SG11201703365VA - Process for in situ water removal from an oxidative esterification reaction using a coupled reactor-distillation system - Google Patents

Process for in situ water removal from an oxidative esterification reaction using a coupled reactor-distillation system

Info

Publication number
SG11201703365VA
SG11201703365VA SG11201703365VA SG11201703365VA SG11201703365VA SG 11201703365V A SG11201703365V A SG 11201703365VA SG 11201703365V A SG11201703365V A SG 11201703365VA SG 11201703365V A SG11201703365V A SG 11201703365VA SG 11201703365V A SG11201703365V A SG 11201703365VA
Authority
SG
Singapore
Prior art keywords
esterification reaction
water removal
distillation system
oxidative esterification
coupled reactor
Prior art date
Application number
SG11201703365VA
Inventor
Zubin B Kuvadia
Kirk W Limbach
Dmitri A Kraptchetov
Mark A Silvano
Original Assignee
Dow Global Technologies Llc
Rohm & Haas
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Global Technologies Llc, Rohm & Haas filed Critical Dow Global Technologies Llc
Publication of SG11201703365VA publication Critical patent/SG11201703365VA/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/39Preparation of carboxylic acid esters by oxidation of groups which are precursors for the acid moiety of the ester
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/42Regulation; Control
    • B01D3/4205Reflux ratio control splitter
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/008Control or steering systems not provided for elsewhere in subclass C02F
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/02Treatment of water, waste water, or sewage by heating
    • C02F1/04Treatment of water, waste water, or sewage by heating by distillation or evaporation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/39Preparation of carboxylic acid esters by oxidation of groups which are precursors for the acid moiety of the ester
    • C07C67/40Preparation of carboxylic acid esters by oxidation of groups which are precursors for the acid moiety of the ester by oxidation of primary alcohols
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/52Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/54Acrylic acid esters; Methacrylic acid esters
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/34Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32
    • C02F2103/36Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32 from the manufacture of organic compounds
    • C02F2103/38Polymers
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency
SG11201703365VA 2014-10-31 2015-10-02 Process for in situ water removal from an oxidative esterification reaction using a coupled reactor-distillation system SG11201703365VA (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201462073285P 2014-10-31 2014-10-31
PCT/US2015/053672 WO2016069199A1 (en) 2014-10-31 2015-10-02 Process for in situ water removal from an oxidative esterification reaction using a coupled reactor-distillation system

Publications (1)

Publication Number Publication Date
SG11201703365VA true SG11201703365VA (en) 2017-05-30

Family

ID=54330058

Family Applications (1)

Application Number Title Priority Date Filing Date
SG11201703365VA SG11201703365VA (en) 2014-10-31 2015-10-02 Process for in situ water removal from an oxidative esterification reaction using a coupled reactor-distillation system

Country Status (12)

Country Link
US (1) US9963419B2 (en)
EP (1) EP3212606B1 (en)
JP (1) JP6608926B2 (en)
KR (1) KR102428000B1 (en)
CN (1) CN107108446B (en)
BR (1) BR112017008420A2 (en)
CA (1) CA2965479C (en)
MX (1) MX2017005053A (en)
SA (1) SA517381376B1 (en)
SG (1) SG11201703365VA (en)
TW (1) TW201615610A (en)
WO (1) WO2016069199A1 (en)

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2848369C3 (en) 1977-11-17 1981-08-06 Asahi Kasei Kogyo K.K., Osaka Process for the preparation of carboxylic acid esters
DE3018071C2 (en) 1979-05-17 1985-06-05 Asahi Kasei Kogyo K.K., Osaka Process for the preparation of carboxylic acid esters
JPS5687530A (en) 1979-12-19 1981-07-16 Asahi Chem Ind Co Ltd Dehydrating method of gas containing unsaturated aldehyde
JPH0244294B2 (en) * 1982-03-15 1990-10-03 Asahi Chemical Ind METAKUROREINNOKAISHUHOHO
JPS58198442A (en) * 1982-05-14 1983-11-18 Asahi Chem Ind Co Ltd Improved method for preparation of methyl methacrylate or methyl acrylate
DE69632788T2 (en) 1995-07-18 2005-07-14 Asahi Kasei Chemicals Corp. CATALYST FOR THE PREPARATION OF CARBOXYLIC ACID ESTERS
DE19536178A1 (en) * 1995-09-28 1997-04-03 Basf Ag Process and device for the continuous production of alkyl esters of (meth) acrylic acid
DE19604267A1 (en) 1996-02-06 1997-08-07 Basf Ag Process for the continuous production of alkyl esters of (meth) acrylic acid
JPH09216850A (en) 1996-02-09 1997-08-19 Mitsubishi Rayon Co Ltd Production of carboxylic acid ester
TW385304B (en) * 1996-09-10 2000-03-21 Asahi Chemical Ind Process for producing methacrylic acid ester or acrylic acid ester
JP3932149B2 (en) * 1997-04-25 2007-06-20 タイコエレクトロニクスアンプ株式会社 Electrical connector assembly and manufacturing method thereof
JPH10306063A (en) * 1997-05-07 1998-11-17 Chiyoda Corp Production of carbonic ester
JP3681285B2 (en) * 1997-07-08 2005-08-10 旭化成ケミカルズ株式会社 Method for producing methyl methacrylate
SG71815A1 (en) 1997-07-08 2000-04-18 Asahi Chemical Ind Method of producing methyl methacrylate
JP3238894B2 (en) * 1998-02-09 2001-12-17 三菱レイヨン株式会社 Method for producing methyl methacrylate
BRPI0408043B1 (en) 2003-02-28 2015-08-18 Arkema Inc Process for conducting equilibrium-limited reactions of at least one reactant to produce at least one product
US8906502B2 (en) 2006-12-29 2014-12-09 Ccp Composites Us Llc Organic powder useful as the replacement of mineral filler in composites
KR102213622B1 (en) * 2013-04-19 2021-02-08 룀 게엠베하 Method for producing methylmethacrylate
CN103420835A (en) * 2013-07-01 2013-12-04 太仓市恒益医药化工原料厂 Method for preparing methyl methacrylate by using methacrolein

Also Published As

Publication number Publication date
CA2965479A1 (en) 2016-05-06
US9963419B2 (en) 2018-05-08
TW201615610A (en) 2016-05-01
CA2965479C (en) 2022-12-06
CN107108446A (en) 2017-08-29
BR112017008420A2 (en) 2018-01-23
SA517381376B1 (en) 2020-06-15
EP3212606B1 (en) 2019-11-20
US20170240500A1 (en) 2017-08-24
KR20170076711A (en) 2017-07-04
WO2016069199A1 (en) 2016-05-06
CN107108446B (en) 2020-05-19
JP6608926B2 (en) 2019-11-20
EP3212606A1 (en) 2017-09-06
KR102428000B1 (en) 2022-08-02
MX2017005053A (en) 2017-07-04
JP2017533214A (en) 2017-11-09

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