RU2821049C1 - Composition of ingredients for alcohol-containing tonic balsam - Google Patents

Abstract

FIELD: alcoholic beverages.

SUBSTANCE: invention relates to production of alcohol-containing beverages. Composition of ingredients for an alcohol-containing tonic balsam contains root and rhizomes of Rhodiola rosea – golden root, inflorescences and flowers of common tansy, cedar nuts, juniper cones, leaves and tops of stems of common valerian, leaves and tops of flowering stems of Artemisia jacutica, ground part of Baikal skullcap, flowers of common marigold, tops of blooming stems of great burnet, broadleaf plantain leaf, lingonberry leaf, bearberry (Arctostaphylos uva-ursi) leaf, black currant leaf, wild strawberry leaf, raspberry leaf, sowing oat grain, fresh seedlings of sowing wheat, reindeer antlers extract – Epsorin, fortified juice of fresh lingonberry, fortified fruit drink from dried rowan fruits, fortified fruit drink from dried rosehips, birch buds, elecampane root, leaves and tops of flowering stems of yellow melilot, common tormentil root, ground part of creeping thyme, sugar syrup, colourant, water-alcohol liquid, is characterized by that it additionally contains common anise fruits, buds of unblown cloves flowers, coriander fruits, cinnamon, nutmeg, Paeonia anomala root, pine buds, marsh Labrador tea, oak bark, linden flowers at a certain ratio of ingredients.

EFFECT: invention increases antioxidant activity of the balsam.

1 cl, 1 tbl, 3 ex

Description

The invention relates to the food industry, in particular to the production of alcohol-containing tonic balms used for the preparation of tonic and medicinal-flavoring drinks.

There is a known composition of ingredients for the bitter tincture-balm "Siberia", containing Rhodiola rosea (golden root), plantain, pine nut, tansy, pantocrine, birch buds, plantain, wormwood, chokeberry juice, etc., bioactive components, as well as color, aqueous-alcoholic liquid (USSR AS No. 726163, C12G 3/06, op. 04/05/1980).

A composition of ingredients for a tonic balm is also known, containing Rhodiola rosea, juniper, wild rosemary, valerian officinalis, wormwood, tansy, skullcap, calendula officinalis, burnet, plantain, leaf, root, pine nut, lingonberry leaf, bearberry, black currant, strawberry , raspberries, oat grains, wheat sprouts, rantorin, dried rowan fruits, dried rose hips, fresh lingonberries, sugar, color and aqueous-alcoholic liquid - the rest - up to 1000 dal with a strength of 45% vol. (RF patent No. 2021342, C12G3/06, op. 10/15/94).

The disadvantage is that these compositions do not have a sufficiently high biological value of the finished product.

The closest to the proposed invention is a composition of ingredients for a tonic balm containing the root and rhizomes of Rhodiola rosea - golden root, inflorescences and flowers of tansy, pine nuts, juniper cones, leaves and stem tips of valerian officinalis, Yakut wormwood herb, skullcap herb, flowers calendula officinalis, tops of flowering stems of burnet, plantain leaf and root, lingonberry leaf, bearberry leaf, black currant, strawberry, raspberry, oat grain, wheat sprouts, fresh lingonberry, dried rowan fruits, dried rose hips, birch buds, elecampane root , leaves and tops of flowering stems of sweet clover, cinquefoil erect root, aerial part of creeping thyme and Epsorin, natural honey, vanillin, lemon essential oil, orange essential oil, citric acid, sugar, color and aqueous-alcoholic liquid (RF patent No. 2764075, C12G3/06, op. 01/13/2022).

However, it, having 10 fewer components in its composition than the claimed composition, has 45% less biological activity in terms of the content of low molecular weight antioxidants (Table 1).

The objective of the present invention is to increase the biological value of a tonic alcohol-containing balm according to the criterion of the content of low molecular weight antioxidants.

The technical result is an increase in the antioxidant activity of the balm infusion.

