RU2567768C2 - Method of alloy production based on titanium from water suspension of particles of ore containing compounds of titanium, and device of its implementation - Google Patents

Abstract

FIELD: metallurgy.

SUBSTANCE: method includes generation of magnetic fields applied to portions of processed raw material, metals restoration from ores upon continuous mixing of the raw material mass with further accumulation and formation of product in form of ring columnar monocrystal comprising intermetallic compound selected from TiAl₃, TiFeAl₂, TiAl₂Fe, TiFe₃, and its unloading. Water suspension comprising particles of ore with dispersion within range 0.001-0.008 mm and in amount of 40-70% of water suspension volume is used as input raw material mass. At that the sawlike magnetic fields with intensity 3·10⁴÷1.5·10⁵ A/m and oscillations frequency 20-80 pulses per 1 minute are used as magnetic fields. Restoration is performed with gas jets supply to the raw material layers, the jets contain compressed atmosphere air and carbon as deoxidant, it present in compressed gases. Invention proposes also the device for this method implementation.

EFFECT: production of alloy directly from ore.

2 cl, 5 dwg, 3 ex

Description

The invention relates to those areas of non-ferrous metallurgy in which metal alloys containing titanium are processed, as well as others that are part of the final products synthesized using such technologies, elements that are present in the form of corresponding compounds in the composition used in the manufacturing process of these alloys, raw materials, as well as devices that provide the ability to carry out the above processes.

At the present time, a technical solution is known, in the implementation of which a multicomponent titanium alloy containing in its composition including the above elements - iron, aluminum; in the process of carrying out its manufacture, a number of additional operations take place, including preliminary preparation of the charge used to obtain this final finished product, and in addition, the formation of the consumable electrode necessary for producing this multicomponent alloy.

Subsequently, upon receipt of such a titanium alloy, a joint melting of a previously manufactured electrode and a previously obtained raw material charge in a vacuum arc furnace is performed.

Used for the implementation of such a known method noted here in the process of forming the above multicomponent alloy, the raw material charge is prepared from titanium waste (see patent RU No. 2425164 "Secondary titanium alloy and method of its manufacture" C22C 14/00, published on 02.27.2011) .

Thus, when applying the above-mentioned known technical analogue, in the end, it is possible to synthesize titanium-containing alloys having stable and strictly regulated rolling properties obtained during processing.

However, due to the presence of the action of the features of its implementation listed above, this well-known solution will necessarily be accompanied by the following significant disadvantages.

First of all, the very necessity of carrying out the operation of remelting the consumable electrode and the initial charge in a vacuum arc furnace inevitably leads to an increase in costs used in the manufacturing process of this known alloy of electrical energy. The presence of the action of such a circumstance has an extremely negative impact on all technical and economic indicators characterizing the degree of efficiency of the process used in processing the feedstock, in the case of using this well-known technical solution directly in the current industrial production.

In addition, in the process of its implementation it is not possible to ensure the formation of the necessary set of physical factors that objectively act on the processed raw material, the influence of which would ensure the receipt of a finished finished product from it, in the form of a structural formation having, for example, a ring shape columnar single crystal, consisting of only intermetallic compounds that are part of it, and containing only titanium in its volume and other necessary my metals. The presence of this circumstance, in turn, does not make it possible to sharply improve the quality characteristics of this new metal structural formation formed by such processing with respect to similar alloys, but synthesized using other “classical” methods for their manufacture known at the present time.

In another, also known, method for producing an alloy based on titanium containing, among others, aluminum and iron, the following necessary additional technological methods are used to increase the technical parameters of the final product formed with its use. The use of the latter, ultimately, allows to increase the physicomechanical characteristics of the final product produced using this well-known technology.

First, the manufacture of the aforementioned multicomponent alloy is carried out using the so-called “aluminothermic method”, as well as using a specially formed multicomponent ligature during its execution.

In the course of the processing carried out with its help, the raw material passes through at least two “remelting”. One of them is made using the “skull - consumable” method, and the second is performed in a separate vacuum arc furnace. The use of all of the above and newly introduced into this technology technical distinctive essential features in this well-known prototype solution provides a certain increase in the physicomechanical indices of the final product manufactured in accordance with this method obtained by processing the initial raw material.

So, for example, the use of all the above additional technological methods when processing raw materials using the above-mentioned known method of manufacturing a multicomponent alloy, allows to increase the tensile strength of the specimen-part formed with its use, to a value of 1293 MPa, and bring the viscosity index to 66.3 MPa · m (see patent RU No. 2463365 "Method for producing an ingot of pseudotitanium alloy containing (4.0-6.0%) Al; (4.5-6.0%) Mo; (2.0-3.6 %) V; Cr (0.2-0.5%); Fe (0.1-2.0%). C22C 14/00; C22B 9/20, published October 10, 2012 - ( hereinafter referred to as the "prototype").

However, as in the previously described other well-known technical solution, when performing this method of producing a multicomponent alloy based on titanium containing aluminum and iron among its main components, a number of disadvantages characteristic of all these known methods are revealed, inevitably identified in the implementation process.

Thus, when processing raw materials using this well-known prototype technology, i.e. upon receipt of the aforementioned titanium alloy, the need arises to perform a preliminary “remelting” of the used raw material, which sharply increases the level of total energy resources needed to meet the corresponding production needs and directly serving its corresponding industrial needs, necessary for all this.

In view of the presence of “special” specific features of the implementation of this known prototype method, for example, such as the need to perform the latter using high-temperature melts that are part of the resulting above-mentioned final product and constitute this alloy of the starting metals used in the implementation of the above raw materials processing equipment, as well as auxiliary technological systems serving its functioning, are distinguished by a high degree of complexity, and therefore nachitelnoy its value.

This well-known prototype technology also has a "strikingly straightforward" irrationality of its organization, used in the process of its implementation, and its own technical structure.

So, for example, its implementation is carried out with the obligatory involvement of a significant number of metallurgical processes necessary to obtain a multicomponent titanium alloy. That is, during its implementation, the initial charge is formed first, then the consumable electrode, and after all this, finally, the final final remelting of the initial raw materials is performed at least twice.

After all this, obtained in the above manner, the ingot is also subjected to additional heat treatment. However, the use of the entire set of the above from significant distinctive technical features, the presence of which as a result interferes with the possibility of widespread industrial application of the above method, ultimately does not ensure the achievement of the set and necessary ultimate goal. Namely, the application of this well-known processing technique does not allow to obtain a finished final product having sufficiently high intrinsic physical and mechanical characteristics.

That is, when using this well-known technical solution, the prototype, nevertheless, it is not possible to synthesize a titanium alloy with layers forming its volume, which would be formed in the form of a combination of the last crystal lattices, the main nodes of which would be obtained directly from the original raw materials corresponding to and included directly in the last titanium-based intermetallic compounds, and the finished final product produced from the initial raw material charge would be an annular column This is a single crystal with a specific and predetermined set of its physicochemical and geometric parameters.

The aim of the invention is the formation during the proposed method for producing an alloy based on titanium, aluminum, iron, a set of necessary conditions; the presence of the action of which would make it possible to synthesize from the used initial ore raw material during its processing, a wide range of intermetallic compounds consisting of the above elements and creating, when constructing their own aggregate crystal lattice, a ring columnar monocrystalline formation, which should also have high intrinsic quality physical and mechanical characteristics, as well as a decrease in the degree of constructive complexity used during the proposed processing technology of this device itself.

Achieving the above goal is ensured by the presence of action when performing the proposed method the following set of significant distinctive technical features.

The first thing to note is that the proposed method necessarily includes, in the course of its implementation, placing a preformed and containing titanium, aluminum and iron compounds of the initial raw material mixture in the internal volume of the device used for its processing. In the above device, after the loading operation of the feedstock is completed, physical fields are also generated that are superimposed on all zones in its cavity containing the processed raw material placed in them. Using these physical fields, the process of restoring the components of the alloy components from the ore material containing their initial compounds is carried out.

The use of these processing physical fields, in the end, ensures the connection of the individual reduced elements included in the composition of the raw material mixture used in the processing into an integral monolithic metal structure - an alloy.

Secondly, you should also pay close attention to the fact that in the process of implementing the proposed method, the mixing of the components of the initial volume of the raw material and included in the last of the layers during its processing is also mandatory. At the same time, the finished product is also accumulated in the device area located in the impact zone of the above-mentioned physical fields used in the processing of raw materials. At the end of the processing process, the finished monolithic formation is also unloaded from the cavity of the device used.

As the containing compounds of titanium, iron, silicon, feedstock when performing the proposed technology, water suspension obtained by introducing into a predetermined volume of water with subsequent distribution of a mixture of titanium, iron and aluminum particles in it is used. The dispersion of the solid components included in the composition of the latter is in the range of 0.001-0.008 mm, and their amount in the total volume of this aqueous suspension corresponds to a value of 40-70%.

The initial ore rocks used to obtain the above raw material mixture form the latter when they are contained in its composition - 33-34% for titanium, 33-35% for iron and aluminum, respectively, the rest, up to 100%.

The alloy obtained at the end of the processing process itself is formed in the form of an annular columnar single crystal consisting of TiAl ₃ or TiFeAl ₂ or TiAlFe ₂ or TiFe ₃ intermetallic compounds.

As the physical fields acting on the raw materials, “sawtooth” magnetic fields are used, the intensity of which is 3 × 10 ⁴ ÷ 1.5 × 10 ⁵ A / m, and the oscillation frequency corresponds to a value of 20-80 units. per minute, and the “processing” clusters formed by these physical fields, consisting of lines of force belonging to them, have a configuration as close as possible to the outline of the spatial formation obtained by rotating a elongated rectangle that rotates about its own longitudinal axis of symmetry.

In this case, the process of forming the finished end product in the form of an annular columnar single crystal is carried out on a metal spacer rod, which acts as a “seed”, located directly in the center of the mobile working chamber used to place the feedstock. On its lateral outer surface at the very first stage of processing, an annular layer is first formed, which is represented by slag waste obtained during processing. Then on this kind of “substrate” the necessary finished finished product is synthesized.

As mentioned earlier, the formation of the latter is carried out in the form of an annular columnar single crystal, which includes the above-mentioned intermetallic compounds consisting of titanium, aluminum, and iron.

When processing using the proposed method of its implementation, the raw materials used are preloaded into a working chamber sealed from the rest of the device’s body.

The latter, when executed, also makes a reciprocating movement along the body cavity using the round-trip directions, and also makes angular rotations relative to its own longitudinal axis of symmetry.

The above-mentioned angular rotations that make up this camera elements are first performed in a circular path, the outline of which coincides with the clockwise movement on the dial - on the initial direct segment of the movement performed by it, and in the opposite direction, respectively, at the end of the processing cycle, the opposite.

The very arrangement of the areas of formation of the "sawtooth" magnetic fields was made using three, or a multiple of this number, another number of spiral-shaped installation cylindrical lines. The latter “encircle” the outer surface of the device’s body, in the cavity of which the reciprocating movement of the working chamber is loaded with the mass of processed raw material loaded into it.

In addition to all of the above, in the implementation of the proposed technology, the formation zone of technological "sawtooth" magnetic fields that its working chamber periodically moving in the cavity of the device’s body periodically intersects, is removed from each other by the same mounting distance, and the number of areas in which the generation of the latter is carried out, ranges from nine to eighteen units per each spiral-shaped enclosing enclosure of the mouth used for their placement rostoy trajectory.

The process of restoration of elements included in a multicomponent alloy is carried out by supplying the layers of ordinary atmospheric air to the components of the processed volume of raw materials.

As the element that provides the fulfillment of this action, the reducing element uses carbon present in the composition of the gases containing this component, which, in turn, form the jets themselves blown through the working chamber of the above product.

The mixing of the volume of the raw material used to obtain the alloy is carried out in the process of moving it in the internal volume of the movable working chamber, which makes a “screw” reciprocating movement in the direction from the rear end of the device to its front part, and then vice versa. The above operation is performed by crushing and transferring from one region of the volume of the cavity of the working chamber to another constituent of the processed mass of its individual microports, which proceeds under the influence of blows created by the intersecting jets of compressed air supplied to the latter. The receipt of this product to the above zones is carried out under excess pressure, the value of which corresponds to a value of 0.4 ÷ 6.0 kgf / cm ² .

Themselves of this kind, "piercing" the material layers of the raw material jet stream flows are formed using specially provided for this action blowing elements - nozzles. The latter are also evenly fixed on three installation spiral lines, which are laid between the corresponding turns of the curves used to place the magnetic generators.

The blasting elements themselves, which ensure the supply of pressures consisting of the above product and directed directly to the volume of the feedstock of this kind of “crossing” flows, have both tangential and radial tilt angles of 30-45 ° with respect to the surface on which this processed material at a given time and is located.

The loading of the feedstock used for processing, as well as the unloading of the finished columnar ring single crystal at the end of the processing process, is carried out in a separate, removable cap compartment connected to the fixed main body of the device designed to perform the above technological transitions.

