SU604499A3 - Способ получени галоидированных эфирохлорангидридов кислот фосфора - Google Patents
Способ получени галоидированных эфирохлорангидридов кислот фосфораInfo
- Publication number
- SU604499A3 SU604499A3 SU762325907A SU2325907A SU604499A3 SU 604499 A3 SU604499 A3 SU 604499A3 SU 762325907 A SU762325907 A SU 762325907A SU 2325907 A SU2325907 A SU 2325907A SU 604499 A3 SU604499 A3 SU 604499A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- chlorine
- acid
- theory
- chloride
- phosphoric acid
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims 4
- 150000003017 phosphorus Chemical class 0.000 title claims 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N phosphoric acid Substances OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims 18
- 229910052801 chlorine Inorganic materials 0.000 claims 14
- 239000000460 chlorine Substances 0.000 claims 14
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 13
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims 11
- 238000004508 fractional distillation Methods 0.000 claims 7
- 150000002148 esters Chemical class 0.000 claims 6
- XUCNUKMRBVNAPB-UHFFFAOYSA-N fluoroethene Chemical compound FC=C XUCNUKMRBVNAPB-UHFFFAOYSA-N 0.000 claims 6
- NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical compound CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 claims 5
- 239000002253 acid Substances 0.000 claims 5
- 238000006243 chemical reaction Methods 0.000 claims 5
- 238000001816 cooling Methods 0.000 claims 5
- -1 1,2-dichloroethyl Chemical group 0.000 claims 4
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims 4
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 claims 4
- 229910052794 bromium Inorganic materials 0.000 claims 4
- 229910021578 Iron(III) chloride Inorganic materials 0.000 claims 3
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims 3
- 238000004821 distillation Methods 0.000 claims 3
- 239000007789 gas Substances 0.000 claims 3
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 claims 3
- 239000000203 mixture Substances 0.000 claims 3
- 229910052698 phosphorus Inorganic materials 0.000 claims 3
- 239000011574 phosphorus Substances 0.000 claims 3
- 238000003756 stirring Methods 0.000 claims 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 2
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 claims 2
- 238000005727 Friedel-Crafts reaction Methods 0.000 claims 2
- 150000001336 alkenes Chemical class 0.000 claims 2
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 claims 2
- 150000001875 compounds Chemical class 0.000 claims 2
- 229910052731 fluorine Inorganic materials 0.000 claims 2
- 239000011737 fluorine Substances 0.000 claims 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 2
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 2
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 claims 2
- YLGYEVGIVHHPKT-UHFFFAOYSA-N 1,2-dichloroethyl dihydrogen phosphate Chemical compound OP(O)(=O)OC(Cl)CCl YLGYEVGIVHHPKT-UHFFFAOYSA-N 0.000 claims 1
- DEWLEGDTCGBNGU-UHFFFAOYSA-N 1,3-dichloropropan-2-ol Chemical compound ClCC(O)CCl DEWLEGDTCGBNGU-UHFFFAOYSA-N 0.000 claims 1
- OEPOKWHJYJXUGD-UHFFFAOYSA-N 2-(3-phenylmethoxyphenyl)-1,3-thiazole-4-carbaldehyde Chemical compound O=CC1=CSC(C=2C=C(OCC=3C=CC=CC=3)C=CC=2)=N1 OEPOKWHJYJXUGD-UHFFFAOYSA-N 0.000 claims 1
- ZNFMTXVCNCJLNM-UHFFFAOYSA-N 2-chloro-1-(2-chloro-1-fluoroethoxy)-1-fluoroethane Chemical class ClCC(F)OC(F)CCl ZNFMTXVCNCJLNM-UHFFFAOYSA-N 0.000 claims 1
- VKEIPALYOJMDAC-UHFFFAOYSA-N 3,3,3-trichloroprop-1-ene Chemical compound ClC(Cl)(Cl)C=C VKEIPALYOJMDAC-UHFFFAOYSA-N 0.000 claims 1
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 claims 1
- 150000007513 acids Chemical class 0.000 claims 1
- 238000009835 boiling Methods 0.000 claims 1
- INLLPKCGLOXCIV-UHFFFAOYSA-N bromoethene Chemical compound BrC=C INLLPKCGLOXCIV-UHFFFAOYSA-N 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- UETQVDZZPKAQIC-UHFFFAOYSA-N chlorane Chemical compound Cl.Cl.Cl.Cl UETQVDZZPKAQIC-UHFFFAOYSA-N 0.000 claims 1
