. The ends of the gas chambers 11, 12, and 13 are disposed to form a multi-stepped flow control unit 60.

換言之,第10圖之化學氣相沉積裝置之流量控制單元60包含第一氣體室11、第二氣體室12以及第三氣體室13,該第二氣體室12較該第一氣體室11為短並從該第一氣體室11凹入,該第三氣體室13較該第二氣體室12為短並從該第二氣體室12凹入。In other words, the flow rate control unit 60 of the chemical vapor deposition apparatus of FIG. 10 includes a first gas chamber 11, a second gas chamber 12, and a third gas chamber 13, which is shorter than the first gas chamber 11. And recessed from the first gas chamber 11, the third gas chamber 13 is shorter than the second gas chamber 12 and is recessed from the second gas chamber 12.

此外,第一區分阻障壁63a係配置在面對該反應爐1之內部的第一氣體室11之末端,第二區分阻障壁63b係配置在面對該反應爐1之內部的第二氣體室12之末端,而第三區分阻障壁63c係配置在面對該反應爐1之內部的第三氣體室13之末端。Further, the first different barrier wall 63a is disposed at the end of the first gas chamber 11 facing the inside of the reaction furnace 1, and the second different barrier wall 63b is disposed at the second gas chamber facing the inside of the reaction furnace 1. The end of the third partitioning wall 63c is disposed at the end of the third gas chamber 13 facing the inside of the reaction furnace 1.

氣體室11、12以及13係由區分構件66a和66b所分離。The gas chambers 11, 12, and 13 are separated by the division members 66a and 66b.

由於上述流量控制單元60之多階結構,上方氣體室(例如:氣體室11)較下方氣體室(例如:氣體室13)為長。 因此,於反應爐1中,冷反應氣體在反應爐1之上方側中相較於在反應爐1之下方側中能夠進一步流動,於是,能夠抑制熱對流而氣流可被穩定並維持均勻。Due to the multi-stage structure of the flow control unit 60 described above, the upper gas chamber (for example, the gas chamber 11) is longer than the lower gas chamber (for example, the gas chamber 13). Therefore, in the reaction furnace 1, the cold reaction gas can flow further in the upper side of the reaction furnace 1 than in the lower side of the reaction furnace 1, so that the heat convection can be suppressed and the gas flow can be stabilized and maintained uniform.

第11圖顯示依照本發明實施例之化學氣相沉積裝置,該裝置包含:顯示於第10圖中之區分阻障壁63a、63b以及63c、區分構件66a、66b以及氣體室11、12以及13;以及第7圖中所示之旋渦防止單元70。Figure 11 shows a chemical vapor deposition apparatus according to an embodiment of the present invention, the apparatus comprising: the different barrier walls 63a, 63b and 63c, the partitioning members 66a, 66b and the gas chambers 11, 12 and 13 shown in Figure 10; And the vortex prevention unit 70 shown in Fig. 7.

藉由以此方式結合流量控制單元60與旋渦防止單元70,反應氣體能夠於反應爐1中更均勻地流動。By combining the flow control unit 60 and the vortex prevention unit 70 in this manner, the reaction gas can flow more uniformly in the reaction furnace 1.

第12圖顯示依照本發明之實施例附加於第10圖之流量控制單元之導引構件和循環線(circulation line)。Fig. 12 shows a guiding member and a circulation line attached to the flow control unit of Fig. 10 in accordance with an embodiment of the present invention.

參照第12圖,複數個導引構件67可以在氣體流量方向上各自被配置在區分阻障壁63a、63b以及63c以導引氣流朝向反應爐1之內側。Referring to Fig. 12, a plurality of guiding members 67 may be disposed in the gas flow direction to distinguish the barrier walls 63a, 63b, and 63c to guide the airflow toward the inside of the reaction furnace 1.

因為導引構件67導引氣流達到一預定的長度,因此氣流可為均勻的。當氣流向下時,導引構件67之長度可以減少。Since the guiding member 67 guides the airflow to a predetermined length, the airflow can be uniform. When the airflow is downward, the length of the guiding member 67 can be reduced.