The device itself, designed to implement a method for producing an alloy based on titanium, iron and aluminum from an aqueous suspension, particles containing compounds of these ore elements, includes a body consisting of two parts. One of the parts of this case is removable and is made in the form of a cap removable cap that fits into the fixed main cylindrical shell-body. Docking is carried out using annular flat connecting flanges, and the length of the fixed element indicated above the assembly, is 80-85% of the total corresponding dimension of the latter. The rest of its length falls on its removable part - a cap. In addition, a movable working chamber is installed in the cavity of the fixed part of the device casing, kinematically connected by means of a travel roller attached to the components of the last parts, with an external drive for transmitting movement, the presence of which ultimately allows its reciprocating movement along the internal cavity of this assembly the device’s body, in the direction there and back, with simultaneously rotating its structural elements relative to its own longitudinal axis sim metrics.

The direction of such rotation changes to the opposite at the time when the mobile working chamber is returned from the final position it occupied by this node to its original initial position.

This working chamber itself is formed by the left and right “piston-like” restrictive cheeks fixed on the roller. Between the above parts of the composite working chamber, a spacer rod-seed is used, which is used to deposit the finished product obtained in it on its lateral outer surface.

At the same time, the cheeks of the working chamber that are moved inside the cavity of the assembly case of the device perform the functions of a double piston and have sealing seals on their outer side surface.

It should also be noted that focusing magnetic nozzles are passed through the walls of the fixed part of the housing, as well as blowing nozzles for forming compressed air jets entering the internal volume of this component of the assembly unit of the device, and in addition, accordingly, clusters of magnetic lines of force lines generated by the focusing nozzles having the configuration of “logs” elongated along a straight line of radial cylindrical rays.

The arrangement of both those and other structural elements of this device is made on cylindrical spiral lines encircling its body.

The number of such kind of installation curves used to fix each such part is three, or any other number that is a multiple of this value, their units. The number of magnetic loops placed on each of these curved paths, which include focusing nozzles, is from nine to eighteen pieces.

Evenly arranged on spirals similar in shape and using the same number of spirals, located in turn between the turns used to arrange the magnetic contours of the curved installation lines, the blowing nozzles have both radial and tangential angles of 30-45 ° with respect to to the surface of the housing on which they are mounted.

The working elements of the processing magnetic generators themselves are made in the form of plates of magnetically conductive material stacked together, with the formation of an F-shaped magnetic circuit during their installation.

In the volume of the individual components of this assembly, three electrical windings of the coil are placed, both in the left and right halves of the circuit.

The total number of such coil windings placed in each circuit is thus six. The electrical elements of the magnetic circuit noted above fulfill the function of solenoids in it.

Each such winding coil is connected to the corresponding "pseudophase" of an external source of electrical power supply. The arrival of sets of electric pulses generated by this external power source, each of which has the shape of a “tooth saw”, is made to separate solenoids with an angular displacement of these signal packets relative to the same, but supplied to adjacent windings-coils, as well as to generators placed on adjacent mounting spirals.

The value of the above angular displacement is a value of 120 °. In the lower horizontal transverse crossbar of each F-shaped magnetic generator, that is, in the recess in it for this purpose, the shank of the cylindrical focusing nozzle is pressed in, the opposite end of which goes into the mounting hole made in the installation sleeve, passed through the walls of the fixed part of the housing. The aforementioned nozzle also has a cavity in the form of a cavity with the configuration of a spatial rotation hyperboloid formed on its lower end part and focusing the magnetic field lines.

The “curvilinear recesses” on the inner side surface of its cavity, obtained in places of passage through the walls of the housing of the mounting sleeves with focusing magnetic nozzles, as well as blowing nozzles, are equipped with “smoothing” washers. The latter are made either of magnetic conductive powder pressed into the volume of these recesses - in the case of placement of magnetic focusing nozzles there, or in the form of split petal membranes of elastic rubber located near the outlet openings of the blowing nozzles.

In addition to all of the above, exhaust pipes are mounted in the left and right halves of the fixed casing for the discharge into the external atmosphere of the excess gas accumulated in the working chamber, equipped with pressure reducing valves. The triggering of these elements is carried out in the case when the pressure value of the volatile compounds formed in the volume of the mobile working chamber exceeds its value specified by the processing technology.

Again, it should be noted that at the points of intersection of the body of these nozzles with the lateral inner surface of the fixed body, plastic perforated smoothing washers are mounted, which ensure the smooth flow of the sliding process in these areas, which are part of the working chamber of its right and left cheek-pistons, as well as the output through the through holes in the above details through the perforations of the excess gas volumes filling it.

It is also necessary to point out that in the upper part of the removable cap of the device there is a loading hopper, the internal volume of which is connected through the through sunroof, made in the same part of the device’s body, to the cavity located underneath the movable working chamber, occupying at the time of its filling the initial "starting" position before the start of the processing cycle.

Based on all the above features of the proposed method, as well as the fact that there is an application of the entire set of the previously mentioned significant structural “distinctive” features in the device used to implement this technology, we can finally conclude that the influence of the latter allows indigenous way to change the nature of the process of formation of a multicomponent refractory alloy based on titanium, iron and aluminum when processing raw materials evyh materials.

In connection with the fact that the above circumstances exist, the previously mentioned technology begins to acquire the following characteristic differences inherent only to it. First, the latter should definitely include the fact that the very initial stage of the implementation of the proposed method includes the stage of the so-called "ultrafine grinding" of pieces of initial ores containing compounds of titanium, iron and silicon.

During its implementation, any known methods of crushing bulk material known in industrial production, for example, performed using conventional ball mills, are used. When applying the above device to achieve this goal, the pieces of the initial raw material used in the proposed technological process were ground using the latter to obtain ore particles from them having overall dimensions in the range from 0.001 to 0.008 mm.

The implementation of the above operation to "grind" large lumps of rock and further provides the possibility of forming from the thus obtained "powder", consisting of these small ore particles, containing, in turn, compounds of titanium, iron and aluminum, a kind of "dry residue ", Entirely composed of the above solid feed components.

The multicomponent "dry residue" used in the processing process includes 33-35% titanium ore, 33-35% iron, and aluminum - the rest, up to 100%.

The above ore components of such an initial mixture immediately before the crushing operation of the ore lumpy material used in its composition passes, respectively, through the preliminary dosage stage, at the end of which the further supply of the starting materials necessary for processing is guaranteed in a predetermined, defined mutual ratio, ensuring the preservation of their technological percentage in the amount of cheese used in its implementation oh. This technological transition itself, that is, this preliminary dosage, is most often carried out by weighing the ore components included in the raw material mixture (that is, titanium, iron and aluminum rocks, respectively).

It is from this “kind of powder” obtained by conducting “ultrafine grinding” that consists of fine particles of titanium, iron and aluminum rock that the formation of the material used in the future for processing raw materials into a multicomponent alloy is made, liquid, homogeneous, not stratified into separate components for a sufficiently long period of time, a mud-like mass - that is, the aqueous suspension itself is made.

In order to synthesize the latter, it will only be necessary to add the required amount of water (30-60% of the total mass of this solid material) to the "powder" volume, which consists of small particles of all the previously mentioned ore rocks, thus obtained. After performing such an action, the two-component substance thus obtained (a mixture of solid particles plus water) is thoroughly mixed.

For the implementation of this technological transition can be used any, designed to achieve the above goals, industrial equipment, for example, an ordinary paddle mechanical mixer. A homogeneous “mud-like” portion of the volume of the aqueous suspension formed at the end of its holding, consisting of these two components listed above, is then placed in the cavity of the loading hopper 2, which is part of the removable part of the housing used in the processing process of this device itself. From the cavity of the loading hopper 2, a water suspension through a through hole “B” in the removable cap 4 (see Fig. 1) by gravity enters the interior of the mobile working chamber, located directly below the loading hopper, and formed by restricting it to the right and on the left side by the cheeks-pistons 3, which are part of such an assembly as mentioned above. Upon completion of the operation of the complete withdrawal of all previously filled the volume of the feed hopper 2 of the raw material mass 1 into the above cavity of the mobile working chamber, the following actions are performed.

Immediately and at the same time they are connected to external power sources that form and feed packets from the “sawtooth” electrical pulses, all of which are part of the F-shaped magnetic generators 11, their coil windings 13.

The roller 8 is set in motion and causes the structural elements making up the working chamber to move from the initial “left” initial position to the very front “right” part of the fixed half of the device assembly 6. Simultaneously with the execution of the above translational motion at a speed of 40-60 mm / min, the details of the working chamber also carry out additional angular rotations relative to its own longitudinal axis of symmetry (2-4 rpm). In addition, to the external supplying air under excess pressure of the line (0.4-6 kgf / cm ² ) connected to the spirals "D" passing between the corresponding turns of the installation curves "G" lines with the generators 11 fixed to them, blowing nozzles 10.

Thus, starting the treatment cycle, the working chamber with the processed raw material 1 caught between the “piston-shaped” cheeks 3 forming it, is pushed “to the right” from the cavity of the cap removable cap 4 and passes after this action, directly into the internal volume of the fixed body 6 (see Fig. 1). As the depth of penetration of the mobile working chamber directly into the above-mentioned cavity of this collection unit increases, the raw material 1 placed in the last raw material 1 is subjected to a constantly increasing force “pressure”, which is implemented as “penetrating” the layers of the initial product “intersecting” among themselves into the masses produced from the nozzles 10 of compressed air, and from the side generated by the focusing nozzles 14 of the magnetic "beam" cylindrical flows "K" (see figure 3). Due to the fact that all the above structural elements are placed on the spirals “G” and “D” encircling the outer side surface of the housing 6 (3 units + 3 units), the internal cavity with a “turtle” speed crawling along the body 6 devices of the working chamber with the raw material 1 placed there being processed into a multicomponent alloy, when performing its movement, inevitably falls into the zone of influence of all these power energy formations listed above.

The above-mentioned spatial technological systems, consisting of the individual individual “physical” elements forming the last, have the same, strictly preserved own configuration, oriented in a certain way relative to the trajectory line that the working chamber lays when performing its translational “screw” movement along the internal surface of the precast device enclosures. That is, taking into account the fact of the presence of the action of the above circumstances, we can confidently assume the following: after a certain, rather insignificant period of time, in a space separating the left and right “piston-shaped” cheeks 3 of this assembly unit, a whole set of physical factors formed using all of the above and used as part of the design of the proposed device, power spiral formations.

Firstly, a mass of processed raw materials 1, covering its bottom, at the moment the working chamber performs such translational movement from the initially occupied last position to the front “right” end of the housing 6, a series of “crossing air strikes” directed at different spatial angles falls.

Such a nature of the flow of action from the side of the air currents formed by the jet nozzles 10 is explained, first of all, by the selected scheme for their installation on the housing 6 (that is, by their placement along the spiral line “D” encircling the device’s body and at “double” tilt angles to the housing surface on which they are fixed).

Feeling a constantly increasing influence from the latter, the compact “heap” of raw materials resting in the very bottom of the working chamber, in the literal sense of the word, is “scattered” into separate, small, previously micro-volumes of it. These new “microscopic” raw material fragments obtained from the starting material are picked up by a peculiar vortex “tornado” “E” formed between the corresponding surfaces of the right and left cheeks 3, and after that they begin to circulate forcibly given by its action in the circuits creating such a spiral flow and generated using nozzles 10, constituting this gas formation and entering into it, its individual jets.

It should also be remembered that due to the ongoing and ongoing application of the aforementioned and consisting of such airborne “attacks” generated directly in the processing zone, they are torn off and distributed in all its constituent parts of the working chamber to its individual areas, the smallest portions of the original of material 1 will inevitably be converted into aerosol bubbles formed from small air gas formations, as well as films of the liquid that covers them from the outside, and also sticks directly to its surface -macroscopic particles of gangue.

As already noted above, almost the entire volume of this type of aerosol foam obtained in the manner described above continues to flow continuously between the cheeks 3 bounding the cavity of the mobile working chamber, and directed along a kind of “orienting” spiral set by the vortex stream “E”, as if forced circulation .

The previously noted nature of the transfer of the constituents of this “aerosol” cloud of layers is protected throughout the entire period of time during which the working chamber is moved in the device casing 6 in a round-trip direction.

In the process of performing this previously noted forced and artificially provided circulation, previously obtained in the cavity of the “working mass” of the “foamed mass” of the “aerosol bubbles”, ore microparticles placed on them necessarily “run” against the body cavity 6 piercing “through and through” and, consequently, the regions constituting the separation space between the cheeks 3 of the mobile working chamber, rectilinear cylindrical and radially directed, rotating clusters “K”, at appropriate to the “sawtooth” magnetic fields created in the device.

The presence of a constant action of this circumstance during the processing of raw materials, again again leads to the inevitable emergence of a number of new physical factors that influence and transform the structure of the ore components of the initial product.