The specified technical result is achieved by a composition of ingredients for an alcohol-containing tonic balm, including the root and rhizomes of Rhodiola rosea - golden root, inflorescences and flowers of tansy, pine nuts, juniper cones, leaves and tops of stems of valerian officinalis, leaves and tops of flowering stems of Yakut wormwood, terrestrial part of skullcap Baikal, flowers of calendula officinalis, tops of flowering stems of burnet, large plantain leaf, lingonberry leaf, bearberry leaf, black currant leaf, wild strawberry leaf, raspberry leaf, oat grain, fresh wheat seedlings, reindeer antlers extract ( Epsorin), alcoholized juice from fresh lingonberries, alcoholized fruit drink from dried rowan fruits, alcoholized fruit drink from dried rose hips, birch buds, elecampane root, leaves and tops of flowering stems of sweet clover, cinquefoil root, ground part of creeping thyme (thyme) , sugar syrup, color, aqueous-alcoholic liquid, according to the invention, additionally contains anise fruits, buds of unblown clove flowers, coriander fruits, cinnamon, nutmeg, peony root, pine buds, wild rosemary, oak bark, linden blossom, natural honey, vanillin, essential lemon oil, essential orange oil, citric acid, with the following ratio of ingredients, kg (liter) per 1000 dal of the finished product:

Rhodiola rosea root and rhizomes - golden root 4.00±0.40 Inflorescences and flowers of common tansy 0.50±0.05 Pine nut 30.00±-3.00 Juniper cones 4.00±-0.40 Leaves and stem tips of Valerian officinalis 0.50±0.05 Leaves and tops of flowering stems of wormwood bitter Yakut 1.00±0.10 Ground part of Scutellaria Baikalensis 0.50±0.05 Calendula officinalis flowers 1.00±0.10 Tops of flowering burnet stems medicinal 1.50±0.15 Great plantain leaf 2.50±0.25 Lingonberry leaf 1.00±0.10 Bearberry leaf 1.00±0.10 Black currant leaf 2.00±0.20 Wild strawberry leaf 1.50±0.15 Raspberry leaf 2.00±0.20 Oat grain 10.00±1.00 Fresh wheat seedlings 2.00±0.20 Reindeer Antler Extract (Epsorin) 0.80±0.08 l Alcoholic juice from fresh lingonberries 250.00±12.5 Alcoholic fruit drink made from dried rowan fruits 100.00±5.00 Alcoholic fruit drink made from dried rose hips 50.00±2.50 Birch buds 0.50±0.05 Elecampane root 1.00±0.10 Leaves and tops of flowering stems of sweet clover medicinal 2.00±0.20 Potentilla erecta root 1.00±0.10 The above-ground part of creeping thyme (thyme) 1.00±0.10 Common anise fruit 1.00±0.10 Buds of unopened carnation flowers 1.00±0.10 Fruits of coriander sativum 1.00±0.10 Cinnamon 0.50±0.05 Nutmeg 1.00±0.10 Evading Peony Root 1.00±0.10 Pine buds 0.50±0.05 Marsh rosemary 0.50±0.05 Oak bark 2.00±0.20 Linden color 0.50±0.05 Natural honey 150.00±15.0 Vanillin 5.00±0.50 Lemon essential oil 1.50±0.015 l Orange essential oil 1.00±0.01 l Lemon acid 15.00±1.50

Finishing the blend

Sugar syrup concentration 65.8 vol. % 921.00±9.2 l Color 800.00±8.00 Rectified ethyl alcohol “Lux” and corrected water (based on strength blend 45 vol. %) rest

A distinctive feature from the prototype is the introduction into the claimed composition for the preparation of an infusion of alcoholic plant raw materials (“balm infusion”), in comparison with the prototype, ten additional spicy-aromatic ingredients (all of them are plants with a high content of bioactive substances - low molecular weight antioxidants): anise (fruits), cloves (buds of unopened flowers), coriander sativum (fruits), cinnamon (fruits), nutmeg, peony evasive (root), pine buds, wild rosemary (leaves), oak bark, linden blossom.

Thus, the claimed composition of an alcohol-containing tonic balm includes forty-four ingredients (including sugar syrup, color and 45 vol.% water-alcohol (ethanol) mixture), forty-one of which are bioactive complexes, including thirty-two from natural plant sources Yakutia, with a high composition of bioactive substances (except for the fruits of coreander, cinnamon, nutmeg, oak bark, linden blossom, vanillin, lemon and orange essential oils, citric acid).

To increase the efficiency of extraction of plant materials, the technological stage of preparing an infusion of alcoholized plant materials was carried out in two steps, preparing balm infusions No. 1 and No. 2.

Accordingly, the composition for the alcohol-containing tonic, medicinal balm “Yakutsky” with increased bioactivity, compared to the prototype, is created as follows.