如第12圖中所示,循環線68可以裝設在氣體室11、12以及13之外側,以允許冷卻劑沿著反應室10之外壁18流動用來冷卻反應室10。As shown in Fig. 12, a circulation line 68 may be disposed on the outer sides of the gas chambers 11, 12, and 13 to allow coolant to flow along the outer wall 18 of the reaction chamber 10 for cooling the reaction chamber 10.

阻障壁構件61、傾斜阻障壁62以及區分阻障壁63a、63b以及63c(下文中,稱之為阻障壁)為多孔的而使得反應氣體能夠自由地流經阻障壁。阻障壁可以由具有複數個細 孔(fine hole)之多孔媒介M所形成,如第13A圖中所示。The barrier rib member 61, the inclined barrier rib 62, and the discrimination barrier walls 63a, 63b, and 63c (hereinafter, referred to as a barrier rib) are porous so that the reaction gas can freely flow through the barrier rib. The barrier wall can be composed of a plurality of thin A porous medium M of fine holes is formed as shown in Fig. 13A.

或者,如第13B圖中所示,阻障壁可以由薄板P所形成,該薄板P上形成複數個貫穿該薄板P並具有相同內徑或不同內徑之孔用以允許反應氣體自由流經。Alternatively, as shown in Fig. 13B, the barrier wall may be formed of a thin plate P on which a plurality of holes penetrating the thin plate P and having the same inner diameter or different inner diameters are formed to allow free flow of the reaction gas.

或者,如第13C圖和第13D圖所示,阻障壁可以由薄板P所形成,該薄板P上形成複數個貫穿該薄板P之水平狹縫S1或垂直狹縫S2用以允許反應氣體自由流經。Alternatively, as shown in FIGS. 13C and 13D, the barrier wall may be formed by a thin plate P on which a plurality of horizontal slits S1 or vertical slits S2 penetrating the thin plate P are formed to allow free flow of the reaction gas. through.

或者,如第13E圖中所示,阻障壁可以由垂直桿P1以及水平桿P2所形成並且具有由垂直桿P1與水平桿P2所界定之預定尺寸之間距S,該水平桿P2以直角或預定角度貫穿該水平桿P1。Alternatively, as shown in Fig. 13E, the barrier wall may be formed by the vertical rod P1 and the horizontal rod P2 and have a predetermined size interval S defined by the vertical rod P1 and the horizontal rod P2, the horizontal rod P2 being at a right angle or predetermined The angle runs through the horizontal rod P1.

依照本發明之實施例,可於化學氣相沉積裝置中進行如下之沉積。如晶圓2之沉積標的物係裝載於配置在反應室10之感受器14的容裝器15中。According to an embodiment of the present invention, deposition as follows can be performed in a chemical vapor deposition apparatus. The deposition target such as wafer 2 is loaded in a container 15 disposed in the susceptor 14 of the reaction chamber 10.

於裝載晶圓2後,供應電力至靠近感受器14之加熱單元30,然後加熱單元30朝向感受器14輻射熱能而使得晶圓2被加熱至大約700℃至大約1200℃,而反應室10之內部保持在高溫狀態。After the wafer 2 is loaded, power is supplied to the heating unit 30 near the susceptor 14, and then the heating unit 30 radiates thermal energy toward the susceptor 14 so that the wafer 2 is heated to about 700 ° C to about 1200 ° C while the interior of the reaction chamber 10 is maintained. At high temperatures.

參照第2圖,操作旋轉馬達24以旋轉該主動齒輪,該主動齒輪22與形成在感受器14之從動齒輪21相嚙合。或者,如第4圖中所示,操作旋轉馬達24a以旋轉主動齒輪22a,該主動齒輪22a與裝設在感受器14之軸16之從動齒輪21a相嚙合。以此種方式,感受器14係朝一個方向旋轉。Referring to Fig. 2, the rotary motor 24 is operated to rotate the drive gear, and the drive gear 22 meshes with the driven gear 21 formed on the susceptor 14. Alternatively, as shown in Fig. 4, the rotary motor 24a is operated to rotate the drive gear 22a, which meshes with the driven gear 21a of the shaft 16 of the susceptor 14. In this manner, the susceptor 14 is rotated in one direction.

