SE514338C2 - Förfarande för rening av sur laklösning - Google Patents
Förfarande för rening av sur laklösningInfo
- Publication number
- SE514338C2 SE514338C2 SE9902008A SE9902008A SE514338C2 SE 514338 C2 SE514338 C2 SE 514338C2 SE 9902008 A SE9902008 A SE 9902008A SE 9902008 A SE9902008 A SE 9902008A SE 514338 C2 SE514338 C2 SE 514338C2
- Authority
- SE
- Sweden
- Prior art keywords
- solution
- stage
- precipitation
- arsenic
- returned
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 24
- 230000002378 acidificating effect Effects 0.000 title claims description 9
- 238000000746 purification Methods 0.000 title claims 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 title 1
- 238000001556 precipitation Methods 0.000 claims abstract description 24
- 239000002244 precipitate Substances 0.000 claims abstract description 19
- 229910052785 arsenic Inorganic materials 0.000 claims abstract description 13
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000002184 metal Substances 0.000 claims abstract description 10
- 229910052751 metal Inorganic materials 0.000 claims abstract description 10
- 150000002739 metals Chemical class 0.000 claims abstract description 6
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims abstract description 5
- 235000011941 Tilia x europaea Nutrition 0.000 claims abstract description 5
- 239000004571 lime Substances 0.000 claims abstract description 5
- 230000003647 oxidation Effects 0.000 claims abstract description 5
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 5
- 239000011343 solid material Substances 0.000 claims abstract description 5
- 239000007787 solid Substances 0.000 claims abstract description 4
- 235000019738 Limestone Nutrition 0.000 claims abstract description 3
- 239000006028 limestone Substances 0.000 claims abstract description 3
- 239000000463 material Substances 0.000 claims abstract description 3
- 239000003795 chemical substances by application Substances 0.000 claims abstract 6
- 235000010855 food raising agent Nutrition 0.000 claims description 5
- 239000010970 precious metal Substances 0.000 claims description 4
- 238000007664 blowing Methods 0.000 claims description 3
- 239000004922 lacquer Substances 0.000 claims description 3
- 230000001590 oxidative effect Effects 0.000 claims 1
- 230000001376 precipitating effect Effects 0.000 claims 1
- 238000012958 reprocessing Methods 0.000 claims 1
- 239000002253 acid Substances 0.000 abstract description 3
- 238000002386 leaching Methods 0.000 abstract description 3
- 239000002667 nucleating agent Substances 0.000 abstract 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 23
- 229910052742 iron Inorganic materials 0.000 description 11
- 239000002562 thickening agent Substances 0.000 description 8
- 239000011701 zinc Substances 0.000 description 7
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 6
- 229910052725 zinc Inorganic materials 0.000 description 6
- 238000000605 extraction Methods 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- 229910017052 cobalt Inorganic materials 0.000 description 3
- 239000010941 cobalt Substances 0.000 description 3
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- 239000004131 EU approved raising agent Substances 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 238000005363 electrowinning Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 239000005909 Kieselgur Substances 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000005667 attractant Substances 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 238000000975 co-precipitation Methods 0.000 description 1
- 238000005056 compaction Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000010440 gypsum Substances 0.000 description 1