Example 1

IA technological stage. Prepare an infusion of alcoholized plant materials (infusion of balm No. 1), which includes the following ingredients: anise fruit 1.0±0.1 kg, birch buds 0.5±0.05 kg, valerian root 0.5±0.05 kg , buds of unopened clove flowers 1.0±0.1 kg, elecampane root 1.0±0.1 kg, pine nut 30.0±3.0 kg, coriander fruits 1.0±0.1 kg, cinnamon 0.5±0.05 kg, cinquefoil root 1.0±0.1 kg, common juniper cones 4.0±0.4 kg, nutmeg 1.0±0.1 kg, peony root 1.0 ±0.1 kg, Rhodiola rosea root 4.0±0.4 kg, pine buds 0.5 ±0.05 kg.

The mixture is poured into 47 dal of 70 vol.% aqueous-alcoholic liquid based on the mass of plant raw materials: the volume of liquid is 1:10, infused for 20 days. For better extraction, stir daily. Then the infusions are removed from the sediments; to reduce losses and increase the yield of infusions, the sediments are centrifuged. The remaining raw materials are poured with aqueous-alcoholic liquid with a strength of 50 vol.%, kept for 10 days with daily stirring. The infusions of the second bay are used to prepare the next batch of Yakutsky balsam.

IB technological stage. Prepare an infusion of alcoholized plant materials (balm infusion No. 2), which includes the following ingredients: wild rosemary 0.5±0.05 kg, lingonberry leaf 1.0±0.1 kg, wild strawberry leaf 1.5±0.15 kg, leaves and tops of flowering stems of sweet clover 2.0±0.2 kg, oak bark 2.0±0.2 kg, flowers of calendula officinalis 1.0±0.1 kg, tops of flowering stems of burnet 1.5± 0.15 kg, linden blossom 0.5±0.05 kg, raspberry leaf (2.0±0.2 kg), oat grain (10.0±1.0), inflorescences and flowers of common tansy (0. 5±0.05), fresh seedlings of wheat (2.0±0.2 kg), large plantain leaf (2.5±0.25), leaves and tops of flowering stems of Yakut wormwood (1.0±0. 1 kg), black currant leaf (2.0±0.2 kg), above-ground part of creeping thyme (1.0±0.1 kg), bearberry leaves (1.0±0.1 kg), above-ground part Baikal skullcap (0.5±0.05 kg).

The mixture is poured with 32.5 (65.0) dal 70 vol.% aqueous-alcoholic liquid based on the mass of plant raw materials: volume of liquid = 1:10, infused for 20 days. For better extraction, stir daily. Then the infusions are removed from the sediments; to reduce losses and increase the yield of infusions, the sediments are centrifuged. The remaining raw materials are poured with aqueous-alcoholic liquid with a strength of 50 vol.%, kept for 10 days with daily stirring. The infusions of the second bay are used to prepare the next batch of Yakutsky balsam.

II technological stage. At the same time, alcoholized lingonberry juice is prepared by pouring lingonberry juice obtained by pressing fresh berries (250±12.5 kg) with alcoholic liquid 45 vol.% 1:1.

III technological stage. The preparation of alcoholized fruit drinks from dried fruits is carried out by infusing a water-alcohol mixture. Dried rowan berries (100±5 kg) are poured with aqueous-alcoholic liquid with a strength of 50 vol.% in a ratio of 1:3; dried rose hips (50±2.5 kg), poured with aqueous-alcoholic liquid with a strength of 50 vol.% in a ratio of 1:5; keep the first floods for 10 days with daily stirring, then drain the liquid part and pour the fruits with an aqueous-alcoholic liquid in an amount equal to the amount of drainage: rowan 45 vol.%; rosehip 45 vol.% and again infusion for 10 days with daily stirring. Next, the fruit drinks from the first and second drains are mixed.

IV technological stage. In a blending container, the following are mixed at the rate of production of 1000 dal of tonic balm “Yakutsky”: 800 ± 8.0 l of infusion of balm No. 1, 1040.0 ± 10.4 l of infusion of balm No. 2, 230 ± 3.0 l of alcoholized lingonberry juice , 380 ± 4. l of alcoholized rosehip fruit drink , 460 ± 5.0 l of alcoholized red rowan fruit drink , 0.8 ± 0.08 l of reindeer antlers extract obtained using technology, the patent holder of which is JSC FAPK "Yakutia" [RF patent No. 2771686 , priority dated 10/21/2021, publ. 05/11/2022]; 150±15.0 kg of natural honey, 5.0±0.05 l of vanillin, 1.5±0.015 l of lemon essential oil, 1.0±0.01 l of orange essential oil, 920 ± 9.0 l of sugar syrup concentration 65.8% , 800±8 kg of color, 15±1.5 kg of citric acid, rectified ethyl alcohol “Lux” and corrected water (based on the blend strength of 45%).