In fact, each separately taken kind of “technological” aerosol bubble, in the process of making its own complex spatial movement along a curved three-coordinate trajectory, as it were, “tears” through the “picket fence” facing it, which again consists of separate generatrices arranged in a spatial spiral its "logs", that is, clusters located radially in the cavity of the device, and stretched directly in its constituent zones, moreover, having the configuration n yamolineynyh cylindrical rotating around its axis of symmetry structural formations formed by magnetic lines of force.

Among other things, the “height” of these movements placed directly on the path of such an “aerosol foam” and, as it were, a kind of obstacle to it, are three at once built along the trajectory of the “stockade” it carries out (magnetic generators 11 are mounted on three encircling buildings 6 set spirals “G”), moreover, and continuously changes its own value.

That is, each “power” log included in this kind of “fence” alternately either increases its length, then again resets this parameter to almost zero, and with all this, it also rotates around its own longitudinal axis.

The aforementioned phenomenon occurs due to the fact that the sets of electric pulses sent to the generating magnetic fields solenoids 13 have a “saw-like” shape (see FIG. 5 — pseudophases a, b, c) and are fed with angular displacement relative to each other.

In addition, the individual logs erected on the path of moving individual aerosol bubbles of this kind of "fence" also have mounting displacements relative to the same exact "stockade" used in neighboring, located next to it (pulses applied to solenoids 13 also shifted into each pseudophase a, b, c sent to the solenoids by an angle of 120 ° - see Fig. 5).

The straightness of the outlines formed by the focusing nozzles 14 clusters (cylindrical logs) generated by the contours of 11 magnetic lines is ensured by the use of the so-called concentrating the last grooves "M" as part of this structural element, made in the form of a depression having the form of a spatial rotation hyperboloid (see Fig. 3 )

Based on the foregoing, we can come to the final conclusion that a “three-way” technological complex consisting of the above-mentioned magnetic barriers, some elements of which also change their height periodically, erected through the erected directly on the trajectory of their movement , and rotate around its axis, the microscopic particles of the processed raw materials inevitably pass through the “continuous downpour" applied directly along them using the entire possible set of spatial directions their influence, as well as continuously changing their own value, generated by the components of these "palisade" logs, powerful force blows.

Under the influence of the latter, the molecules constituting the last of their initial compounds, containing the metals forming the single crystal, are crushed into separate “fragmentary” components, which are included in the composition of aerosol bubbles “attached” to the film coating, microscopic solid particles of the initial ore rock. At the same time, all types of valence bonds forming their elements, both ionic and covalent, earlier connecting them, are broken.

The individual atoms that previously made up their molecules, under the influence of the powerful external continuously performed external energy action indicated above, rearrange their original structure - the electrons they have go from lower orbits relative to their core to higher ones, their spin moments change. As a result of all this, in the final final variant of carrying out such structural adjustment, the atoms - “fragments” located directly in the processing zone and obtained in the above manner are converted into positively or negatively charged particles - that is, into ions. But this kind of technological complex, as if formed from a “vibrating peak” of a kind of jackhammers (this tool is the power flows generated by magnetic circuits 11 and sent through nozzles 14), “breaks”, and also turns into a set of “activated fragments” not only the compounds contained in solid raw particles and processed into the final product of the constituent elements, but also “breaks” the gas molecules in the same zone containing the reducing element, that is, carbon. The latter, as already noted earlier, is part of the gases necessarily present in atmospheric air and its constituent gases (СО ₂ ; СН ₄ ).

The appearance of a carbon ion synthesized in the above manner, that is, a substance with the pronounced properties of a reducing component, in the immediate vicinity of activated fragmented fragments containing charged metal particles activated using powerful magnetic fluxes and provides a “strong” compound released upon destruction the original molecules, compounds of oxygen atoms, which subsequently instantly form strong valence bonds with the above-mentioned element will restore Lemma and eventually removed from the field of treatment, becoming a new volatile compound gas.

The volumes of gas thus formed leave the cavity of the working chamber at times when it moves through the installation areas of the outlet pipes 18 (Fig. 1) equipped with pressure reducing valves 19. When the latter are actuated, they are configured for a specific and predetermined process overpressure accumulated in the cavity portions of already unnecessary volatile compounds are sent through the upper end of the exhaust pipe 18 directly to the surrounding device, the external atmosphere.

These new components of the alloy being produced in this way themselves are formed directly from the elements necessary for this and recovered from the compounds present therein and create, in the treatment area at the very initial stage of its implementation, microscopic crystallization centers, mainly consisting of the obtained thus the finished product.

Under the influence of the vortex stream continuously circulating in the cavity of the working chamber and the artificially generated vortex there, such “microcrystals” at this, so to say, “starting” processing stage, move in it so far only in the direction from its left cheek 3 to the right one, and then vice versa , as if carrying out at the same time a kind of process of "free swimming" in its rotating spiral jets.

It is necessary to pay additional attention to the fact that when conducting a more detailed consideration of the features of the technology for forming these, as if without any “noticeable” “difficulties” “soaring” in the “tornado” and its constituent air layers, metal "grains - nuclei" of the future single-crystal ring formation, the presence of the fact of the action of another, but very significant circumstance, which greatly facilitates, so to speak, the process itself, is inevitably revealed x smooth appearance on the "white light".

Separated aerosol foam bubbles created there by a spiral hurricane created there, containing microparticles used in ore processing, moving in the volume of a mobile working chamber using a complex set of curvilinear spatial trajectories, repeatedly change their positioning relative to their own three-axis symmetry axes. At the same time, such “foam formations” also constantly shift “here and there”, “here and there”, in different directions from the direction of the alloy components specially carried out in the area of restoration and continuously created in the device itself, necessary to perform the above operation, technological force action, formed in the same processing area, where all these bubbles at a given time themselves are located.

Figuratively speaking, each separate raw material particle of this kind at the time of applying a “powerful” power processing blow exposes one “side” or the other under it, and continuously rotating at the same time, provides an occasion for it to all its own volume components and forming it microlayers of the starting material.

Due to the action of the above-mentioned factor, the processing magnetic fluxes generated in the device acquire the most optimal conditions for free access to all structural structures that make up these solid microparticles, and thereby guarantee the achievement of the highest possible conversion speed of the initial compounds included in the latter, into the desired finished product.

The previously noted free air “planning” of newly arising nuclei formed directly from a multicomponent alloy in vortex-like jet streams continues until, for some reasons that are objectively manifesting themselves, the mass of the latter becomes so significant that the force acting on them the force of gravity will not begin to significantly exceed the aerodynamic lift created by the vortex formation.

This kind of "growth" of small grains of the alloy into larger "larger granules" becomes possible due to the presence of the influence of two immediately, ensuring the inevitable implementation in practice of this factor, simultaneously operating processes.

In accordance with the first of the above, a grain of a multicomponent alloy “flying” in the thickness of an aerosol cloud will inevitably fasten other, smaller solid “ore” particles surrounding it on all its sides, appropriately placed at this moment in time, to the smallest adjacent aerosol bubbles. The latter, encountering a solid “huge” crystalline grain flying “directly in the forehead” at high speed at them, simply “collapse”, throwing out ore microparticles previously attached to the surface of this air bubble and transferred to it. As a result of the completion of a number of such numerous collisions, the outer surface of the crystalline nucleus “floating” in the air flow acquires a kind of “coat” consisting of microporosity scattered around it by other neighboring aerosol bubbles, and as a result of the above action “adhered” directly to him ore breed. Due to the fact that the process of its movement continues to take place in swirling air streams covering the “embryo” from all sides, the latter crosses repeatedly and periodically with its whole body created by installation spirals radially located along the installation spirals used in the device and piercing its clusters of magnetic lines of force of the physical fields generated there, a kind of “cylindrical vibrating fringe” processing and hanging in the volume of the working chamber itself.

The aforementioned processes of conversion contained in the layers of ore rock contained in the adhering to the crystalline nucleus body, consisting of the compounds that make up the alloy of components, continue to be carried out there in accordance with the technological scheme already discussed above. As a result of this, the “enveloping” body of the “grain” transferred by the vortex currents of the “seed coat” element, ultimately turns into a full-fledged metal coating uniformly distributed over the entire outer surface of the latter. Located directly under the very base of this metal film formed from a raw "fur coat", and the "surface" layers of the crystalline nucleus adjacent to it, in this case, they function as a substrate — a seed, on which the process of its growth is carried out. As a result, the alloy crystal “flying” through the cavity of the mobile working chamber, as a result of all this, significantly increases its initial overall dimensions, and, consequently, its volume and its own mass.

Simultaneously with the above-mentioned scheme for the growth of larger metal crystals from any previously formed “germ” fines in the processing zone, there is another, second mechanism for synthesizing similar large-sized structural formations. The latter is carried out as follows. When performing complex spatial displacements in the space bounded by the cavity of the mobile working chamber with small, just newly crystallized metal grains of metal, situations inevitably arise when these microscopic metal “grains” directly collide with each other. Since in the zone of such “mutual collisions”, as a rule, clusters of magnetic lines of force are placed, collected in a “tight” cylindrical beam, that is, there is always a kind of “processing fringe” created by the magnetic circuits 11 and focusing nozzles 14, then the small metal nuclei that "came across" each other, as a result of this, are glued together under the influence of the above-mentioned power "tools", forming as a result a new composite structure. It is quite clear that it has large linear dimensions, relative to those that had the original, constituting its individual formations.

In practice, the above mechanisms for the formation of large-sized granule-like structures from any metallic fines that appeared in the area of raw material processing occur simultaneously and simultaneously, which ensures the transformation of small crystalline "grains" that appear in it into a kind of large-sized structures from those obtained in the zone processing lumpy finished product.

Since the above “combined” formations are no longer able, due to a serious increase in their own weight, to continue the process of “swimming” in the jets of the whirling air flow created in the cavity of the mobile working chamber, the latter fall vertically downward under the influence of gravitational forces and reach the most extreme "lower" horizontal level of its possible subsequent placement in the device. On the outer lateral surface of the seed rod 7, installed directly along the longitudinal axis of symmetry of the device, an annular layer "G" has formed by this point in time (see Fig. 2), consisting of those formed during the direct reduction of metal from its ore compounds “Sticky” slag waste. The latter, as a rule, consist of 80-85% of the volume of slag included in the above “tailings” obtained and accumulated in this zone, i.e. the so-called ferroaluminitanosilicates.

This intermediate layer “Zh” enveloping the outer surface of the seed rod 7 appears there primarily due to the fact that in the central zone of the working chamber aerodynamic forces practically do not act on the particles placed in it, which are created mainly by “peripheral” jets of the swirling swirling through it air flow "E". That is, this seed rod 7 is placed, as it were, in the very "eye of the storm", where the "calm" always reigns. Possessing good “adhesive” ability, small particles of slag waste synthesized in the working chamber under the influence of air flows created in its cavity and directed from its periphery to the center of the air (from the high pressure zone in the region of maximum vacuum) almost always carry out its own radially directional movement, which, ultimately, collects them together and causes the ring layer “G” to “stick together” into the encircling rod-seed 7 (see FIG. 2). The latter has a rather "loose" structure, and subsequently easily disconnects into its component parts when the finished product is removed from the device body, which has the shape of an annular columnar single crystal "And" (see figure 2).

Similar processes take place when receiving in the device the most multicomponent finished product. That is, a part of the strongly “sprouted” crystalline nuclei of the synthesized metal falls vertically downward, falling directly onto the outer surface of the annular layer of “Zh” slag located in the center of the chamber and formed there earlier and getting stuck on its plane in contact with them, creating in this case, as it were, “secondary zones” of the course of further crystallization of the alloy. Once again, particles of the synthesized finished final product that have moved there begin to use these pieces of metal that have previously fallen into the above region as a supporting base substrate, which enables their further growth to occur and, ultimately, to form in the above zones due to the “merging” of all of its individual crystalline “grains” of an integral monolith having the configuration of a columnar ring single crystal, consisting mainly of intermetallic compound.

A somewhat different picture is observed when alloy grains that have increased their own initial mass, due to the action of a complex of negative factors, fly “past the target” —that is, they fall down, bypassing the central seed rod 7, and eventually fail in the lowest region of the fixed body 6.

Once on its very “bottom”, they can either fall directly onto the petals of the split smoothing washer 17 (see FIG. 4), covering the nozzle outlet 10, or onto the surface of a kind of gap separating such distributed over the lateral outer surface of the assembly 6 included in its composition blowing elements 10.

In the first version, a “blasting” stream of compressed air at a sufficiently high pressure, bending the radial petals of the smoothing washer 17 to the side (see Fig. 4), immediately throws a “grain” of metal into this zone at an inclined angle towards that plane, on which it lay, as well as up.