於此狀態中,反應氣體係透過連接至反應室10之外壁18之氣體引入單元40來供應。如第1圖至第4圖中所示,所供應之反應氣體暫時停留在該氣體室11、12以及13,該等氣體室係界定於反應室10之外壁18以及與外壁18間隔一段預定距離之流量控制單元60之間。然後,反應氣體以層流形式(laminar flow)透過由多孔主體所形成之阻障壁構件61流至反應室10之內部。In this state, the reaction gas system is supplied through the gas introduction unit 40 connected to the outer wall 18 of the reaction chamber 10. As shown in FIGS. 1 to 4, the supplied reaction gas temporarily stays in the gas chambers 11, 12, and 13, which are defined in the outer wall 18 of the reaction chamber 10 and spaced apart from the outer wall 18 by a predetermined distance. Between the flow control units 60. Then, the reaction gas flows into the inside of the reaction chamber 10 through the barrier member 61 formed of the porous body in a laminar flow.

也就是說,當反應氣體之氣流通過控制單元60時,反應氣體之氣流變成層狀而使得反應氣體之層流能夠在反應室10的外側至中央的方向上被形成。That is, when the gas stream of the reaction gas passes through the control unit 60, the gas stream of the reaction gas becomes layered so that the laminar flow of the reaction gas can be formed in the outer to central direction of the reaction chamber 10.

於此時,供應自反應室10之外側之反應氣體會受到由加熱至高溫之感受器14之頂部表面與反應室10之天花板之間之熱對流所引起之向上浮力,並因此反應氣體之氣流將變得不穩定。At this time, the reaction gas supplied from the outside of the reaction chamber 10 is subjected to buoyancy caused by thermal convection between the top surface of the susceptor 14 heated to a high temperature and the ceiling of the reaction chamber 10, and thus the gas flow of the reaction gas will Become unstable.

為防止這種情況,如第6圖和第7圖中所示,本發明之化學氣相沉積裝置包含介於阻障壁構件61與反應室10之天花板之間之旋渦防止單元70,用以朝向氣體引入單元40漸漸減少感受器14與反應室10之間之距離,而使得反應氣體之氣流能夠穩定並保持均勻。To prevent this, as shown in FIGS. 6 and 7, the chemical vapor deposition apparatus of the present invention includes a vortex preventing unit 70 interposed between the barrier member 61 and the ceiling of the reaction chamber 10 for facing The gas introduction unit 40 gradually reduces the distance between the susceptor 14 and the reaction chamber 10, so that the flow of the reaction gas can be stabilized and kept uniform.

如第8和9圖中所示,流量控制單元60可以有傾斜之形狀,或如第10圖和第11圖中所示,流量控制單元60可以有多階之形狀,以便使得冷空氣在反應爐1之上方內側中相較於在反應爐1之下方內側中能夠進一步流動。於此 情況,能夠抑制熱對流,且反應氣體之氣流可以穩定並保持均勻。As shown in Figures 8 and 9, the flow control unit 60 may have a slanted shape, or as shown in Figures 10 and 11, the flow control unit 60 may have a multi-step shape to allow cold air to react. The upper inner side of the furnace 1 can flow further than the lower inner side of the reaction furnace 1. herein In the case, heat convection can be suppressed, and the flow of the reaction gas can be stabilized and kept uniform.

透過配置在反應室10之周圍側之流量控制單元60供應至反應室10之中央部位之反應氣體與晶圓2之頂部表面(沉積表面)發生反應用來藉由化學沉積而均勻地於晶圓2之頂部表面上生長層。其後,將反應氣體(廢氣)連同副產品從反應室10之中央部分透過反應室10之上方或下方側排放至反應室10之外側。The reaction gas supplied to the central portion of the reaction chamber 10 through the flow control unit 60 disposed on the peripheral side of the reaction chamber 10 reacts with the top surface (deposition surface) of the wafer 2 for uniform deposition on the wafer by chemical deposition A layer is grown on the top surface of 2. Thereafter, the reaction gas (exhaust gas) together with the by-product is discharged from the central portion of the reaction chamber 10 through the upper or lower side of the reaction chamber 10 to the outside of the reaction chamber 10.