V-th technological stage. The blend is stirred, brought to a volume of 1000 dal and a strength of 45.0 ± 0.2 vol.%, settled, filtered and served for bottling.

The resulting balm has the following analytical indicators: strength 45 vol.%; the content of the total extract is 15.7±0.1 g/100 ml (see table).

Organoleptic characteristics: color – dark brown with a reddish tint; taste – burning, tart; The aroma is complex, harmonious with spicy tones. The organoleptic assessment of the quality of the Yakut balsam, made on a 10-point scale, is 10 points.

Table 1 shows the content of low molecular weight antioxidants - a parameter reflecting the biological activity of the balm in the claimed composition in relative units compared to the prototype.

To achieve optimal efficiency of extraction of biologically active substances at IA and IB technological stages of preparing alcoholized plant infusions of balm No. 1 and No. 2, we varied the ratio of the mass of ingredients of plant raw materials to the volume of 70 vol.% aqueous-alcoholic liquid poured at IA and IB technological stages (examples 2 and 3).

Example. 2. When preparing infusion of balm No. 1 (technological stage IA), the mixture is poured with 23.5 dal of 70 vol.% aqueous-alcoholic liquid based on the mass of plant raw materials: volume of liquid = 1:5, and infused for 20 days. When preparing the infusion of balm No. 2 (technological stage IB), the mixture is poured with 16.25 dal of 70 vol.% aqueous-alcoholic liquid, also based on the mass of plant raw materials: volume of liquid = 1:5, and infused for 20 days.

At the same time, the strength of the resulting balm (45 vol.%), organoleptic indicators (color is dark brown with a reddish tint; the taste is pungent, tart; the aroma is complex, harmonious with spicy tones) and the organoleptic assessment of the quality of the Yakut balm, made by 10- The point scale (10 points) did not change. The concentration of extractive substances (in mass%) decreased by 9%, and the content of low molecular weight antioxidants (in relative units) decreased by 21% (see Table 1). The results obtained indicate that a 2-fold decrease in the ratio of the volume of 70 vol.% aqueous-alcoholic liquid to the mass of ingredients of plant raw materials at technological stages IA and IB of the preparation of alcoholized herbal infusions of balm No. 1 and No. 2 leads to a significant decrease in the efficiency of extraction and , as a consequence, to a decrease in biological activity, the indicator of which is the content of low molecular weight antioxidants in the final product.

Example 3. When preparing an infusion of balm No. 1 (technological stage IA), the mixture is poured with 94 dal of 70 vol.% aqueous-alcoholic liquid based on the mass of plant raw materials: volume of liquid = 1:20, and infused for 20 days. When preparing the infusion of balm No. 2 (technological stage IB), the mixture is poured into 65 dal of 70 vol.% aqueous-alcoholic liquid, also based on the mass of plant raw materials: volume of liquid = 1:20, and infused for 20 days.

At the same time, the strength of the resulting balm (45 vol.%), organoleptic indicators (color is dark brown with a reddish tint; the taste is pungent, tart; the aroma is complex, harmonious with spicy tones) and the organoleptic assessment of the quality of the Yakut balm, made by 10- The point scale (10 points) did not change. The concentration of extractives (in mass %) increased by 1.3% (within the error), and the content of low molecular weight antioxidants (in rel. units) increased by 2.8% (within the error; see Table 1). The results obtained indicate that a 2-fold increase in the ratio of the volume of 70 vol.% aqueous-alcoholic liquid to the mass of ingredients of plant raw materials at technological stages IA and IB of the preparation of alcoholized herbal infusions of balm No. 1 and No. 2 does not lead to a significant increase in extraction efficiency and, as a consequence, to a significant increase in biological activity, the indicator of which is the content of low molecular weight antioxidants in the final product.

Table 1. Content of low molecular weight antioxidants (rel. units) and extractive substances (wt.%) in the claimed composition (example 1), prototype, with a 2-fold reduction in the ratio of the mass of plant ingredients/volume of 70 vol.% aqueous-alcoholic liquid poured at technological stages IA and IB (example 2) and when it is increased by 2 times (example 3).