As a result of performing the above own movement, the direction of which is determined by the existing tangential and radial angles of inclination of the blowing nozzles 10 installed on the sheathing spiral “D”, and a metal particle falling under the impact of an air stream will either be thrown into the central region of the working chamber and as a result of this again it will turn out to be glued to the growing single crystal “I”, or it will come into direct contact with the surface of the moving cavity enclosing the cavity with one of its sides n, piston cheeks 3. With this collision, the “grain of alloy” makes a rebound, and again, it either “bounces” from the plane of this element of the device and moves to the “core” of the working chamber filled with an expanding metal single crystal “I”, or falls in the lower region of the housing 6. In this case, the cycle of movement of the metal grains is repeated in exactly the same way. The “metal grains” that fell on the “isthmus of the isthmus” between the nozzles 10 installed in the device’s case sooner or later are pushed out from their original location by the surface of the continuously and progressively moving cheek-piston 3 of the working chamber, which, moreover, also “scrolls” around its own longitudinal axis of symmetry.

Thus, this part of the metal particles accumulated on the "bottom" of the housing 6 is "retracted" to parts of its surface through which jets of compressed air entering the volume of the working chamber are passed.

Caught in these areas of the surface of the housing 6, and this accumulation of “grains” of the alloy obtained in the working chamber will go through the entire previously disassembled cycle consisting of “rebounds” and “rebounds”, which ultimately, due to the action of ordinary laws of statistical probability, will force the latter occupy the necessary final position fixed directly in the thickness of the grown single crystal “I”.

The above-mentioned processes of forming an annular columnar single crystal “And” on a seed rod 7 (see FIG. 1) continue throughout the entire period of time during which the working chamber is moved in the “back and forth” direction, the corresponding dimension of which in connection with the above and is 15-20% of the value of this parameter, which determines the total length of the device used for its movement. Based on the need to create optimal conditions for completing the processing, the choice of the value of the speed of its longitudinal feed (40-60 mm / min) was made. The working chamber makes angular rotations of the latter around its own longitudinal axis of symmetry at an insignificant speed - only 2-4 rpm.

When reversing to the other side (the reverse segment of the path of its movement carried out by the working chamber), the “seed-rod” 7, as it were, “winds” the metal layers forming around it onto its outer surface, thereby increasing the uniformity of the distribution of their own thicknesses along the entire length of the body synthesized in the working chamber of the "I" single crystal.

So, having reached its extreme final front “right” position, and having received the appropriate commands from the external power supply and control unit used in the device, the working camera begins to move in the opposite direction, that is, it begins to move to the very back “left” part of the device’s body 6 until it again occupies the same initial position in the cavity of the removable cap 4, in which it was at the very initial stage of the processing process. During the implementation of this part of the cycle of this kind of "reverse movement" of this working unit of the device, which is performed at the same speed as the direct one, the processes of "final completion" of the formation of the resulting columnar ring single crystal consisting of the synthesized intermetallic compound continue to be carried out in it. That is, in fact, a “finishing” refinement of its configuration and composition to the final standards required by the processing technology is carried out.

Having moved to the leftmost position and having again taken its initial position, upon completion of the above steps, the working chamber of the device ends thereby the entire cycle of the process of processing the feedstock into the desired finished product. Accordingly, at this stage they are switched off: a drive that ensures reciprocating and rotational movement of the working chamber, the solenoids 13 of the magnetic generators 11 are de-energized, and the nozzles 10 are disconnected from the external supply line of compressed air. At the same time, from the back of the housing 6 due to the release of the pressed flanges 9, a removable cap 4 is detached.

After that, the piston-like cheek 3 is unscrewed and the nut 9 is pulled to the supporting shoulders of the seed rod 7, and the cheek 3 is removed from the corresponding end of the roller 8 (see FIG. 1). The single crystal “I” obtained by processing, due to the presence of an intermediate loose layer of slag waste “Ж”, easily collides with the outer surface of the seed rod 7 and is sent for its intended use. The processing cycle can be considered complete.

The processes of direct reduction themselves of the constituents of a multicomponent alloy of elements from their ore compounds, at the moment they are directly affected by artificially created powerful magnetic fluxes, are carried out in accordance with the following schemes for transforming the initial components.

CO ₂ → C ⁺⁴ + 2O ^-2 ; H ₂ O → 2H ⁺ + O ^-2 ;

CH ₄ → C ⁺⁴ + 4H ⁺ + 8e;

TiO ₂ + 2O ^-2 + C + ⁴ → TiO ₃ + CO;

TiO ₃ → Ti ⁺⁶ + 3O ^-2 ;

Fe ₃ O ₄ → Fe ₂ O ₃ + FeO;

Fe ₂ O ₃ + 3C + ⁴ → 2Fe ⁺³ + 3CO + 8e;

FeO → Fe + ² + O ^-2 ;

СО + СО → 2С ⁺⁴ + 2O ^-2 + 4е;

Al ₂ O ₃ + 3C + ⁴ → 2Al + ² + 3CO + 8e;

Ti ^{+ 6} + 3Al + ² → TiAl ₃ + 12e;

Ti ^{+ 6} + 3Fe + ² → TiFe ₃ + 12e;

Ti ^{+ 6} + 2Al + ² + Fe + ² → TiAl ₂ Fe + 12е;

Ti ^{+ 6} + 2Fe + ² + Al ² → TiFe ₂ Al + 12е;

Fe ₂ O ₃ + TiO ₂ + Al ₂ O ₃ + SiO ₂ → Fe ₂ O ₃ × TiO ₂ × Al ₂ O ₃ × SiO ₂ ;

C ⁺⁴ + 2O ^-2 → CO ₂ ;

H ⁺ + H ⁺ → H ₂ + 2e;

2H ⁺ + O ^-2 → H ₂ O;

where e is an electron; or a single charge with a negative value of the intrinsic valency obtained in the process of ionizing the atoms that make up the raw materials and form them.

Thus, by considering the synthesis performed in accordance with the above schemes for the synthesis of the components of the alloy of metals and non-metals from their compounds, we can conclude that directly and inverse molecular transformations continuously occur directly in the processing zone during the implementation of the proposed method of raw materials with a shift in the chemical equilibrium formed in it towards the formation of a columnar single-crystal structure in this region - alloy It consists of intermetallic compounds of titanium, iron, and aluminum, as well as the external atmosphere that emanates into the surrounding device, which are emitted during the complex of these reactions of microvolumes of the above volatile gaseous products (CO ₂ ; H ₂ O; H ₂ ).

Thus, their previous analysis allows us to state that the carbon element C ⁺ , obtained from carbon-containing molecules that make up the atmosphere and include this component (CO ₂ ; CH ₄ ) gases, during the implementation of “magnetic shocks” applied to them ⁴ as a result, and it takes away from the corresponding compounds of titanium, iron and aluminum the atomic oxygen released during the decomposition of these components, while being firmly attached to the latter. In addition to direct ones, as was previously reported, reverse reactions also occur in the treatment zone, during which volatile gases are formed that have a minimum of their internal energy (H ₂ O; CO under the conditions of this powerful and continuously performed “field” energy effect) ₂ ; H ₂ , etc.).

Due to the influence of the entire complex of conditions indicated above, the multicomponent alloy thus obtained is a stable, in relation to the influence of all these external, artificially created force factors, annular columnar single crystal having the same predefined spatial configuration, the components of which do not go into connection with other active components located next to it under the conditions of this intensively conducted external energy impact.

The characteristic features of crystallization of the individual constituent components — intermetallic compounds — should include, first of all, the fact that the formation of these last elements is clearly defined by such a basic parameter of the technological process of processing as the intensity of the initial metal and nonmetallic metals formed in the transformation zone compounds into the final product, sawtooth magnetic fields generated there.

That is, a well-marked and easily revealed regularity of the synthesis progress of the constituents of the resulting columnar ring single crystal of intermetallic compounds, depending on the value used during processing and its above parameter, is traced. With its relatively small values, the “I” single crystal formed on the seed rod 7 is formed exclusively from TiAl ₃ intermetallic compound (3-4.0 × 10 ⁴ A / m). At higher magnetic field strengths, other intermetallic compounds are synthesized - first, TiAl ₂ Fe; and then TiFe ₂ Al. Upon reaching the highest possible values of this technological parameter, the tension N, already approaching the upper boundary of the range specified by the processing technology, a final product is formed that closes this technological chain — that is, TiFe ₃ intermetallic compound (1.3-1.5 × 10 ⁵ A / m).

At the same time, it should be pointed out that the composition of the initial raw material mixture used to obtain this from any of the above items, a specific finished product, remains the same. The formation of varieties of the latter that differ from each other in their composition is ensured by only one change in the main technological modes of the processing process.

In general, it should be considered that the previously mentioned specific features inherent in the processing technology performed in the above manner, as it were, allow us to simulate the conditions for the so-called "melting zone". That is, the implementation of the crystal process in the working chamber constantly moving in the cavity of the working chamber with its angular rotations around its own longitudinal axis of symmetry, the filing of sawtooth pulses having angular displacements relative to each other and in adjacent pseudophasic packets composed of them, and provides the “final” formation of the crystal structure obtained in the device in the form of a columnar annular monolithic formation consisting exclusively of to some intermetallic compounds.

Other substances and pollutants, which are also present in the composition of the impurities present in the initial raw material mixture, will necessarily and inevitably be transformed into new crystalline formations, which subsequently synthesize finely divided loose slag waste that appears at the end of the treatment process. The latter are grains of yellow-brown color with a violet tint, with overall dimensions from 0.1 to 0.6 mm. The composition of these “tails” for the most part is represented by ferrotitanium aluminum silicates (80-85% of their total mass - Fe ₂ O ₃ × TiO ₂ × Al ₂ O ₃ × SiO ₂ ). The above substance can be used after additional grinding and mixing with water, for the formation of products consisting of electrical insulating, refractory ceramics.

In the role of the feedstock for the implementation of the proposed method can be a variety of ore concentrates, the composition of which as one of the constituents of the latter components includes compounds of titanium, iron and aluminum. Their processing can be carried out without involving any additional operations for their preliminary post-treatment.

The processing of the raw feed slurry, carried out in accordance with the proposed technology, is carried out at a “trapezoidal” magnetic field strength measured directly in the cavity of the working chamber used, amounting to 3 × 10 ⁴ ÷ 1.5 × 10 ⁵ A / m. The oscillation frequency of these force formations used for processing the initial ore materials is in the range from 30 to 80 units, passed through the solenoids of the processing magnetic sawtooth pulses for one minute.

When performing the proposed method for processing raw materials, i.e. upon receipt of titanium, iron, and aluminum alloys from the initial ore material, a technological magnetic system mounted on three encircling the outer side surface of the device case was used, which in turn consisted of F-shaped magnetic circuits, in the lower part of which there were “passed” through the walls of this assembly unit of the device focusing nozzles, located, in turn, in the installation sleeves. The number of such magnetic generators fixed on each installation spiral passing through the device casing was from nine to eighteen units.

The F-shaped magnetic circuits processing the raw materials on the surface of the device case were mounted in such a way that the focusing nozzle contained in them, located in the mounting cavity of the installation sleeve, passed through the case walls in a radial direction relative to the longitudinal axis of symmetry of this assembly (i.e., at an angle 90 ° to the installation spiral line).

The angles at which the blasting nozzles O were fixed were equal to 30-45 ° (both tangential and radial) relative to the surface of the casing on which they were mounted. The installation of these nozzles 10 was carried out in exactly the same way as the processing magnetic circuits 11, that is, also using three mounting spirals. Before entering the process of producing a multicomponent metal alloy, 60 liters of the initial raw material mass were loaded into the feed hopper 2, which was directly included in the removable flap cap 4. The latter was a two-component mud-like water suspension obtained by mixing small, consistency of powder, particles of titanium, iron and aluminum ores containing aluminum in a given volume of water. The solid components used in the composition of this initial raw material product, forming the so-called “dry residue” in it, were obtained from the nearest processing plants where concentrates were made from quarry ore rocks being developed nearby, in order to further use the resulting product to satisfy the relevant the needs of existing metallurgical production.

Before starting the preparation of the raw aqueous suspension, an operation was carried out to break up the pieces of ore concentrates of the pieces that are described above into fine particles, carried out using a conventional ball mill. Before crushing pieces of rock, dosing of the ore concentrates used in the "dry residue" of the used raw material mixture was carried out, which ensures the formation of the latter with the specified technology by the content of its starting components (Ti; Fe; Al compounds).

Obtained during the "ultrafine grinding" particles of the feedstock had overall dimensions in the range from 0.001 to 0.008 mm. The processing time of the above volume of raw materials using this kind of “three-helix” magnetic system containing F-shaped processing magnetic circuits with radial focusing nozzles and using the previously indicated range of magnetic field strengths averaged 12–30 minutes. The yield of the finished metal single crystal, calculated on the use of 60 liters of raw aqueous suspension to obtain it, reached a value of 17.4 kg to 20.1 kg (29% -33.5%) of the total volume used in processing it). These indicators come close enough to the theoretically possible limit that determines the total amount of metal alloy produced from the initial mass of the raw material for the given percentage of titanium, iron and aluminum compounds used in the processing process and including these components of the used ore rocks.

The concentration of the main component of the formed columnar ring single crystal of intermetallic compound, in the total mass of the latter, has a value of 99.9999% -99.99999%.