也就是說,於配置在感受器14之底側之軸16係由具有連接至排氣線52之排氣孔51之中空管所形成之情況下(如第1和2圖中所示),廢氣從反應室10之中央部分透過排氣孔51和排氣線52排放至反應室10之下方外側。That is, in the case where the shaft 16 disposed on the bottom side of the susceptor 14 is formed by a hollow tube having a vent hole 51 connected to the exhaust line 52 (as shown in FIGS. 1 and 2), The exhaust gas is discharged from the central portion of the reaction chamber 10 through the exhaust hole 51 and the exhaust line 52 to the lower side of the reaction chamber 10.

或者,於排氣孔51a形成在反應室10之頂部中央部分並連接至排氣線52a之情況下(如第3和4圖中所示),藉由加熱感受器14至高溫所引起之強烈熱對流而平穩地將廢氣從反應室10之中央部分透過排氣孔51a和排氣線52a排放至反應室10之上方外側。Alternatively, in the case where the vent hole 51a is formed at the top central portion of the reaction chamber 10 and connected to the exhaust line 52a (as shown in FIGS. 3 and 4), the intense heat caused by heating the susceptor 14 to the high temperature is caused. The exhaust gas is convectively and smoothly discharged from the central portion of the reaction chamber 10 through the exhaust hole 51a and the exhaust line 52a to the upper side of the reaction chamber 10.

依照本發明之化學氣相沉積裝置,即便當為了生長高溫沉積層之沉積狀況下而增加製程壓力時,室內之氣體密度仍然能夠保持實質均勻的狀態。According to the chemical vapor deposition apparatus of the present invention, even when the process pressure is increased in order to deposit a deposition state of a high temperature deposition layer, the gas density in the chamber can maintain a substantially uniform state.

此外,透過連接至反應室之外側之氣體引入單元被供應至反應室之周圍側之反應氣體係暫時儲存於流量控制單元中,接著被供應至反應室之中央部分,以便防止或將氣 體引入單元附近由於加熱感受器之表面至高溫所引起之熱對流所產生之旋渦最小化。再者,廢氣能夠從反應室排放至反應室之上方或下方外側。因此,能夠改善氣流之均勻性,並防止在反應室內部發生密集之蒸汽反應。於是,能夠在晶圓上製造均勻生長之高品質沉積層。Further, the reaction gas system supplied to the peripheral side of the reaction chamber through the gas introduction unit connected to the outside of the reaction chamber is temporarily stored in the flow control unit, and then supplied to the central portion of the reaction chamber to prevent or remove gas. The vortex generated by the heat convection caused by the surface of the heating susceptor to the high temperature is minimized in the vicinity of the body introduction unit. Further, the exhaust gas can be discharged from the reaction chamber to the upper side or the lower side of the reaction chamber. Therefore, the uniformity of the gas flow can be improved, and a dense steam reaction inside the reaction chamber can be prevented. Thus, a uniformly grown high quality deposited layer can be fabricated on the wafer.

雖然本發明已針對示範實施例而作了相關之說明,但是對於在此技術領域中具有通常知識者將了解到本發明可作某些修飾和改變而不會偏離如隨附之申請專利範圍所界定之精神與範籌。Although the present invention has been described in connection with the exemplary embodiments, it will be understood by those of ordinary skill in the art Defining the spirit and the standard.

1‧‧‧反應爐1‧‧‧Reaction furnace

2‧‧‧晶圓2‧‧‧ wafer

10‧‧‧反應室10‧‧‧Reaction room

11、12、13‧‧‧氣體室11, 12, 13‧ ‧ gas chamber

14‧‧‧感受器(加熱元件)14‧‧‧ susceptor (heating element)