Composition of tonic balm Content of low molecular weight antioxidants, rel. units ^*) Concentration of extractive substances, wt.% Prototype 1.00 ±0.07 11.4±1.1 Composition of ingredients for alcohol-containing tonic balm “Yakutsky” (example 1) 1.45±0.09 15.7±1.5 Composition of ingredients for alcohol-containing tonic balm “Yakutsky” (example 2) 1.15±0.09 14.3±1.4 Composition of ingredients for alcohol-containing tonic balm “Yakutsky” (example 3) 1.49±0.09 15.9±1.5

^*) The content of low molecular weight antioxidants was determined according to the method “Content and activity of low molecular weight antioxidants in food and medicinal plants”, V.A. Volkov, N.N. Sazhina, P.M. Pakhomov, V.M. Misin. // Chemical physics, 2010, volume 29, no. 8, p. 73-77.

A comparison of the results given in Table 1 shows that almost maximum extraction is achieved already with a ratio of the mass of plant ingredients/volume of 70 vol.% aqueous-alcoholic liquid poured at technological stages IA and IB of 1:10. This ratio was included in the description of the technology for preparing the claimed composition.

Claims (6)

Composition of ingredients for an alcohol-containing tonic balm, including the root and rhizomes of Rhodiola rosea - golden root, inflorescences and flowers of tansy, pine nuts, juniper cones, leaves and tops of stems of valerian officinalis, leaves and tops of flowering stems of Yakut wormwood, the ground part of Skullcap Baikal, Calendula officinalis flowers, tops of flowering stems of burnet, large plantain leaf, lingonberry leaf, bearberry leaf, black currant leaf, wild strawberry leaf, raspberry leaf, oat seed, fresh wheat sprouts, reindeer antlers extract - Epsorin, alcoholized juice from fresh lingonberries, alcoholized fruit drink from dried rowan fruits, alcoholized fruit drink from dried rose hips, birch buds, elecampane root, leaves and tops of flowering stems of melilot officinalis, cinquefoil erect root, ground part of creeping thyme (thyme), sugar syrup, color , an aqueous-alcoholic liquid, characterized in that it additionally contains common anise fruits, buds of unblown clove flowers, coriander fruits, cinnamon, nutmeg, peony root, pine buds, wild rosemary, oak bark, linden blossom in the following ratio of ingredients, kg/1000 dal of finished product: Rhodiola rosea root and rhizomes - golden root 4.00±0.40 Inflorescences and flowers of common tansy 0.50±0.05 Pine nut 30.00±3.00 Juniper cones 4.00±0.40 Leaves and stem tips of Valerian officinalis 0.50±0.05 Leaves and tops of flowering stems of wormwood bitter Yakut 1.00±0.10 The ground part of the Baikal skullcap 0.50±0.05 Calendula officinalis flowers 1.00±0.10 Tops of flowering burnet stems medicinal 1.50±0.15 Great plantain leaf 2.50±0.25 Lingonberry leaf 1.00±0.10 Bearberry leaf 1.00±0.10 Black currant leaf 2.00±0.20 Wild strawberry leaf 1.50±0.15 Raspberry leaf 2.00±0.20 Oat grain 10.00±1.00 Fresh wheat seedlings 2.00±0.20 Birch buds 0.50±0.05 Elecampane root 1.00±0.10 Leaves and tops of flowering stems of sweet clover medicinal 2.00±0.20 Potentilla erecta root 1.00±0.10 The above-ground part of creeping thyme - thyme 1.00±0.10 Common anise fruit 1.00±0.10 Buds of unopened carnation flowers 1.00±0.10 Fruits of coriander sativum 1.00±0.10 Cinnamon 0.50±0.05 Nutmeg 1.00±0.10 Evading Peony Root 1,000.10 Pine buds 0.50±0.05 Marsh rosemary 0.500.05 Oak bark 2.00±0.20 Linden color 0.50±0.05 Natural honey 150.00±15.0 Vanillin 5.00±0.50 Lemon acid 15.00±1.50 Color 800.00±8.00, and also with the following ratio of ingredients, l/1000 dal of the finished product: Reindeer Antler Extract - Epsorin 0.80±0.08 Alcoholic juice from fresh lingonberries 230.00±3.0 Alcoholic fruit drink made from dried rowan fruits 460.00±5.00 Alcoholic fruit drink made from dried rose hips 380.00±4.00 Lemon essential oil 1.50±0.015 Orange essential oil 1.00±0.01, finishing of the blend Sugar syrup concentration 65.8 vol. % 921.00±9.2 Rectified ethyl alcohol “Lux” and corrected water (based on strength blend 45 vol. %) rest