The proposed method for producing the above alloy is performed at room temperature (17-27 ° C), and the processing of the feedstock is carried out under the action of compressed air jets supplied to the zones of structural transformations under an overpressure of 0.4 ÷ 6.0 kgf / cm ² .

The technological modes assigned for the processing of initial raw materials are the intensity of the “sawtooth” magnetic fields, the frequency of oscillations that create these fields of current pulses, the processing time, the amount of excess pressure in the volumes of compressed air supplied to the raw material (etc., etc. .d.), assigned on the basis of considerations of the formation of the most optimal conditions for the accelerated flow of structural transformations specified by the technology for producing a multicomponent alloy, which are part of p uds of metal compounds into this necessary finished product itself, i.e. alloy.

The percentage in the mixture of "dry residue formed from solid particles used to obtain the metal of the original ore rocks in the composition of the aqueous suspension used in the processing is determined based on the presence of the following factors.

When the concentration of this kind of component in the latter is less than 40%, the raw material used automatically turns into “poor”, which negatively affects the efficiency of the process of processing raw materials, since the yield of the required finished product is significantly reduced. With an increase in its content above a value of 70%, the processed raw material sharply reduces the indicators determining the degree of its plasticity. This, in the end, significantly complicates the process of moving it from the volume of the loading hopper into the cavity of the mobile working chamber, as well as the subsequent transfer of the microportions of this material that make up the mass of raw materials through the processing magnetic fields generated in it.

The particle sizes used to obtain an aqueous suspension of ore rocks, the dimensions of which are determined by a value of 0.001 ÷ 0.008 mm, are determined on the basis of the need to form with their use a “stable” plastic mud-like raw material mass.

The latter should not be stratified into its individual components for the time period necessary for the complete completion of the processing process.

To perform the process of producing an alloy based on titanium, iron, silicon, carried out using the proposed method, a mixture was used consisting of ore concentrates containing both titanium and iron and aluminum compounds (respectively, ilmenite, magnetic "iron ore" and "kaolin" )

Ore rocks used as the main initial components to obtain the necessary raw material contained in their composition:

I Titanium concentrate "ilmenite":

1. TiO ₂ - 52%;

2. Fe ₂ O ₃ - 23%;

3. FeO - 20%;

4. Al ₂ O ₃ - 2%;

5. CaO - 0.2%;

6. MgO - 0.07%;

7. SiO ₂ - the rest, up to 100%;

II Magnetite concentrate:

1. Fe ₃ O ₄ - 78%;

2. Fe ₂ CO ₃ - 12.6% (spar iron ore);

3. FeO - 6.5%;

4. Al ₂ O ₃ - 1.5%;

5. CaO - 0.5%;

7. MgO - 0.08%;

8. SiO ₂ - the rest, up to 100%;

III Kaolin concentrate:

1.Al ₂ O ₃ - 47.5%;

2. SiO ₂ - 42.5%;

3.Na ₂ O; K ₂ O - 2%;

4. Cao - 1.5%;

5. Fe ₂ O ₃ - the rest, up to 100%.

Before grinding the above ore rocks, they were pre-dosed, ensuring the content of the latter in the so-called “dry residue” used in the preparation of a viscous aqueous suspension in the following amounts:

- titanium rock - 34%;

- iron ore - 33%;

- aluminum rock - the rest, up to 100%.

When carrying out all the experiments below to obtain an alloy based on titanium, iron and aluminum using the proposed method to achieve this goal, the same type of raw material was used containing the components listed above, including titanium, iron and aluminum compounds, which have the same previously marked composition here.

Before the preparation of the aqueous suspension loaded into the processing device, the pieces of the initial ore components used in it were crushed using a ball mill to obtain from these bulk materials included in these large-sized particle formations, the dispersion of which corresponded to a value of 0.001-0.008 mm.

The finished final product formed at the end of the processing process was a columnar ring single crystal consisting of the above components, and “tails” —fine-grained slag wastes — were formed from the contaminants used in the ore. Milled into small particles, that is, to the state of “powder”, containing titanium, iron and aluminum compounds, the initial ore rocks were then poured with a predetermined processing technology by the volume of water and mixed in it until a homogeneous, viscous, plastic, mud-like, was obtained from all of the above raw materials suspensions.

After the manufacture of the latter, the mass of the dirt-like substance formed during this operation was loaded directly into the loading hopper of the device used to obtain the multicomponent alloy.

Further, the process of implementing the proposed method is illustrated using a number of examples below.

Example 1. In the feed hopper 2, having a volume of 60 l, was placed an aqueous suspension containing a raw material mixture, which included solid particles obtained from titanium, iron and aluminum concentrates. The content of this “dry residue” in the volume of the aqueous suspension used during the treatment was 40% (24 kg). The remaining mass of the load was represented by water - 60% (36 liters).

After completion of the loading operation of the source material being processed 1 and the completion of the operation for releasing the inner cavity of the hopper 2 from it, from where the mud-like water suspension through gravity hatch “B” by gravity entered directly directly into the space of the mobile working chamber, the following were simultaneously turned on:

- an external drive of the device, providing reciprocating movement of the roller 8, as well as kinematically connected with it by the working chamber itself, while simultaneously performing angular rotations around its own longitudinal axis of symmetry;

- all winding coils 13 included in the magnetic circuits 11 were connected to the electronic unit present in the circuit of an external source of electrical supply, the presence of which provided a supply to the above-mentioned elements of pulse packets, each of which had the form of a “saw tooth”;

- through all the blowing nozzles 10 placed on the housing 6 of the device, the supply of compressed air jets began.

Its receipt to the above-mentioned blowing elements 10 from an external supply line in this example was carried out under an overpressure of 0.4 kgf / cm ² . The tension generated in the cavity of the working chamber and having the form of a kind of spiral-shaped “cylindrical” “fringe” of “sawtooth” magnetic fields corresponded to a value of 3 × 10 ⁴ A / m.

The frequency of arrival of pulses having the configuration of a “tooth of a saw" on the winding coils 13 of the generators 11 was 80 units in one minute.

The mobile working chamber moved from the loading zone to the front “right” end of the device body 6, and then back to its original “left” position at a speed of 40 mm / min. Moreover, she made revolutions around her own longitudinal axis of symmetry. The number of the latter was 4 rpm. When making the transition from “direct movement” of the working chamber to “reverse”, the direction of the structural components that make it up was reversed, which was replaced by the opposite.

The time of the entire processing cycle of the starting raw material 1 in the total result amounted to 30 minutes (0.5 hours).

The raw material mass 1 moved “back and forth” together with the movable working chamber under the influence of the magnetic radiation generated in the device, generated by the generators 11 and the focusing nozzles 14, was transformed into a columnar ring single crystal “I” upon completion of the processing process. The latter was deposited directly on the slag waste layer “Ж”, covering the lateral surface of the spacer rod-seed 7, and consisted entirely of TiAl ₃ intermetallic. The content of this metal compound indicated above in the volume of the final product thus formed was 99.99999%.

The color tone of the obtained single crystal was light gray, with a purple hue. The mass of the finished product thus obtained was consistent with a value of 12.8 kg. The weight of the processing of fine-grained slag waste was 7.8 kg. The rest of the mass of the original raw material was spent on the formation of volatile gas compounds that were ejected from the cavity of the device into the outside atmosphere.

The specific bulk density of the above final product corresponded to a value of 2.22 g / cm ³ ;

- melting point - 1617 ° C;

- hardness HRC - 58 units;

- specific volume electrical resistivity ρ - 31 N · Ohm · m;

- specific thermal conductivity - 0.018 kcal / cm · sec · deg;

- compressive strength σ _m - 0.98 GPa;

- bending σ _and - 0.54 GPa;

- gap σ _p - 0.74 GPa.

Example 2. The processing of feedstock was carried out in accordance with the same scheme as was indicated in example 1.

The initial ore mixture contained a “dry residue”, the amount of which relative to the total volume of water suspension used was 70% (42 kg). The remaining volume of the initial product was water - 30% or 18 liters. The air supply to the processed raw materials was carried out under excess pressure equal to 6.0 kgf / cm ² . The working chamber was moved with the raw material loaded into it at a speed of 60 mm / min, and the angular rotation of the structural elements included in it was carried out at a value of this parameter corresponding to 2 rpm.

The tension generated in the volume of the working chamber and forming there a spiral cylindrical magnetic fringe - the “stockade” of physical “sawtooth” magnetic fields corresponded to 6 × 10 ⁴ A / m. The number of 13 sawtooth electric pulses transmitted through the coil windings of 13 magnetic generators was equal to 20 units per minute.

The processing time under these conditions corresponded to a period of 12 minutes (0.2 hours). The weight of the columnar ring single crystal obtained at the end of this process, consisting of the TiAl ₂ Fe intermetallic compound, was 22.2 kg. The amount included in the formed during the processing of the crystalline structure of the above element was a value equal to 99.9999%.

The remaining amount of unused raw material was used up for receiving fine-grained slag waste - 14.2 kg and volumes of volatile gas compounds sent to the outside atmosphere.

The specific bulk density of this formed during processing of the final single-crystal product corresponds to a value of 3.6 g / cm ³ ;

- its melting point Tm is - 2170 ° C;

- specific volume electric resistance - ρ - 38 N · Ohm · m;

- surface hardness HRC - 62 units

Its strength indices, as well as thermal conductivity, repeat the corresponding data given in Example 1. The color shade of the crystal can be characterized as light gray.

Example 3. The processing obtained from the particles of the source ores of the rocks of the raw material suspension was carried out in accordance with the same scheme as was already indicated in examples 1, 2.

The content of the so-called "dry residue" in the composition used in the processing of the aqueous suspension formed from particles included in its mass of ore rocks amounted to 60% of its total amount or 36 kg. The remaining volume of the raw suspension was water - 40% (24 liters).

The supply of compressed air through the blowing nozzle 10 was carried out under an overpressure of 4 kgf / cm ² .

The longitudinal movement of the working chamber along the housing of the device was carried out at a feed rate of 50 mm / min. The angular rotation speed of its constituent elements was equal to a value of 2.8 rpm.

The intensity of the processing magnetic fields generated in the volume of the working chamber was 9 × 10 ⁴ A / m. The number of 13 sawtooth pulses suppressed to the winding coils supplied from an external power source was 50 units per minute. The processing time corresponded to a value of 17 minutes (0.2666 hours).

As a result of the process of processing the feedstock on the seed rod 7, a columnar ring single crystal was formed entirely consisting of TiFe ₂ Al intermetallic. The weight of the obtained crystal was 17.2 kg. The degree of purity of the content in its composition of the main compound forming it, intermetallic compound, corresponded to a value of 99.9999%. The rest of the material used to obtain the material was spent on the formation of finely dispersed slag waste of 11.4 kg, as well as volatile gas compounds sent to the outside atmosphere.

The specific bulk density of this material was 4.8 g / cm ³ ;

The melting point Tm was - 2200 ° C;

The specific volume electric resistance corresponded to the value - ρ - 52 N · Ohm · m;

Surface hardness was HRC - 70 units.

Specific thermal conductivity - 0.2 kcal / cm · sec · deg;

Tensile Strength:

Compression σ _m - 1.0 GPa;

Bending σ _and - 0.58 GPa;

The gap σ _p - 0.79 MPa.

The color shade of this material meets the definition of dark gray.

Example 4. Obtaining the desired final product in the processing of the starting raw material was carried out in accordance with the scheme specified in examples 1; 2; 3.

The raw material used during the processing contained crushed ore rocks, the total amount of which in the mass of the so-called "dry residue" reached 55% (or 33 kg). The remaining volume used in the processing of viscous raw slurry was water (45.0% or 27 liters). The supply of compressed air to the exhaust jets, consisting of this product, blowing nozzles was carried out under an excess pressure of 3.0 kgf / cm ² .

The magnitude of the longitudinal feed when moving the working chamber along the cavity of the device casing was 55 mm / min. The rotational speed of its structural elements included in the above assembly assembly corresponded to a value of 3.4 rpm.

The time interval after which the process of processing raw materials was completed was 14 minutes (0.2333 hours). The intensity of the sawtooth physical fields generated in the volume of the working chamber, which were artificially formed in the form of a “three-band” spiral-shaped magnetic cylindrical fringe-paling, amounted to 1.5 × 10 ⁵ A / m.

The number of sawtooth pulses sent to the solenoids 13, which are part of all the magnetic generators 11, corresponded to a value of 40 units per minute.

Upon completion of the processing process on the seed rod 7, which was part of the chamber used in the processing, an annular columnar single crystal was obtained, which was entirely composed of TiFe ₃ intermetallic compound. The percentage of this basic component making up a single crystal component reached 99.99999%. The weight of the single crystal formed in the device was 19.6 kg.

The specific bulk density of this finished final product was 4.98 g / cm ³ ;

The melting point Tm was 2470 ° C;

The specific volume electric resistivity corresponded to the value ρ - 61 N · Ohm · m;

The surface hardness was HRC 76 units.

