SG11202102770XA - Process for bio-1,3-butanediol purification from a fermentation broth - Google Patents

Process for bio-1,3-butanediol purification from a fermentation broth

Info

Publication number
SG11202102770XA
SG11202102770XA SG11202102770XA SG11202102770XA SG11202102770XA SG 11202102770X A SG11202102770X A SG 11202102770XA SG 11202102770X A SG11202102770X A SG 11202102770XA SG 11202102770X A SG11202102770X A SG 11202102770XA SG 11202102770X A SG11202102770X A SG 11202102770XA
Authority
SG
Singapore
Prior art keywords
bio
fermentation broth
butanediol
purification
butanediol purification
Prior art date
Application number
SG11202102770XA
Other languages
English (en)
Inventor
Mario Baldassarre
Alberto Cesana
Fabrizio Bordes
Original Assignee
Versalis Spa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Versalis Spa filed Critical Versalis Spa
Publication of SG11202102770XA publication Critical patent/SG11202102770XA/en

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Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/20Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only oxygen atoms as heteroatoms
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/26Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction
    • B01D15/361Ion-exchange
    • B01D15/362Cation-exchange
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/26Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction
    • B01D15/361Ion-exchange
    • B01D15/363Anion-exchange
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D21/00Separation of suspended solid particles from liquids by sedimentation
    • B01D21/26Separation of sediment aided by centrifugal force or centripetal force
    • B01D21/262Separation of sediment aided by centrifugal force or centripetal force by using a centrifuge
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/02Reverse osmosis; Hyperfiltration ; Nanofiltration
    • B01D61/027Nanofiltration
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14Ultrafiltration; Microfiltration
    • B01D61/147Microfiltration
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/58Multistep processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D69/00Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/02Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor characterised by their properties
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/10Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of rare earths
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J47/00Ion-exchange processes in general; Apparatus therefor
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/20Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only oxygen atoms as heteroatoms
    • C07C1/24Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon starting from organic compounds containing only oxygen atoms as heteroatoms by elimination of water
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00Aliphatic unsaturated hydrocarbons
    • C07C11/12Alkadienes
    • C07C11/16Alkadienes with four carbon atoms
    • C07C11/1671, 3-Butadiene
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18Polyhydroxylic acyclic alcohols
    • C07C31/20Dihydroxylic alcohols
    • C07C31/2071,4-Butanediol; 1,3-Butanediol; 1,2-Butanediol; 2,3-Butanediol
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F36/00Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds
    • C08F36/02Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds the radical having only two carbon-to-carbon double bonds
    • C08F36/04Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds the radical having only two carbon-to-carbon double bonds conjugated
    • C08F36/06Butadiene
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00Preparation of oxygen-containing organic compounds
    • C12P7/02Preparation of oxygen-containing organic compounds containing a hydroxy group
    • C12P7/04Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic
    • C12P7/18Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic polyhydric
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00Preparation of oxygen-containing organic compounds
    • C12P7/62Carboxylic acid esters
    • C12P7/625Polyesters of hydroxy carboxylic acids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2325/00Details relating to properties of membranes
    • B01D2325/02Details relating to pores or porosity of the membranes
    • B01D2325/0283Pore size
    • B01D2325/02834Pore size more than 0.1 and up to 1 µm
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2325/00Details relating to properties of membranes
    • B01D2325/34Molecular weight or degree of polymerisation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2523/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group C07C2521/00
    • C07C2523/10Catalysts comprising metals or metal oxides or hydroxides, not provided for in group C07C2521/00 of rare earths

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Water Supply & Treatment (AREA)
  • Zoology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Biotechnology (AREA)
  • Biochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Microbiology (AREA)
  • Nanotechnology (AREA)
  • Materials Engineering (AREA)
  • Analytical Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Inorganic Chemistry (AREA)
SG11202102770XA 2018-09-21 2019-09-19 Process for bio-1,3-butanediol purification from a fermentation broth SG11202102770XA (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
IT201800008820 2018-09-21
PCT/EP2019/075123 WO2020058381A1 (en) 2018-09-21 2019-09-19 Process for bio-1,3-butanediol purification from a fermentation broth

Publications (1)

Publication Number Publication Date
SG11202102770XA true SG11202102770XA (en) 2021-04-29

Family

ID=64607119

Family Applications (1)

Application Number Title Priority Date Filing Date
SG11202102770XA SG11202102770XA (en) 2018-09-21 2019-09-19 Process for bio-1,3-butanediol purification from a fermentation broth

Country Status (20)