15‧‧‧容裝器15‧‧‧ Container

16‧‧‧軸16‧‧‧Axis

18‧‧‧外壁18‧‧‧ outer wall

20‧‧‧驅動單元20‧‧‧Drive unit

21、21a‧‧‧從動齒輪21, 21a‧‧‧ driven gear

22、22a‧‧‧主動齒輪22, 22a‧‧‧ drive gear

23、23a‧‧‧驅動軸23, 23a‧‧‧ drive shaft

24、24a‧‧‧旋轉馬達24, 24a‧‧‧Rotary motor

30‧‧‧加熱單元30‧‧‧heating unit

40‧‧‧氣體引入單元40‧‧‧ gas introduction unit

41‧‧‧第一氣體引入單元41‧‧‧First gas introduction unit

42‧‧‧第二氣體引入單元42‧‧‧Second gas introduction unit

43‧‧‧第三氣體引入單元43‧‧‧ Third gas introduction unit

44、45、46‧‧‧氣體引入孔44, 45, 46‧‧‧ gas introduction holes

50‧‧‧氣體排放單元50‧‧‧ gas emission unit

51、51a‧‧‧排氣孔51, 51a‧‧‧ vents

52、52a‧‧‧排氣線52, 52a‧‧‧ exhaust line

60‧‧‧流量控制單元60‧‧‧Flow Control Unit

61‧‧‧阻障壁構件61‧‧‧Resistance wall members

62‧‧‧傾斜阻障壁62‧‧‧Tilting barrier

63a、63b、63c‧‧‧區分阻障壁63a, 63b, 63c‧‧ ‧ distinguish barrier walls

64a、64b‧‧‧區分構件64a, 64b‧‧‧ distinguishing components

65a、65b‧‧‧區分構件65a, 65b‧‧‧ distinguishing components

66a、66b‧‧‧區分構件66a, 66b‧‧‧ distinguishing components

67‧‧‧導引構件67‧‧‧Guide members

68‧‧‧循環線68‧‧‧Circular line

70‧‧‧旋渦防止單元70‧‧‧Vortex prevention unit

71‧‧‧水平表面71‧‧‧ horizontal surface

72‧‧‧傾斜表面72‧‧‧Sloping surface

73‧‧‧曲面73‧‧‧ Surface

M‧‧‧多孔媒介M‧‧‧Porous medium

P‧‧‧薄板P‧‧‧thin sheet

P1‧‧‧垂直桿P1‧‧‧ vertical rod

P2‧‧‧水平桿P2‧‧‧ horizontal pole

S‧‧‧狹縫(間距)S‧‧‧slit (pitch)

S1‧‧‧水平狹縫S1‧‧‧ horizontal slit

S2‧‧‧垂直狹縫S2‧‧‧ vertical slit

由上述之詳細說明結合隨附圖式將更清楚地了解本發明之上述和其他態樣、特徵和其他優點,其中:第1圖為顯示依照本發明之實施例的化學氣相沉積裝置之示意圖;第2圖為顯示第1圖之化學氣相沉積裝置之側剖面圖;第3圖為顯示依照本發明之另一實施例的化學氣相沉積裝置之示意圖;第4圖為顯示第3圖之化學氣相沉積裝置之側剖面圖;第5圖為顯示能夠於本發明之化學氣相沉積裝置之反應室中被產生之旋渦之示意圖;第6圖為顯示依照本發明之實施例包含於化學氣相沉積裝置中之流量控制單元和旋渦防止單元之圖式;第7圖為顯示依照本發明之另一實施例包含於化學氣 相沉積裝置中之流量控制單元和旋渦防止單元之圖式;第8圖為顯示依照本發明之另一實施例包含於化學氣相沉積裝置中之流量控制單元之圖式;第9圖為顯示包含於第7圖之旋渦防止單元和第8圖之流量控制單元之化學氣相沉積裝置;第10圖為顯示依照本發明之再另一實施例包含於化學氣相沉積裝置中之流量控制單元之圖式;第11圖為顯示包含於第7圖之旋渦防止單元和第10圖之流量控制單元之化學氣相沉積裝置;第12圖為顯示依照本發明之實施例附加於第10圖之流量控制單元之多個導引構件和多個循環線之圖式;第13A至13E圖為顯示依照本發明之實施例化學氣相沉積裝置之阻障壁之例子之圖式。The above and other aspects, features, and other advantages of the present invention will be more clearly understood from the aspects of the appended claims. 2 is a side cross-sectional view showing the chemical vapor deposition apparatus of FIG. 1; FIG. 3 is a schematic view showing a chemical vapor deposition apparatus according to another embodiment of the present invention; and FIG. 4 is a view showing FIG. A side cross-sectional view of a chemical vapor deposition apparatus; FIG. 5 is a schematic view showing a vortex that can be generated in a reaction chamber of the chemical vapor deposition apparatus of the present invention; and FIG. 6 is a view showing an embodiment according to the present invention. A schematic diagram of a flow control unit and a vortex prevention unit in a chemical vapor deposition apparatus; and FIG. 7 is a view showing a chemical gas contained in another embodiment according to the present invention. FIG. 8 is a view showing a flow control unit included in a chemical vapor deposition apparatus according to another embodiment of the present invention; FIG. 9 is a view showing a flow control unit and a vortex prevention unit in a phase deposition apparatus; a chemical vapor deposition apparatus comprising the vortex prevention unit of FIG. 7 and the flow control unit of FIG. 8; and FIG. 10 is a flow control unit for inclusion in a chemical vapor deposition apparatus according to still another embodiment of the present invention. Figure 11 is a chemical vapor deposition apparatus showing the vortex prevention unit of Fig. 7 and the flow control unit of Fig. 10; Fig. 12 is a view showing an embodiment according to the present invention attached to Fig. 10 A plurality of guiding members of the flow control unit and a plurality of circulation lines; FIGS. 13A to 13E are diagrams showing an example of a barrier wall of the chemical vapor deposition apparatus according to an embodiment of the present invention.