- 125000001309 chloro group Chemical group Cl* 0.000 claims 1
- HRYZWHHZPQKTII-UHFFFAOYSA-N chloroethane Chemical compound CCCl HRYZWHHZPQKTII-UHFFFAOYSA-N 0.000 claims 1
- 238000000354 decomposition reaction Methods 0.000 claims 1
- SNVCRNWSNUUGEA-UHFFFAOYSA-N dichlorophosphoryloxymethane Chemical compound COP(Cl)(Cl)=O SNVCRNWSNUUGEA-UHFFFAOYSA-N 0.000 claims 1
- YBBUMZUSUMRUKT-UHFFFAOYSA-N dimethyl hydrogen phosphate hydrochloride Chemical compound Cl.COP(O)(=O)OC YBBUMZUSUMRUKT-UHFFFAOYSA-N 0.000 claims 1
- 229960003750 ethyl chloride Drugs 0.000 claims 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims 1
- 125000005843 halogen group Chemical group 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- SYSQUGFVNFXIIT-UHFFFAOYSA-N n-[4-(1,3-benzoxazol-2-yl)phenyl]-4-nitrobenzenesulfonamide Chemical class C1=CC([N+](=O)[O-])=CC=C1S(=O)(=O)NC1=CC=C(C=2OC3=CC=CC=C3N=2)C=C1 SYSQUGFVNFXIIT-UHFFFAOYSA-N 0.000 claims 1
- 239000003921 oil Substances 0.000 claims 1
- 150000003254 radicals Chemical class 0.000 claims 1
- 239000011541 reaction mixture Substances 0.000 claims 1
- 238000005292 vacuum distillation Methods 0.000 claims 1
- 235000005074 zinc chloride Nutrition 0.000 claims 1
- 239000011592 zinc chloride Substances 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/08—Esters of oxyacids of phosphorus
- C07F9/09—Esters of phosphoric acids
- C07F9/14—Esters of phosphoric acids containing P(=O)-halide groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2507779A DE2507779C2 (de) | 1975-02-22 | 1975-02-22 | Phosphorsäureesterhalogenide sowie Verfahren zu deren Herstellung |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU604499A3 true SU604499A3 (ru) | 1978-04-25 |
Family
ID=5939608
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU762325907A SU604499A3 (ru) | 1975-02-22 | 1976-02-20 | Способ получени галоидированных эфирохлорангидридов кислот фосфора |
Country Status (22)
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2630561A1 (de) * | 1976-07-07 | 1978-01-19 | Bayer Ag | 1-fluor-2-halogen-aethyl-thionophosphor (phosphon)-saeureester, verfahren zu ihrer herstellung und ihre verwendung als insektizide, akarizide und nematizide |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IL30533A (en) * | 1967-09-01 | 1972-01-27 | Bayer Ag | Thiol-or thionothiol-phosphoric or-phosphonic acid esters |
| DE2417143C2 (de) * | 1974-04-09 | 1982-04-15 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von (Thio) Phosphor(Phosphon)säureestern |
-
1975
- 1975-02-22 DE DE2507779A patent/DE2507779C2/de not_active Expired
-
1976
- 1976-01-21 HU HU76BA3358A patent/HU175203B/hu unknown
- 1976-02-18 CH CH200576A patent/CH623058A5/de not_active IP Right Cessation
- 1976-02-19 RO RO7684853A patent/RO68979A/ro unknown
- 1976-02-19 NL NLAANVRAGE7601697,A patent/NL187355C/xx not_active IP Right Cessation
- 1976-02-20 CA CA246,203A patent/CA1072574A/en not_active Expired
- 1976-02-20 SU SU762325907A patent/SU604499A3/ru active
- 1976-02-20 ZA ZA761006A patent/ZA761006B/xx unknown
- 1976-02-20 LU LU74395A patent/LU74395A1/xx unknown
- 1976-02-20 PL PL1976187346A patent/PL99859B1/pl unknown
- 1976-02-20 FR FR7604795A patent/FR2301531A1/fr active Granted
- 1976-02-20 CS CS7600001144A patent/CS181696B2/cs unknown
- 1976-02-20 JP JP51017191A patent/JPS5910677B2/ja not_active Expired
- 1976-02-20 DD DD191380A patent/DD125577A5/xx unknown
- 1976-02-20 BE BE2054842A patent/BE838737A/xx not_active IP Right Cessation
- 1976-02-20 DK DK70576A patent/DK141936C/da not_active IP Right Cessation
- 1976-02-20 AT AT122076A patent/AT341543B/de not_active IP Right Cessation
- 1976-02-20 GB GB6791/76A patent/GB1513341A/en not_active Expired
- 1976-02-20 BR BR7601096A patent/BR7601096A/pt unknown
- 1976-02-20 IL IL7649077A patent/IL49077A/xx unknown
- 1976-02-20 IT IT48195/76A patent/IT1053874B/it active
- 1976-02-20 ES ES445370A patent/ES445370A1/es not_active Expired
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