Country Link
US (1) US20210380512A1 (ko)
EP (1) EP3853197B1 (ko)
JP (1) JP7390369B2 (ko)
KR (1) KR20210068049A (ko)
CN (1) CN113166008B (ko)
AU (1) AU2019344574B2 (ko)
BR (1) BR112021005183B1 (ko)
CA (1) CA3113477A1 (ko)
CL (1) CL2021000700A1 (ko)
DK (1) DK3853197T3 (ko)
EA (1) EA202190811A1 (ko)
ES (1) ES2975943T3 (ko)
FI (1) FI3853197T3 (ko)
HU (1) HUE065469T2 (ko)
IL (1) IL281601B2 (ko)
MX (1) MX2021003364A (ko)
PL (1) PL3853197T3 (ko)
PT (1) PT3853197T (ko)
SG (1) SG11202102770XA (ko)
WO (1) WO2020058381A1 (ko)

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1908620A1 (de) 1969-02-21 1970-09-03 Basf Ag Verfahren zur Herstellung modifizierter Polyolefinwachse
JPS6165834A (ja) * 1984-09-07 1986-04-04 Daicel Chem Ind Ltd 1,3−ブチレングリコ−ルの精製法
US6361983B1 (en) 1999-09-30 2002-03-26 E. I. Du Pont De Nemours And Company Process for the isolation of 1,3-propanediol from fermentation broth
BRPI0410685B8 (pt) * 2003-05-06 2017-05-30 Du Pont processos de purificação do 1,3-propanodiol e composição
EP3865569B1 (en) 2009-04-30 2023-10-04 Genomatica, Inc. Organisms for the production of 1,3-butanediol
KR102237801B1 (ko) * 2009-06-04 2021-04-07 게노마티카 인코포레이티드 발효액 성분들의 분리 방법
WO2012177619A2 (en) 2011-06-22 2012-12-27 Genomatica, Inc. Microorganisms for producing 1,3-butanediol and methods related thereto
CA2845681A1 (en) * 2011-08-19 2013-02-28 Genomatica, Inc. Microorganisms and methods for producing 2,4-pentadienoate, butadiene, propylene, 1,3-butanediol and related alcohols
IN2014CN02584A (ko) 2011-09-08 2015-08-07 Genomatica Inc
BR112014008195B1 (pt) * 2011-10-14 2021-04-20 Toray Industries, Inc método para produzir 2,3-butanodiol
EP3964493B1 (en) * 2013-03-15 2024-03-27 Genomatica, Inc. Process and systems for obtaining 1,4-butanediol from fermentation broths
US20140275465A1 (en) 2013-03-15 2014-09-18 Genomatica, Inc. Process and systems for obtaining 1,4-butanediol from fermentation broths
JP2014176567A (ja) 2013-03-15 2014-09-25 Makita Corp クリーナ
BR112015024633B1 (pt) * 2013-04-12 2022-03-15 Toray Industries, Inc Processos de produção de 1,4-butanodiol e de um poliéster
EP3072974B1 (en) * 2013-11-22 2019-07-24 Toray Industries, Inc. Method for producing 2,3-butanediol
RU2695786C2 (ru) 2014-05-16 2019-07-26 ВЕРСАЛИС С.п.А. Способ получения алкенолов и его применение для получения 1,3-бутадиена
BR112017012500B1 (pt) * 2014-12-12 2022-05-03 Versalis S.P.A. Processo para a produção de 1,3-butadieno a partir de 1,3- butanodiol
WO2016135605A1 (en) 2015-02-23 2016-09-01 Versalis S.P.A. Process for the dehydration of oxygenated compounds
RU2692477C2 (ru) 2015-02-23 2019-06-25 ВЕРСАЛИС С.п.А. Способ получения диенов
IT201600105178A1 (it) * 2016-10-19 2018-04-19 Versalis Spa Procedimento per la produzione di dieni
US20210101855A1 (en) * 2017-03-31 2021-04-08 Genomatica, Inc. Process and systems for obtaining 1,3-butanediol from fermentation broths

Also Published As

Publication number Publication date
BR112021005183A2 (pt) 2021-06-29
CN113166008A (zh) 2021-07-23
MX2021003364A (es) 2021-08-16
CN113166008B (zh) 2024-02-06
BR112021005183B1 (pt) 2024-03-12
EP3853197B1 (en) 2024-01-24
CA3113477A1 (en) 2020-03-26
WO2020058381A1 (en) 2020-03-26
PT3853197T (pt) 2024-02-22
KR20210068049A (ko) 2021-06-08
CL2021000700A1 (es) 2021-10-08
EA202190811A1 (ru) 2021-06-17
AU2019344574B2 (en) 2024-01-25
IL281601B1 (en) 2023-11-01
JP7390369B2 (ja) 2023-12-01
ES2975943T3 (es) 2024-07-18
PL3853197T3 (pl) 2024-05-20
IL281601B2 (en) 2024-03-01
DK3853197T3 (da) 2024-02-12
US20210380512A1 (en) 2021-12-09
JP2022502364A (ja) 2022-01-11
AU2019344574A1 (en) 2021-04-29
IL281601A (en) 2021-05-31
HUE065469T2 (hu) 2024-06-28
FI3853197T3 (fi) 2024-03-01
EP3853197A1 (en) 2021-07-28

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