SU239341A1 - - Google Patents

Info

Publication number

SU239341A1

SU239341A1 SU1194834A SU1194834A SU239341A1 SU 239341 A1 SU239341 A1 SU 239341A1 SU 1194834 A SU1194834 A SU 1194834A SU 1194834 A SU1194834 A SU 1194834A SU 239341 A1 SU239341 A1 SU 239341A1

Authority

SU

USSR - Soviet Union

Prior art keywords

mol

water bath

benzene

art

tryptophol

Prior art date

Links

• Espacenet
• Global Dossier
• Discuss

• OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
• UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
• 238000000034 method Methods 0.000 description 5
• BUDQDWGNQVEFAC-UHFFFAOYSA-N Dihydropyran Chemical compound C1COC=CC1 BUDQDWGNQVEFAC-UHFFFAOYSA-N 0.000 description 3
• 238000004519 manufacturing process Methods 0.000 description 3
• LYPSVQXMCZIRGP-UHFFFAOYSA-N 3-(1h-indol-3-yl)propan-1-ol Chemical compound C1=CC=C2C(CCCO)=CNC2=C1 LYPSVQXMCZIRGP-UHFFFAOYSA-N 0.000 description 2
• FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 2
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
• 239000000010 aprotic solvent Substances 0.000 description 2
• 238000010438 heat treatment Methods 0.000 description 2
• 150000003839 salts Chemical class 0.000 description 2
• MBBOMCVGYCRMEA-UHFFFAOYSA-N tryptophol Chemical compound C1=CC=C2C(CCO)=CNC2=C1 MBBOMCVGYCRMEA-UHFFFAOYSA-N 0.000 description 2
• 238000002211 ultraviolet spectrum Methods 0.000 description 2
• JKTCBAGSMQIFNL-UHFFFAOYSA-N 2,3-dihydrofuran Chemical compound C1CC=CO1 JKTCBAGSMQIFNL-UHFFFAOYSA-N 0.000 description 1
• 230000002378 acidificating effect Effects 0.000 description 1
• KSTSKZBJCVLLKS-UHFFFAOYSA-N benzene;propan-2-ol Chemical compound CC(C)O.C1=CC=CC=C1 KSTSKZBJCVLLKS-UHFFFAOYSA-N 0.000 description 1
• 238000009835 boiling Methods 0.000 description 1
• 230000005494 condensation Effects 0.000 description 1
• 238000009833 condensation Methods 0.000 description 1
• 238000001816 cooling Methods 0.000 description 1
• 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 description 1
• 150000002148 esters Chemical class 0.000 description 1
• 239000000706 filtrate Substances 0.000 description 1
• 230000003993 interaction Effects 0.000 description 1
• 239000012280 lithium aluminium hydride Substances 0.000 description 1
• -1 lithium aluminum hydride Chemical compound 0.000 description 1
• JOVOSQBPPZZESK-UHFFFAOYSA-N phenylhydrazine hydrochloride Chemical compound Cl.NNC1=CC=CC=C1 JOVOSQBPPZZESK-UHFFFAOYSA-N 0.000 description 1
• 229940038531 phenylhydrazine hydrochloride Drugs 0.000 description 1
• 239000000047 product Substances 0.000 description 1
• 239000007858 starting material Substances 0.000 description 1