- 229910052602 gypsum Inorganic materials 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- 235000014413 iron hydroxide Nutrition 0.000 description 1
- NCNCGGDMXMBVIA-UHFFFAOYSA-L iron(ii) hydroxide Chemical compound [OH-].[OH-].[Fe+2] NCNCGGDMXMBVIA-UHFFFAOYSA-L 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B23/00—Obtaining nickel or cobalt
- C22B23/04—Obtaining nickel or cobalt by wet processes
- C22B23/0453—Treatment or purification of solutions, e.g. obtained by leaching
- C22B23/0461—Treatment or purification of solutions, e.g. obtained by leaching by chemical methods
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B15/00—Obtaining copper
- C22B15/0063—Hydrometallurgy
- C22B15/0084—Treating solutions
- C22B15/0089—Treating solutions by chemical methods
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B19/00—Obtaining zinc or zinc oxide
- C22B19/20—Obtaining zinc otherwise than by distilling
- C22B19/26—Refining solutions containing zinc values, e.g. obtained by leaching zinc ores
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Geochemistry & Mineralogy (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Removal Of Specific Substances (AREA)
Priority Applications (9)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE9902008A SE514338C2 (sv) | 1999-06-01 | 1999-06-01 | Förfarande för rening av sur laklösning |
| AU27668/00A AU761108B2 (en) | 1999-06-01 | 2000-04-11 | A method of purifying acid leaching solution |
| US09/551,576 US6406676B1 (en) | 1999-06-01 | 2000-04-18 | Method of purifying acid leaching solution by precipitation and oxidation |
| CA 2306015 CA2306015C (en) | 1999-06-01 | 2000-04-18 | A method of purifying acid leaching solution |
| ZA200002201A ZA200002201B (en) | 1999-06-01 | 2000-05-05 | A method of purifying acid leaching solution. |
| EA200000476A EA002674B1 (ru) | 1999-06-01 | 2000-05-30 | Способ очистки раствора кислотного выщелачивания |
| EP20000850095 EP1059361A1 (de) | 1999-06-01 | 2000-05-30 | Verfahren zur Entfernung von Eisen aus einer sauren Laugelösung |
| PE2000000518A PE20010341A1 (es) | 1999-06-01 | 2000-05-30 | Metodo para purificar una solucion acida de lixiviado |
| MXPA00005341A MXPA00005341A (es) | 1999-06-01 | 2000-05-31 | Metodo para purificar una solucion acida de lixiviado. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE9902008A SE514338C2 (sv) | 1999-06-01 | 1999-06-01 | Förfarande för rening av sur laklösning |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| SE9902008D0 SE9902008D0 (sv) | 1999-06-01 |
| SE9902008L SE9902008L (sv) | 2000-12-02 |
| SE514338C2 true SE514338C2 (sv) | 2001-02-12 |
Family
ID=20415837
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SE9902008A SE514338C2 (sv) | 1999-06-01 | 1999-06-01 | Förfarande för rening av sur laklösning |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US6406676B1 (de) |
| EP (1) | EP1059361A1 (de) |
| AU (1) | AU761108B2 (de) |
| CA (1) | CA2306015C (de) |
| EA (1) | EA002674B1 (de) |
| MX (1) | MXPA00005341A (de) |
| PE (1) | PE20010341A1 (de) |
| SE (1) | SE514338C2 (de) |
| ZA (1) | ZA200002201B (de) |
Families Citing this family (33)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7314604B1 (en) * | 1999-09-30 | 2008-01-01 | Billiton Intellectual Property, B.V. | Stable ferric arsenate precipitation from acid copper solutions whilst minimising copper losses |
| US6843976B2 (en) * | 2001-02-27 | 2005-01-18 | Noranda Inc. | Reduction of zinc oxide from complex sulfide concentrates using chloride processing |
| US7455715B2 (en) | 2001-07-13 | 2008-11-25 | Teck Cominco Metals Ltd. | Heap bioleaching process for the extraction of zinc |