The specific thermal conductivity is 0.03 kcal / cm · sec · deg;

Tensile Strength:

Compression σ _m - 1.3 GPa;

Bending σ _and - 0.62 GPa;

The gap σ _p - 0.84 GPa.

The color shade of the columnar ring single crystal obtained from this intermetallic can be considered as “completely black”.

The rest of the raw material used in the processing was spent on the formation of finely dispersed (0.1-0.6 mm) slag waste - 9.4 kg, as well as volatile gas compounds microvolumes sent to the surrounding device.

From all the examples presented above it is clearly seen that the formation of a fairly wide range of alloys based on titanium, iron and aluminum, synthesized in the form of columnar circular circular single crystals, and also having a high degree of purity in the content of the main component of this finished end product of intermetallic compound, and in addition to Moreover, obtained by the manufacture of sufficiently good performance relative to its own refractoriness, it can be carried out using widespread and long used to meet the relevant needs of the current metallurgical production of ore concentrates, without any additional operations for their post-treatment or appropriate refinement.

Further, in the materials presented below, structural principles are set forth in accordance with which the device itself used to implement this method is implemented. The presence of the latter, in turn, ensures that the necessary positive effect is obtained during the application of this unit.

The drawings show a device for implementing the proposed method for producing alloys based on titanium, aluminum, iron.

Figure 1 - longitudinal section is a diagram of the device with the main installed on its body, providing functional processing of raw materials, serving the above process nodes.

Figure 2 is a transverse section of the housing of the device along AA, passing directly through its working chamber with a columnar ring formation formed in it, consisting of Ti; Fe; Al.

Figure 3 - image of the node 1 (see figure 2), which on an enlarged scale shows the installation of the F-shaped power magnetic circuit 11 on the housing 6 used in the processing of the device.

Figure 4 - node II (see figure 2), with the image fixed on the housing 6 of the device blowing nozzle 10, which feeds into the cavity of the last jets of compressed air.

Figure 5 presents a diagram of the supply of "sawtooth" current pulses sent to each of the constituent magnetic circuits 11 of the winding coils 13 that perform the functions of solenoids in these magnetic generators.

On all these figures, in turn, are indicated:

Pos.1 - the initial raw material substance, with the use of which the necessary final product is obtained - a multicomponent alloy.

Pos.2 - loading hopper, in the cavity of which is processed the initial mass, containing in its composition particles of the ore used, is placed before the start of the processing process.

Pos. 3 - the right and left “cheeks” of the double movable piston, forming the cavity of the working chamber, in the volume of which the recovery of the metal alloy component from the initial ore compounds proceeds.

Pos.4 - removable cap, in the cavity of which the working chamber is loaded with processed raw material, as well as after its dismantling, and unloading of finished products after the processing process is completed.

Pos.5 - a set of flat annular connecting flanges with quick-detachable threaded fasteners, with the help of which the removable cap 4 is docked with the device body 6, as well as its dismantling after the end of the processing of the original raw material.

Pos.6 - the device case is its fixed part, on the outer surface of which all power units serving the processing process are fixed, and screw reciprocating movement of the movable working chamber is carried out in its cavity. The volume of the internal space in the latter is formed between the right and left piston-shaped cheeks 3.

Pos.7 - an expansion rod-seed, on which the products of processing the feedstock obtained in the volume of the mobile working chamber are deposited, and also with its help, the left and right cheeks 3, which are part of the translational assembly moving above in the cavity of the casing 6, are rigidly fixed node.

Pos.8 - a running roller attached to the left cheek of the working chamber, under the influence of which the latter can make a reciprocating transfer in the cavity of the housing 6, and also perform angular rotations around its own longitudinal axis of symmetry.

Pos. 9 - a fixing nut, mounted on a threaded shank-bolt, located at the very end of the seed rod 7, when unscrewed which creates the appropriate conditions for free removal of the right piston-shaped cheek 3 of the working chamber, and thereby provides free access to received her end products processing.

Pos.10 - blowing nozzle mounted on the outer surface of the housing 6 and passing through its walls, and installed there in compliance with the specified technological parameters of the angles of its inclination - tangential β ° and radial α °, the value of which corresponds to a value of 30-45 °.

Pos.11 - F-shaped power magnetic circuits, providing when connected to an external source of sawtooth pulses, the formation of magnetic fluxes in their working elements 12, which, in turn, flows to the body of the focusing nozzle 14.

Pos.12 - working elements made in the form of plates, with the mutual docking of which the body of the F-shaped magnetic generator 11 is formed.

Pos.13 - winding coils mounted directly in the body volume of the working elements 12 and performing functions there creating individual magnetic fields of solenoids.

Pos.14 - a focusing nozzle pressed directly into the mounting technological hole in the body of the magnetic circuit 11, with the help of which cylindrical “elongated” cylindrical clusters of magnetic field lines-rays “K” are sent straight into the internal volume of the housing 6.

Pos.15 - installation of a hollow sleeve, rigidly fixed directly to the outer surface of the housing 6, the inner cavity of which is in communication with the volume of the latter, and in its upper part there is a threaded thread. With the help of its manufacturer, the connection of the inner surface of the installation sleeve with the external end threaded part of the focusing cylindrical nozzle 14 intended for installation in the same area.

Pos.16 - curved liner washer that provides filling of the volume obtained when installing the F-shaped magnetic circuit 11 of the recess directly adjacent to the inner side surface of the cavity of the housing 6 and eliminating the appearance of protruding sharp edges at the borders of this cavity (that is, it “smooths out” when fixing the washer “flush” with the plane of the internal cavity of this housing 6). The curved washer 16 is made of pressed into the last mass of small crumbs of magnetically conductive metal (for example, including sawdust of cobalt or cast iron shavings).

Pos.17 - almost the same as in the previous case, the “smoothing” washer, the installation of which is also carried out in a curved recess formed during installation of the body of the blowing nozzle 10 passing through the walls of the body 6. The material for the manufacture of this kind of “leveling” element any sufficiently “slippery” plastic can serve - for example, elastic sheet rubber. This washer also has split “petals” diverging from its center to the periphery, which bend downward from its own central core — the base, at the moment of passage of compressed air sent there through the cavity of the blowing nozzle 10.

Pos.18 - a pipe for the withdrawal from the internal cavity of the working chamber of the device of the portions of volatile gas compounds newly arising there during the recovery of metals and nonmetals, as well as excess volumes of compressed air received therein.

Pos.19 - pressure reducing valves, the opening of which is carried out at times when the overpressure in the working chamber begins to exceed the limits specified by the processing technology.

Pos.20 - the front end wall that overlaps the cavity of the fixed part of the precast housing 6, with a hole made in the center for the passage of the moving roller body 8 moving in it.

In turn, in the presented images of figure 1 - figure 5 - the letters indicate:

"A", "b", "c" - figure 5, individual pseudophases involved in the process of supplying electrical power and addressed to the winding coils 13 of the magnetic circuits 11, and, in turn, consisting of arranged in a certain order and sets of “sawtooth” current pulses forming them.

In - hole-hatch connecting the cavity of the loading hopper 2 with the internal volume of the working chamber formed by the left and right "cheeks" 3.

G - installation cylindrical spiral lines laid on the outer side surface of the housing 6, on which are located processing magnetic circuits 11.

D - the same kind of spiral curves used to fix the blowing nozzles 10, supplying a stream of compressed air to the raw material.

E - formed in the inner surface of the housing 6, as well as in the volume of the mobile working chamber, a vortex-shaped jet air gas stable formation - "tornado".

And - obtained on the outer surface of the rod 7, a columnar ring single crystal, consisting of a multicomponent metal alloy.

G - a loose layer formed on the plane of the same rod 7, obtained from slag waste formed during the processing of ore raw materials.

K — clusters of force lines generated by magnetic circuits 11 formed in the form of straight cylindrical cylindrical formations, which, in turn, belong to force-processing physical fields created using focusing nozzles 14.

M is a cavity-cavity made at the lower end of the nozzle 14 with a configuration that maximally coincides with the outlines of the spatial rotation hyperboloid, and is designed to generate clusters of magnetic field lines, the shape of which almost completely duplicates the one that is obtained by rotating around its own longitudinal axis of symmetry elongated in the length of the rectangle, spatial formation (i.e. imitates the shape of a figure made in the form of a segment of a round volume cylinder).

α ° - radial tilt angles (30-45 °), with the use of which the blasting nozzles 10 are fixed on the surface of the housing 6.

β ° - respectively, the tangential angles (30-45 °) of the same elements, determined relative to the lateral outer surface of the same assembly unit 6 of the device on which they are placed.

t ₁ t ₂ - segments along the abscissa axis (see figure 5), specifying the relative angular displacement of the components of the "pseudophase"a;b; in their individual impulses.

Based on the foregoing, it is imperative that necessary clarifications be made regarding the design features of the performance of the apparatus proposed for processing raw materials.

As can be clearly seen from the drawings presented in the application, the production of annular columnar monocrystals “I”, consisting exclusively of a multicomponent alloy including titanium, iron and aluminum, flows directly into the cavity of the mobile working chamber formed by the right and left cheeks belonging to it 3 .

Its total length is 1/5 relative to the size of the same dimension, which determines the corresponding similar parameter of the entire proposed design. The piston-shaped cheeks 3 are fixed in this above-mentioned assembly by “stringing” them onto the roller. In the process of their installation in the “regular” permanent position, the structural elements noted here are passed along the lateral outer surface of this part and reach the persistent end shoulders of the seed rod 7. When this end position is reached, they are finally fixed in it with threaded nuts 9 ( see figure 1). The winding of these fasteners 9 is carried out according to the thread made on the corresponding parts of the surface of the roller 8 (not shown). In addition, on the outer side surface of the piston-shaped cheeks 3, forming a working chamber with a crystalline formation grown in its cavity, plastic sealing elements are installed to insulate its volume from its external environment (not shown in the seal drawing). Upon completion of the processing process, the working chamber enters, finally, again in the cavity of the removable cap 4, occupying a fixed extreme position there.

The removable cap 4 after the placement of the aforementioned working chamber in it and the complete stop of the movement drives used in the device, as well as all the systems servicing it, is disconnected from the fixed part of the housing 6. This kind of assembly is disassembled by releasing the coupling ring flat flanges 5, carried out by loosening and moving to the starting position used as part of the site quick-release fasteners (not shown). After the operation of removing the cap 4, the nut 9 was released, with which the right cheek was fixed 3. The latter, in turn, upon completion of all the transitions listed above without any special difficulties, upon completion of all the transitions listed above, is removed from the corresponding end of the roller 8, thereby opening up free access to the annular monocrystal “I” located on the seed-rod 7. This metal formation can then, without particularly noticeable and necessary efforts, be moved to the right, and subsequently completely removed from the volume used to obtain it.

The roller 8, providing a “helical” movement of the working chamber during processing of the initial raw material mixture, is connected to the corresponding external drive, the presence of which allows the necessary changes in its angular positioning, as well as the translational movement of the constituent components of the latter along the cavity of the housing 6, to round-trip direction. That is, first to the front "right" end of the housing 6, and then from it to the very rear "left" part of this device.

For the installation of the processing magnetic circuits 11, a set of curved lines is used, consisting of three installation spirals “G”. Blowing nozzles 10, in a similar manner, are also fixed on the corresponding three curved paths "D", laid between the turns that make up the installation lines "G".

To prevent premature failure of the plastic sealing seals mounted on the outer side surface of the left and right cheeks 3, at the joints of the power units 10 and 11 used in the device, with the walls of the housing 6, the following technique is additionally applied.

In the zone of formation of the curvilinear cavity, resulting from the intersection of the above-mentioned elements 10 and 11 of this design, with the lateral inner surface of the cavity of the fixed part of the housing 6, additional “smoothing” washers 16 and 17 are placed.

Their surface facing the volume of the body cavity 6 has outlines that fully copy the configuration of the curved cylindrical inner side surface of this assembly. That is, in the places where they conduct their own installation, they, as it were, hermetically overlap the mounting holes obtained during their passage, located on the corresponding surface of the body cavity, and some kind of cutting “edges” formed there, and thus form a “patch” there, providing perfect match and "alignment" between adjacent "adjacent" planes (as if connecting them "flush"),

In this case, the washer 16 is made of a finely dispersed metal powder pressed into the aforementioned curvilinear recess, having a low value of its specific magnetic resistance (made, for example, of small cobalt particles).

The “smoothing” washer 17, in order to ensure the passage of compressed air jets formed in the nozzles 10, is made in the form of elastic rubber petals extending from the center, which open at the moment of supply of the above product and close back under the influence of the “lateral” external the surface passing along the cavity of the body and having a "sealing" seal cheek 3. The most successful material for the manufacture of the above structural element will be elastic rubber.