10‧‧‧反應室10‧‧‧Reaction room

16‧‧‧軸16‧‧‧Axis

18‧‧‧外壁18‧‧‧ outer wall

40‧‧‧氣體引入單元40‧‧‧ gas introduction unit

41‧‧‧第一氣體引入單元41‧‧‧First gas introduction unit

42‧‧‧第二氣體引入單元42‧‧‧Second gas introduction unit

43‧‧‧第三氣體引入單元43‧‧‧ Third gas introduction unit

50‧‧‧氣體排放單元50‧‧‧ gas emission unit

52‧‧‧排氣線52‧‧‧Exhaust line

60‧‧‧流量控制單元60‧‧‧Flow Control Unit

61‧‧‧阻障壁構件61‧‧‧Resistance wall members

64a、64b‧‧‧區分構件64a, 64b‧‧‧ distinguishing components

Claims (16)

一種化學氣相沉積裝置,包括:反應室,其包括感受器與反應爐,該感受器上載放晶圓,該反應爐中藉由化學氣相沉積而加工該晶圓;氣體引入單元,其係配置在該反應室之外壁用以將反應氣體自該反應爐的外側供應至該反應爐之中央部分;以及氣體排放單元,其係配置在該反應室之中央部分用以於該反應氣體被用於該反應爐中的反應之後將該反應氣體排放至該反應室之上方或下方外側,其中該氣體排放單元配置在該反應室之頂部中間部分或該感受器的中央部分。 A chemical vapor deposition apparatus comprising: a reaction chamber comprising a susceptor and a reaction furnace, wherein the susceptor carries a wafer, wherein the wafer is processed by chemical vapor deposition; the gas introduction unit is configured The outer wall of the reaction chamber is for supplying a reaction gas from the outside of the reaction furnace to a central portion of the reaction furnace; and a gas discharge unit is disposed at a central portion of the reaction chamber for the reaction gas to be used for the The reaction gas in the reaction furnace is discharged to the upper side or the lower side of the reaction chamber, wherein the gas discharge unit is disposed at a top intermediate portion of the reaction chamber or a central portion of the susceptor. 如申請專利範圍第1項之化學氣相沉積裝置,復包括配置在該氣體引入單元和該氣體排放單元之間之流量控制單元,以便造成由該氣體引入單元至該氣體排放單元之均勻氣流。 A chemical vapor deposition apparatus according to claim 1, further comprising a flow control unit disposed between the gas introduction unit and the gas discharge unit to cause a uniform gas flow from the gas introduction unit to the gas discharge unit. 如申請專利範圍第2項之化學氣相沉積裝置,復包括提供旋轉動力以朝一個方向旋轉該感受器的驅動單元。 A chemical vapor deposition apparatus according to claim 2, further comprising a driving unit that provides rotational power to rotate the susceptor in one direction. 如申請專利範圍第2項之化學氣相沉積裝置,復包括配置靠近於該感受器之加熱單元以提供熱至該感受器。 A chemical vapor deposition apparatus according to claim 2, further comprising a heating unit disposed adjacent to the susceptor to provide heat to the susceptor. 如申請專利範圍第2項之化學氣相沉積裝置,其中,該流量控制單元包括:阻障壁構件,其係配置於該反應爐之外側以界定該 反應室中的該反應爐,並將供應自該氣體引入單元之該反應氣體引入至該反應爐中,同時調整該反應氣體之壓力;以及至少一個氣體室,其係配置於該反應室之外壁與該阻障壁構件之間用來儲存供應自該氣體引入單元之該反應氣體並透過該阻障壁構件供應該反應氣體。 The chemical vapor deposition apparatus of claim 2, wherein the flow control unit comprises: a barrier member disposed on an outer side of the reactor to define the a reaction furnace in the reaction chamber, and introducing the reaction gas supplied from the gas introduction unit into the reaction furnace while adjusting the pressure of the reaction gas; and at least one gas chamber disposed on the outer wall of the reaction chamber The reactive gas supplied from the gas introduction unit is stored between the barrier member and supplied through the barrier member. 