| CA2353002C (en) | 2001-07-13 | 2009-12-01 | Teck Cominco Metals Ltd. | Heap bioleaching process for the extraction of zinc |
| US6863825B2 (en) | 2003-01-29 | 2005-03-08 | Union Oil Company Of California | Process for removing arsenic from aqueous streams |
| US7399454B2 (en) | 2004-04-29 | 2008-07-15 | Metalox International, Llc | Metallurgical dust reclamation process |
| US7124777B2 (en) * | 2004-09-03 | 2006-10-24 | Ranco Incorporated Of Delaware | Reversing valve with flowsplitter |
| FI119438B (fi) | 2005-05-03 | 2008-11-14 | Outokumpu Oy | Menetelmä arvometallien ja arseenin talteenottamiseksi liuoksesta |
| US8066874B2 (en) | 2006-12-28 | 2011-11-29 | Molycorp Minerals, Llc | Apparatus for treating a flow of an aqueous solution containing arsenic |
| CN101842504B (zh) | 2007-05-21 | 2012-11-14 | 奥贝特铝业有限公司 | 从铝土矿石中提取铝和铁的工艺 |
| US8252087B2 (en) | 2007-10-31 | 2012-08-28 | Molycorp Minerals, Llc | Process and apparatus for treating a gas containing a contaminant |
| US20090107925A1 (en) * | 2007-10-31 | 2009-04-30 | Chevron U.S.A. Inc. | Apparatus and process for treating an aqueous solution containing biological contaminants |
| US8349764B2 (en) | 2007-10-31 | 2013-01-08 | Molycorp Minerals, Llc | Composition for treating a fluid |
| US20090145856A1 (en) * | 2007-12-11 | 2009-06-11 | Raymond Letize A | Acid recycle process with iron removal |
| WO2009114903A1 (en) * | 2008-03-20 | 2009-09-24 | Bhp Billiton Ssm Development Pty Ltd | Process for the recovery of nickel and/or cobalt from high ferrous content laterite ores |
| AU2010270723A1 (en) * | 2009-07-06 | 2012-02-09 | Molycorp Minerals Llc | Ceria for use as an antimicrobial barrier and disinfectant in a wound dressing |
| RU2588960C2 (ru) | 2011-03-18 | 2016-07-10 | Орбит Элюминэ Инк. | Способы извлечения редкоземельных элементов из алюминийсодержащих материалов |
| US9233863B2 (en) | 2011-04-13 | 2016-01-12 | Molycorp Minerals, Llc | Rare earth removal of hydrated and hydroxyl species |
| US9410227B2 (en) | 2011-05-04 | 2016-08-09 | Orbite Technologies Inc. | Processes for recovering rare earth elements from various ores |
| WO2012162817A1 (en) | 2011-06-03 | 2012-12-06 | Orbite Aluminae Inc. | Methods for preparing hematite |
| BR112014006275A2 (pt) | 2011-09-16 | 2017-04-11 | Orbite Aluminae Inc | processos de preparação de alumina e de vários outros produtos |
| EP2802675B1 (de) | 2012-01-10 | 2020-03-11 | Orbite Aluminae Inc. | Verfahren zur behandlung von rotschlamm |
| AU2013203808B2 (en) | 2012-03-29 | 2016-07-28 | Aem Technologies Inc. | Processes for treating fly ashes |
| BR112015000626A2 (pt) | 2012-07-12 | 2017-06-27 | Orbite Aluminae Inc | processos para preparação de óxido de titânio e outros produtos variados |
| BR112015006536A2 (pt) | 2012-09-26 | 2017-08-08 | Orbite Aluminae Inc | processos para preparar alumina e cloreto de magnésio por lixiviação com hcl de vários materiais. |
| US9534274B2 (en) | 2012-11-14 | 2017-01-03 | Orbite Technologies Inc. | Methods for purifying aluminium ions |
| MX2013004855A (es) * | 2013-04-29 | 2014-10-29 | Servicios Condumex Sa | Procedimiento de biolixiviacion y extracción por disolventes con recuperación selectiva de cobre y zinc a partir de concentrados polimetalicos de sulfuros. |
| CA2952568C (en) | 2014-01-31 | 2018-07-10 | Goldcorp Inc. | Process for separation of at least one metal sulfide from a mixed sulfide ore or concentrate |
| BR112016020631A2 (pt) | 2014-03-07 | 2018-05-15 | Secure Natural Resources Llc | óxido de cério (iv) com excepcionais propriedades de remoção de arsênico |
| CN104846199A (zh) * | 2015-06-10 | 2015-08-19 | 云南驰宏锌锗股份有限公司 | 一种脱除硫酸铜溶液中铁、砷的方法 |
| CN107915291A (zh) * | 2017-11-17 | 2018-04-17 | 金川集团股份有限公司 | 一种利用废水沉砷渣对含砷硫酸铜溶液进行除砷的方法 |