In the same way, the docking areas are formed, the exhaust gases of the nozzles 18 with the internal cavity of the housing 6. In the area of the appearance of exactly the same curved recesses during installation of the latter, smoothing plastic washers are again placed, but in this particular embodiment they will be provided with through holes perforations large enough to allow the passage of microvolumes of volatile gas compounds, but at the same time too “small” to allow passage of solid particles through them ore rocks being abatable in the working chamber (the above unit is not shown in the drawing).

The installation of blowing nozzles 10 is carried out, as already noted, on three spiral cylindrical lines "D" with the formation of tangential β ° and radial α ° angles of inclination to the outer surface of the housing 6 at the points of their fastening. The value of the above angles is 30-45 ° .

The installation of magnetic F-shaped circuits 11 is carried out in exactly the same way using three cylindrical spiral lines “G” laid on the outer surface of the housing 6. The number of power nodes located on each of these three curved trajectories “G” is from nine to eighteen units.

Fastening of the F-shaped generators is carried out using the installation sleeves 15, the mounting internal cavity of which in the upper part is threaded (not shown in the drawing). The bushings 15 pass through the walls of the housing 6, forming an angle equal to 90 ° relative to its outer "convex" surface.

The assembly 11 itself, consisting of an F-shaped magnetic circuit and a focusing nozzle 14 pressed into its lower part, also has a fixing mounting thread made on the outer side surface of the above element 14. At the time of the final fixing of the latter on the body of the housing 6, it is screwed into the sleeve 15, occupying the desired end position required by the device design (mating threads are not shown in the drawing).

The cavity recess “M” located in the lower part of the focusing nozzle 14, at its end, ensures the formation of a physical field with its magnetic, “radial-ray” lines “K”, which are very elongated and create a kind of “processing spiral cylindrical fringe. "

Each of the winding coils 13 included in the F-shaped circuit is connected to its “pseudophase” (or “a”; or “b”; or “c” - see FIG. 5) supplied to them from an external electric power source, providing the supply of the latter through the corresponding available in it electronic circuit, forming sets of packets of sawtooth pulses of electric current. Each component constituting the last individual impulse has corresponding offsets-segments t ₁ ; t ₂ , marked in figure 5, relative to the same generated in adjacent "pseudophases" (in the drawing, the external power source is not shown). Installation of the device case with all assembly units located on it on the technological basis itself was carried out using a system consisting of ordinary mounting racks (these elements are not shown in the drawing).

To fix in the position specified by the processing technology, as well as to perform subsequent detachment of cap 4, a quick-release fastener system is used (not shown in the drawing).

The central hole in the front end cap-plug 20, through which the drive roller 8 passes, has sealing seals installed on its inner side surface (not shown in the drawing). Their presence provides isolation of the internal cavity of the fixed part of the prefabricated housing 6 from the external atmosphere, and at the same time does not prevent the implementation of the corresponding movements of both translational and rotational, used as part of the device a kind of "traction" element, that is, the above-mentioned roller 8 .

The work of the proposed device when performing the processing process of the source ore ore proceeds as follows:

After completion of the operation to fill with the raw material 1 the cavity of the loading hopper 2, mounted in the upper part of the removable cap cap 4, and also at the end of the process of emptying through the through hatch "B" (see figure 1), which is provided by spontaneous by flowing out a viscous aqueous suspension filling it, the latter subsequently goes therefrom directly into the volume of the mobile working chamber formed between the components of its right and left cheeks 3. After doing all this in It supposes:

- an external drive to move the roller 8 (in the drawing, an external drive is not shown). Simultaneously with the beginning of the implementation of the structural elements that make up the mobile working chamber, translational and rotational movements, all electrical windings-coils 13, which are the main component of the F-shaped magnetic circuits 11, located in turn on three encircling the outer, are connected to an external power source the surface of the body is 6 cylindrical spirals "G". Blowing nozzles 10, mounted in the same way on the surface of the fixed part of the prefabricated assembly 6, on the above, and also using the same number of units of curved lines "D" used at the same time, are connected to the external supplying compressed air under excess pressure, the supply line (not shown in the drawing).

Thus, having a rigid kinematic connection with the roller 8, the working chamber with the processed raw material 1 placed in its cavity is pushed out of the internal volume of the removable cap cap 4, leaving the loading area, and begins to carry out the process of translational and rotational movement in the stationary cavity part of the housing 6, in which it is, ultimately, and "pushed". The outline of the path of movement of the processed raw material 1, which is picked up by the piston-shaped cheeks 3, located in the cavity of the above structural unit, moving from the feed loading zone to the front end of the housing 6, completely duplicates the configuration of this movement along the inner surface of this kind housing 6 spatial curved path.

The latter, due to the presence of the elements that make up the working chamber, the fact that they immediately act on two types of motion, both translational and rotational, ultimately, is a segment of a multi-turn helical spiral that is very elongated in length. Since the working chamber moved in such a way to a new position inevitably opens access to its internal volume by jets of compressed air formed by blowing nozzles 10 mounted on the outer surface of the housing 6, which have both radial α ° and tangential angles of inclination β °, then located at the very bottom of the working chamber, the "bulk mass" of raw material 1 collapses a whole hail of a kind of "air strikes" generated in the area of the latter "crossing" at spatial angles s this product.

The presence of this kind of “behavior” features in the processing zone of the above-mentioned gas “flows” created in the cavity of the working chamber is provided by the obligatory influence on the above process of the specific design factors noted above used in the power elements used in the device (that is, the installation of blowing nozzles 10 along the encircling the outer surface of the fixed part of the housing 6 of the spiral lines "D", the presence of radial α ° and tangential β ° inclination angles - see figure 1, figure 2, figure 4).

Under the influence of continuously carried out and the above-mentioned intense force, the volume of this "bulk mass" of processed raw materials 1 is divided into small, previously constituting it "microportions", which are "pulled" in all directions by a vortex stream formed by the same air jets " E ”(tornado). When exposed to the raging currents in the body of the “E” vortex, these individual microvolumes, firstly, are transformed into small bubbles of gas-liquid aerosols, and, secondly, they are spread throughout the cavity of the mobile working chamber, uniformly filling almost all its parts, with the exception of the central zone, where a kind of small discharge is created (“eye of the storm”).

The whole mass of the raw material 1, completely transformed into the aerosol cloud in the aforementioned manner in the above manner, subsequently continues to perform complex curvilinear helical movement over all the inner zones of the device body 6, carrying it out together and simultaneously with the latter used and hermetically isolated from other volumes surrounding it space, the cavity of the mobile working chamber of this unit. Synchronously with all this, the presence of the fact of the action on the processed raw material used is another one, necessary to obtain the finished final product specified by the processing technology, and also artificially created in this device, specifically affecting the raw material used, an external force factor.

The thing is that when you turn on all the windings-coils 13 that are part of the magnetic generators 11, which are available in the device, into the external electric network, since they perform the functions of solenoids directly in the volume of the working elements 12 themselves, in which, in fact, the assembly of these structural elements of the machining F-shaped contours was carried out, individual magnetic fields are created almost instantly.

Due to the fact that the body of each generator 11 has the configuration of the letters F, folded one from the other, the eyelets, these newly arising fields merge in a closed loop used for the processing process into a single total. Thus, the total flow circulating in a closed F-shaped loop of the body of the processing circuit is generated immediately by six windings. Each winding coil 13 is connected to its own, which feeds "sawtooth" pulse packets only for it, by a circuit-circuit of an external power source (not shown in the drawing).

Due to all this, the total field obtained in each magnetic generator 11 will have all the same characteristic features that are inherent to the same individual physical formations forming the last (the main parameters of such a force formation are changed in accordance with a schedule recording the behavior of the “sawtooth” function , and also the fact that this total field structure obtained in this way necessarily has an angular displacement of the clusters belonging to it is magnetic relative to the adjacent power lines, etc.).

Due to the fact that the upper tail of the focusing nozzle 14 is pressed into the lower crossbar of each F-shaped contour 11 (see Fig. 3), at the lower end of which a collection of magnetic field lines is made into a single cylindrical segment “K” focusing cavity “ M ", having the form of a spatial rotation hyperboloid, the total magnetic flux sent to it and received from six windings-coils 13 generates a technological processing physical field in the body of this nozzle 14, outlines of clusters of field lines in which they have the indicated in figure 2; figure 3 "special" configuration.

Since the uniform arrangement of all magnetic generators 11 was made immediately on three spirals “G” encircling the body of the body 6, and the number of such processing loops on each curve of the installation line “G” is a number equal to nine to eighteen units, the presence of all of these above factors, ultimately, inevitably leads to the fact that in the cavity of the housing 6 of the device as if formed consisting of radially directed from the surface of the installation zone-base, directly directly to the center of the housing Cylindrical rotating magnetic clusters "K", a kind of technological processing system (see FIG. 2). The latter is a kind of spatial power cylindrical “fringe”, consisting of individual logs collected in a “stockade”. The number of such processing located in the internal volume of the housing 6 and consisting of cylindrical magnetic structures assembled into a spiral - spatial structures, respectively, in the embodiment of the device shown in FIG. 1, FIG. 2, FIG. 3 is, in total, at least three units.

It should also be noted that the technological processing systems included in the above, used to carry out the recovery of metals and non-metals from ore compounds, magnetic clusters “K”, consisting of a kind of cylindrical force formations - “logs”, periodically change their own geometric parameters ( supplied for powering the winding coils 13 are in the form of a “saw tooth” and are shifted relative to each other by a predetermined, predetermined offset angle — see FIG. 5).

That is, their individual elements that make up such a “fringe-fence” - “logs”, then “stretch” in height, then, on the contrary, sharply “shorten”. Moreover, each “forming” the above-mentioned “barriers”, a separate picket fence, in the process of changing the height of its constituent elements, performs this periodically renewed kind of oscillatory cycle with a shift in time of its conduct relative to the same ones as it, but neighboring ones located next to the similar installation helix "G" (see the order of filing "sawtooth" pulses - figure 5). The effect of the above circumstance is ensured by the fact that the pulses used in the feeding pseudophases "a", "b", "c" are offset relative to the same neighboring ones by angles of about 120 ° —the segments t ₁ ; t ₂ in figure 5.

As a result of the joint action of all the specific features listed above, the formation of power structural formations carrying out processing of raw materials carried away by vortex flows belonging to the jet air stream “E” (see FIG. 1) results in the “smallest” air-liquid aerosol bubbles formed in the cavity of the working chamber "Raw cloud", move along with it along the fixed part of the housing 6. Moreover, the above components of such a "foam formation" as if forcibly "prot “they ask” through quite often barrage timbered palisades - ranks - magnetic fences (processing cylindrical “fringe”) placed on the path of their movement.

On small particles of the processed ore compounds, which are fastened onto a “film liquid base” of such “foam bubbles” formed in the cavity of the working chamber and moving in it, when the latter carry out this kind of “punching” through the spiral-shaped “magnetic fence” indicated above, it is as if applied entire series of multidirectional and intensively performed power energy strikes.

Since the movement of these microscopic ore components proceeds along rather complex spatial curved "twisted" trajectories, the rock layers that make up their body are always in the most optimal position for their further structural transformation, when access to the last microvolumes of raw materials for penetrating these particles " magnetic ray-logs, ”it turns out to be practically unshielded in almost nothing. That is, the microvolumes of the compounds that make up small particles of ore rock are “pierced” by processing rotating cylindrical magnetic fluxes “K” using the entire range of directions of their possible spatial effects.

All this, listed above, facilitates the process of recovering the constituent metals of the alloy from the “small” particles of ore compounds “glued” to the aforementioned “film” base, and also provides an increase in the percentage of the main intermetallic compounds forming it in the body. That is, ultimately, the application of the above methods and guarantees the achievement of sufficiently high indicators characterizing the percentage in the volume of the annular columnar ring formation of the “main” component itometallide synthesized in accordance with this technology.

So, when carrying out the transfer of small particles of initial ore rocks carried away by “flying through” aerosol foam bubbles through an artificially created and having a proprietary technology configuration of their own magnetic spatial structure, small crystalline “nuclei” inevitably form in the jets of the “E” tornado, consisting of previously metal elements recovered from ore.

The appearance of the "microscopic" grains "mentioned above, entirely consisting of these previously noted elements, is ensured, first of all, by the obligatory presence in the surrounding areas of small ore particles passing through the cavity of the working chamber, the volumes of ions of the reducing element filling it with air , that is, a kind of "champion" in the framework of this specialization: carbon C ⁺⁴ . The latter is generated from molecules containing the aforementioned component of gases, always present in the composition of ordinary atmospheric air, which is supplied to the treatment zone under slight excess pressure.

The presence of the very fact of the occurrence of this atomic oxygen, a reducing ion, which is "released" during the decomposition of a metal-containing compound during decomposition, is again ensured by a "crushing" impact action exerted by those "directly exposed" to the vortex formation "on the way" E "gas flows concentrated in a narrow section of power accumulations consisting of logs collected in separate barriers, i.e. a kind of "beams" formed from magnetic lines belonging to the processing physical fields.