如申請專利範圍第5項之化學氣相沉積裝置,其中,當提供有複數個該氣體室時,該化學氣相沉積裝置復包括至少一個用以分離該複數個氣體室之區分構件。 A chemical vapor deposition apparatus according to claim 5, wherein, when a plurality of the gas chambers are provided, the chemical vapor deposition apparatus further comprises at least one distinguishing member for separating the plurality of gas chambers. 如申請專利範圍第5項之化學氣相沉積裝置,復包括配置在該反應室中於面對該感受器的那側之旋渦防止單元,以便朝向該氣體引入單元漸漸減少該感受器與該反應室之間之距離。 A chemical vapor deposition apparatus according to claim 5, further comprising a vortex preventing unit disposed in the reaction chamber on a side facing the susceptor to gradually reduce the susceptor and the reaction chamber toward the gas introduction unit The distance between them. 如申請專利範圍第2項之化學氣相沉積裝置,其中,該流量控制單元包括:傾斜阻障壁,其係配置於該反應爐之外側用以界定該反應室內之該反應爐,並將供應自該氣體引入單元之該反應氣體引入至該反應爐中,同時調整該反應氣體之壓力,該傾斜阻障壁以預定的角度傾斜;以及複數個氣體室,其係配置於該反應室之外壁與該傾斜阻障壁之間,用以儲存供應自該氣體引入單元之該反應氣體並透過該傾斜阻障壁供應該反應氣體;以及至少一個區分構件,其係用以分離該等氣體室。 The chemical vapor deposition apparatus of claim 2, wherein the flow control unit comprises: a sloped barrier wall disposed on an outer side of the reactor to define the reaction chamber in the reaction chamber, and is supplied from The reaction gas of the gas introduction unit is introduced into the reaction furnace while adjusting the pressure of the reaction gas, the inclined barrier wall is inclined at a predetermined angle; and a plurality of gas chambers disposed on the outer wall of the reaction chamber and the Between the inclined barrier walls, for storing the reaction gas supplied from the gas introduction unit and supplying the reaction gas through the inclined barrier wall; and at least one distinguishing member for separating the gas chambers. 如申請專利範圍第8項之化學氣相沉積裝置,復包括配置在該反應室中於面對該感受器的那側之旋渦防止單元,以便朝向該氣體引入單元漸漸減少該感受器與該反應室之間之距離。 The chemical vapor deposition apparatus of claim 8, further comprising a vortex prevention unit disposed in the reaction chamber on a side facing the susceptor to gradually reduce the susceptor and the reaction chamber toward the gas introduction unit The distance between them. 如申請專利範圍第2項之化學氣相沉積裝置,其中,該流量控制單元包括:複數個氣體室,其係配置於該反應室中;至少一個區分構件,其係用以分離該等氣體室,而使得該氣體室具有不同的長度並成階梯狀;以及區分阻障壁,其係配置於該氣體室之末端部份用以將由該氣體引入單元所供應之該反應氣體引入至該反應爐中,同時調整該反應氣體之壓力,其中,該氣體室係配置於該反應室之外壁與該區分阻障壁之間用以儲存由該氣體引入單元所供應之該反應氣體並透過該區分阻障壁供應該反應氣體。 