| CN109607872B (zh) * | 2019-01-07 | 2021-11-19 | 紫金矿业集团股份有限公司 | 一种含砷污酸的综合利用及砷的安全处置方法 |
| CN109574319B (zh) * | 2019-01-07 | 2021-11-19 | 紫金矿业集团股份有限公司 | 有色金属冶炼高砷污酸的固砷工艺 |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE125827C (de) | 1901-04-03 | 1901-12-07 | ||
| US3510259A (en) | 1967-07-13 | 1970-05-05 | Union Carbide Canada Ltd | Simultaneous leaching of zinc and manganese ores |
| JPS525563B2 (de) * | 1972-08-11 | 1977-02-15 | ||
| DE2342729C2 (de) * | 1973-08-24 | 1975-09-11 | Duisburger Kupferhuette, 4100 Duisburg | Verfahren zur Ausfällung und Abtrennung von Arsen aus kupferhaltigen Lösungen |
| US3985856A (en) | 1975-02-06 | 1976-10-12 | Continental Oil Company | Removal of iron from aqueous acid solutions containing iron and copper |
| DD125827A1 (de) * | 1976-03-26 | 1977-05-18 | ||
| JPS533992A (en) * | 1976-06-30 | 1978-01-14 | Daido Kagaku Sochi | Recovery and treating process for waste sulfuric acid |
| JPS5482307A (en) * | 1977-12-14 | 1979-06-30 | Dowa Mining Co | Arsenic removing method |
| US4244734A (en) | 1979-07-19 | 1981-01-13 | Hazen Research, Inc. | Process for recovering metal values from materials containing arsenic |
| CA1139466A (en) * | 1980-08-22 | 1983-01-11 | Donald R. Weir | Removal of arsenic from aqueous solutions |
| JPS602916B2 (ja) * | 1981-09-04 | 1985-01-24 | 同和工営株式会社 | 含砒素・硫酸第１鉄溶液の脱砒処理法 |
| JPS5952583A (ja) * | 1982-09-18 | 1984-03-27 | Dowa Mining Co Ltd | 鉄酸化バクテリアを使用する砒素と鉄を含有する水溶液の処理法 |
| ZW23883A1 (en) * | 1982-11-11 | 1984-06-13 | Interox Chemicals Ltd | Metals recovery |
| JPS59164639A (ja) * | 1983-03-08 | 1984-09-17 | Nippon Mining Co Ltd | ひ素の分離法 |
| SU1735404A1 (ru) | 1990-07-11 | 1992-05-23 | Государственный научно-исследовательский институт цветных металлов "Гинцветмет" | Способ очистки сульфатных цинковых растворов от мышь ка |
| JP3208746B2 (ja) | 1991-04-16 | 2001-09-17 | 住友金属鉱山株式会社 | ニッケル電解液のヒ素除去方法 |
| ZA928157B (en) * | 1991-10-25 | 1993-06-09 | Sasox Processing Pty Ltd | Extraction or recovery of metal values. |
| CA2084327A1 (en) * | 1992-12-02 | 1994-06-03 | Nural Kuyucak | Lime neutralization process for treating acidic waters |
| AUPN439395A0 (en) | 1995-07-25 | 1995-08-17 | Bactech (Australia) Pty Limited | Process for the removal of arsenic from bacterial leach liquors and slurries |
| US5912402A (en) | 1995-10-30 | 1999-06-15 | Drinkard Metalox, Inc. | Metallurgical dust recycle process |
-
1999
- 1999-06-01 SE SE9902008A patent/SE514338C2/sv not_active IP Right Cessation
-
2000
- 2000-04-11 AU AU27668/00A patent/AU761108B2/en not_active Expired
- 2000-04-18 US US09/551,576 patent/US6406676B1/en not_active Expired - Lifetime
- 2000-04-18 CA CA 2306015 patent/CA2306015C/en not_active Expired - Lifetime
- 2000-05-05 ZA ZA200002201A patent/ZA200002201B/xx unknown
- 2000-05-30 PE PE2000000518A patent/PE20010341A1/es not_active Application Discontinuation
- 2000-05-30 EP EP20000850095 patent/EP1059361A1/de not_active Withdrawn
- 2000-05-30 EA EA200000476A patent/EA002674B1/ru not_active IP Right Cessation
- 2000-05-31 MX MXPA00005341A patent/MXPA00005341A/es active IP Right Grant
Also Published As
| Publication number | Publication date |
|---|---|
| EA200000476A2 (ru) | 2000-12-25 |
| SE9902008L (sv) | 2000-12-02 |
| CA2306015C (en) | 2004-06-22 |
| PE20010341A1 (es) | 2001-04-05 |
| SE9902008D0 (sv) | 1999-06-01 |
| MXPA00005341A (es) | 2002-03-08 |
| AU761108B2 (en) | 2003-05-29 |
| CA2306015A1 (en) | 2000-12-01 |
| EA002674B1 (ru) | 2002-08-29 |
| US6406676B1 (en) | 2002-06-18 |
| EP1059361A1 (de) | 2000-12-13 |
| EA200000476A3 (ru) | 2001-04-23 |
| ZA200002201B (en) | 2000-11-14 |
| AU2766800A (en) | 2000-12-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| NUG | Patent has lapsed |