The chemical vapor deposition apparatus of claim 2, wherein the flow control unit comprises: a plurality of gas chambers disposed in the reaction chamber; at least one distinguishing member for separating the gas chambers And the gas chamber has different lengths and is stepped; and the barrier wall is disposed at an end portion of the gas chamber for introducing the reaction gas supplied by the gas introduction unit into the reaction furnace And adjusting the pressure of the reaction gas, wherein the gas chamber is disposed between the outer wall of the reaction chamber and the different barrier wall for storing the reaction gas supplied by the gas introduction unit and passing through the different barrier wall. The gas should be reacted. 如申請專利範圍第10項之化學氣相沉積裝置,復包括配置在該反應室中於面對該感受器的那側之旋渦防止單元,以便朝向該氣體引入單元漸漸減少該感受器與該反應室之間之距離。 A chemical vapor deposition apparatus according to claim 10, further comprising a vortex prevention unit disposed in the reaction chamber on a side facing the susceptor to gradually reduce the susceptor and the reaction chamber toward the gas introduction unit The distance between them. 如申請專利範圍第10項之化學氣相沉積裝置,復包括複數個於實質水平方向上配置於該等區分阻障壁上之平行導引構件用以導引反應氣體之流動。 The chemical vapor deposition apparatus of claim 10, further comprising a plurality of parallel guiding members disposed on the different barrier walls in a substantially horizontal direction for guiding the flow of the reactive gas. 如申請專利範圍第6項之化學氣相沉積裝置,其中,該 氣體引入單元包括複數個與該等氣體室連通之氣體供應線用以供應不同的氣體至該等氣體室。 A chemical vapor deposition apparatus according to claim 6 of the patent application, wherein The gas introduction unit includes a plurality of gas supply lines in communication with the gas chambers for supplying different gases to the gas chambers. 如申請專利範圍第3項之化學氣相沉積裝置,其中,該驅動單元包括:從動齒輪,其係形成在該感受器之外表面;主動齒輪,其係與該從動齒輪嚙合;以及旋轉馬達,其係配置在旋轉該主動齒輪之驅動軸之末端用以提供旋轉動力。 The chemical vapor deposition apparatus of claim 3, wherein the driving unit comprises: a driven gear formed on an outer surface of the susceptor; a driving gear engaged with the driven gear; and a rotary motor It is disposed at the end of the drive shaft that rotates the drive gear to provide rotational power. 如申請專利範圍第3項之化學氣相沉積裝置,復包括配置在該感受器之中央部分用以旋轉該感受器之軸,該軸包括位於該軸中之氣體排放單元,其中,該驅動單元包括:從動齒輪,其係配置在該感受器;主動齒輪,其係與該從動齒輪嚙合;以及旋轉馬達,其係配置在旋轉該主動齒輪之驅動軸之末端。 A chemical vapor deposition apparatus according to claim 3, further comprising a shaft disposed in a central portion of the susceptor for rotating the susceptor, the shaft comprising a gas discharge unit located in the shaft, wherein the driving unit comprises: a driven gear disposed in the susceptor; a drive gear engaged with the driven gear; and a rotary motor disposed at an end of the drive shaft that rotates the drive gear. 如申請專利範圍第2項之化學氣相沉積裝置,其中,該氣體排放單元包括:排氣孔,其形成於該反應室之內部頂端部份或該感受器之中央部分;以及排氣線,其係與該排氣孔連通。 The chemical vapor deposition apparatus of claim 2, wherein the gas discharge unit comprises: a vent hole formed in an inner top end portion of the reaction chamber or a central portion of the susceptor; and an exhaust line It is in communication with the vent.
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