Like ore microscopic particles, upon encountering this spiral-shaped force palisade, carbon-containing gas molecules are separated into separate fragments, while ensuring delivery of the reducing ion necessary for conducting the release of metals and non-metals from their ore compounds (the latter is generated by decomposition into individual constituent gases CO ₂ ; CH ₄ ). The very subsequent movement of such layers that again appeared in the bulk of the "aerosol cloud" in the spiral vortex flow "E", crystalline nuclei, due to the continuous "growth" of these metal "grains" that flows in the same processing zone, continues to those until their mass becomes so large that these "jet currents" will no longer have great potential to continue supporting such "grains" that are constantly increasing their overall dimensions, by weight. Because of this, the latter stop their free soaring in the components of the vortex flow “E” layers, and then they are already moving under the action of gravitational forces, from the highest level belonging to the aerosol cloud located in the working chamber, as close to its lower part as possible. The process of increasing the initial dimensions initially obtained during the formation of crystals of a multicomponent alloy proceeds under the influence of two immediately accompanying this technology for the synthesis of the aforementioned finished product from the original ore compounds, which actively influence the progress of its implementation, significant factors.

First, during the movement of aerosol bubbles in the jets of a “tornado” formed in the cavity of the working chamber, these components of the “aerosol foam” inevitably collide with “flying” through these same areas of the above “vortex”, which reappeared in them and are still very small crystalline "nuclei".

In the process of such a mutual “collision”, aerosol bubbles “flying” onto such solid “grains” of the alloy inevitably collapse, and the microscopic ore particles placed on their liquid film shell are “thrown” directly onto the outer surface of the “crashed” into this bubble is a metallic crystalline.

As a result of all this, the latter is covered, as it were, with a “raw coat”, consisting of such small solid ore components “thrown” directly onto his body. Since the process of magnetic irradiation of all the suspended microscopic particles moving in the jet vortex formation “E” and the suspended microscopic particles present in it does not stop there, this kind of specifically obtained “raw shell” will inevitably subsequently be converted into a full-fledged metal coating. The latter grows on the outer layers of the crystalline alloy, using it as a kind of substrate-base for conducting its subsequent formation. That is, in this case, the “embryo", acquiring this kind of additional metal layer that is built up directly on its body, will inevitably increase its original overall dimensions.

Secondly, during the “flight” between the restrictive cheeks 3 of the working chamber, the small crystalline “grains” carrying it out, the multicomponent alloy obtained there, also have a rather high probability of a “point” getting into the “final” situation, in which case they are inevitable enter into close mutual contact (ie, their “head-on” collision occurs, as it were).

At the moment of the implementation of the above mutual close contact, their subsequent “magnetic” “bonding” is inevitable, and, as an indispensable consequence of the fact that this circumstance exists, is the formation of a larger, composite structure from these tiny metal fragments.

It is understandable that both of the above factors for the enlargement of "nuclei of a multicomponent alloy" work in parallel and simultaneously. That is, as the length of the path along which the working chamber moves from its original initial position towards the front end of the housing 6 increases, sooner or later, all small “fragments” consisting of new structural formations synthesized directly in the cavity of the latter will thus , converted to large monolithic granules.

The latter, as already noted, upon completion of the process of their own enlargement, seek to move from the upper level of their initial location, to the lowest zone of the device used for processing.

Performing the aforementioned vertical movement, some part of the thus formed sufficiently massive metal “flakes” can “accidentally” meet the surface of the seed rod 7 of the loose layer “F” that had previously settled on the lateral outer surface of the rod and formed from the finely dispersed “ sticky "slag waste. As a result of the existence of the fact of the effect of such a “random hit”, these “overgrown” granules, with a rather high degree of probability, may simply be “tightly” “glued” into the enveloping seed-seed 7 loose non-metallic formation “G” (see Fig. 2), which has quite pronounced indicators of its own adhesion.

Due to the incessant influence of the technological factors listed above, these “adhering” particles of the multicomponent alloy will steadily continue the process of formation of more and more new body constituents of the structural formation of metal layers obtained there, based on the use of this “growth” aerosol foam volumes surrounding the latter on all sides.

The very process of deposition on the outer side surface of the seed rod 7 of the aforementioned intermediate slag layer "Ж", which is formed at the "start" stage of the implementation of the proposed processing technology, proceeds as follows.

Due to the fact that various kinds of impurity compounds from other pollutant elements present in the same place, which were simultaneously released during the reduction of metals and non-metals from ore particles and also directly directly in their composition, were obtained in exactly the same way Since crystals are also transformed, ultimately, into grains of non-metallic slag waste, due to the presence of this circumstance, the following characteristic pattern will be observed in the cavity of the used mobile working chamber.

Consisting of particles of non-metallic waste sticking together, enlarged lumps of slag associates, making a “flight” in the thickness of the same “tornado” of “E” streams, and moving into them under the influence of the same force factors noted earlier, from the peripheral regions of the vortex “ E ”, to its core-center, such“ tail ”structural formations will ultimately, without fail, prove to be displaced directly into the zone of“ constantly maintained calm calm ”.

Due to the fact that the above-mentioned small slag associates adhere well to any surface that comes into close contact with them, they will form in this way, on the peripheral lateral parts of the core of the core, the seed 7, a loose intermediate non-metallic “sticky” layer “G”, on which the “capture” and “fixation” of the “overgrown” granules of the multicomponent alloy obtained in the vortex flows are subsequently carried out. In addition, and enlarged “flakes” of the same alloy flying past the outer surface of the seed rod 7, again, maybe a little earlier, maybe a little later they will be “deliberately” thrown back onto the plane of the expanding ring single crystal structure “I” (see figure 2).

The fact of the obligatory onset of this event is determined, first of all, by the presence of the influence of the next action, which determines the inevitability of the moment of its practical implementation, an essential technical circumstance.

The “grains” of alloy flying past the seed rod 7 “enlarged” in the jets of the vortex ultimately fall either directly onto the split petal membrane-washer 17 directly over the nozzle inlet 10 (see FIG. 4), or are located on the “intermediate” ”The“ isthmus ”section adjacent to this zone itself, the surface of the bottom 6. Both those and other“ pieces ”of the multicomponent alloy will be necessarily moved by the cheek surface 3 moving and periodically making angular rotations, from the original place ia of its “basing”, directly to the central outlet of the jet of compressed air, an outlet made in the center of the above structural element 17.

Since the pressure created in the cavity of the working chamber by the blowing nozzles 10 of the air flows is quite high (overpressure corresponds to a value of 0.4-0.6 kgf / cm ² ), metal fragments from this Ti alloy falling into their last jets are made; Fe; Al; in the literal sense of the word, they are simply “kicked out” of the zone of their location and are thrown up and to the side at oblique angles α and β.

Having encountered any obstacle on the trajectory of this kind of “approach”, for example, the surface of a moving cheek-piston 3, these pieces of metal zirconium bounce off of it and change, as a result, the direction of their movement. In this case, there again appears a rather high probability that these “thrown up” metal “fragments” will be thrown directly onto the outer surface of the annular columnar formation “I” grown on the seed rod 7. Indeed, in this central zone of the working chamber, unlike all the others located on its periphery, "calm calm" always reigns, because the so-called "eye of the storm" is located in this area. If, even after this single “jump” is completed, a piece of metal flies past the surface of the “I” single crystal grown in the device, the previously indicated cycle of repeated “tosses” and “flights” will continue until this event nevertheless turns into "Practically realized."

Ultimately, granules from this alloy that got on the surface of the “I” single crystal during the execution of a series of such “bounces” and “rebounds” “tightly” “stick” to his body and continue together with the components of this crystalline structure and which had previously settled on it the body "base" layers to carry out a joint process of its further growth.

An increase in the uniformity of the distribution of the thickness of the components of the annular columnar single crystal “I” along its entire length of the walls, as well as an increase in the degree of purity of its outer side surface during its formation, is ensured by the constant execution of a series of turns carried out with a small angular velocity (2-4 rpm), around its longitudinal axis of symmetry.

To eliminate the appearance of possible “gross” errors obtained by this formation in a ring shape, on the second, already “reverse” segment of the path of its movement along the surface of the cavity of the housing 6, the direction of rotation of this crystalline structure “I” is reversed (it is reversed).

All the above events performed in the cavity of the mobile working chamber are completed and proceed in its volume throughout the entire cycle of its movement inside the housing used to process this device itself. When this prefabricated assembly reaches the extreme front right position; (the straight segment of the path of its movement has been completely traveled), the travel limit switch (not shown in the drawing) is triggered, and the translational movement of the working chamber begins with the transfer of its constituent structural elements, bringing them closer to the "left" rear part of the device 6.

The direction of the angular movement of the components making up this chamber around its own longitudinal axis of symmetry, at this point in time, as already mentioned, also changes to the opposite.

Thus, during the second, “final” stage of the cycle of its reverse movement, in the volume of the working chamber, the last stages of the process of forming the body of the “And” columnar ring single crystal synthesized on the seed rod 7 are completely completed, which ensures that the last specified processing technology produces high-quality “conditions” . That is, as if a “finishing” “refinement” of this already almost completely final product is carried out to obtain the required technical parameters specified by it and stipulated by the technical conditions. Ultimately, moving in the opposite direction, the working chamber again returns to its original initial position it occupied, that is, it again falls into the cavity of the removable cap 4, in which its volume was previously loaded with the processed raw material 1.

In the process of passing through the working chamber of the corresponding areas of the housing 6, a periodic “bleeding” of the volumes of volatile gas compounds newly obtained in the process of recovering metals and non-metals from ore particles from the ore particles from the ore particles as well as excessively received portions of compressed air supplied thereto was periodically “bleed”. To carry out this operation, we used outlet pipes 18 fixed on the device casing 6, the cavity of which was connected to the volume of the working chamber at the moments of operation of the pressure reducing valves 19. The latter were opened if the overpressure in the cavity of the mobile working chamber exceeded the value specified by the processing technology .

The opening of the pressure reducing valves 19, in the end, provided the emission of gas volumes unnecessary for the process of forming the “I” single crystal directly into the outside atmosphere surrounding the device.

Since on the lateral outer surface of the right and left piston-shaped cheeks 3, which are part of the mobile working chamber, it is planned to install elastic “slippery” seals to seal its volume, then to prevent their premature failure (seals are not shown in the drawing), during manufacture the proposed device used the following design methods.

Formed in the places of installation communicating with the internal volume of the housing 6 and used in the device structural elements 10; fourteen; 18 curvilinear recesses, obtained as if by themselves when mutually crossing contacting each other mating curved surfaces of the bodies of revolution, are filled with smoothing washers (see figure 3 - position 16; figure 4 - position 17). The latter are made in the form of petal membranes with a “hole” in the center, installed in the area of placement of the lower outlet openings of the blowing nozzles 10, and also the outlet pipes 18, and elastic rubber is used as the material for their manufacture.

When carrying out the installation of the focusing nozzles 14 in the cavity of the mounting sleeves 15 (see Fig. 3), the above “curved” recesses on the inner surface of the housing 6 are filled in tightly pressed into these powder obtained on its inner surface-cavity, consisting of small particles of cobalt or cast iron (washer pos.17 - figure 3).

And in this, and in another case, the use of the above structural elements allows you to completely eliminate the possibility of forming on the inner side surface of the housing 6, at the intersection of it with the surface of the nodes 10, 14, 18 sharp cutting edges. It turns out that all the mating zones of the latter with the housing 6 are, as it were, “flush” with neighboring sections of its inner surface, and have absolutely smooth planes at the points of possible passage of the cheek-pistons 3 on the lateral outer surface and their sealing seals.

The installation of the F-shaped magnetic generators 11 with the nozzles 14 located in their lower part on the surface of the housing 6 is carried out using rigidly fixed guide hollow sleeves 15, and through the use of fastening threads made on the mating surfaces of the above parts (see Fig. 3). To increase the accuracy of the mutual fixation of the structural components that are assembled into a single unit, 2 lock nuts can be additionally strung on the mounting thread on the external surface of the focusing nozzle 14 (the above-mentioned performance features of these parts are not reflected in the drawing).

So, after the mobile working chamber with the columnar ring monocrystal intermetallic "I" formed inside its volume completely occupies its original initial position in the volume of the cap removable cap 4, and the fact of the occurrence of this event will receive the corresponding signal from the sensor used for this fixing its final position (for example, from the limit switch), all systems that service the operation of the installation are disconnected from the applied external power sources (drive; electric tertiary circuits for supplying electric current to magnetic generators supplying jets of compressed air to the nozzle from the external line conducting this product).

Subsequently, from the housing 6, by disconnecting from each other annular flat docking flanges 5, carried out using quick-release fasteners (not shown in the drawing), the cap cap 4 is removed. Then, the lock nut 9 is unscrewed, fixing on the threaded neck of the roller 8 a piston-shaped left cheek 3, and the latter is “pulled out” from its previous position in the aforementioned node. This opens up free open access to the annular columnar formation “I” formed in this chamber (see FIG. 2), and the latter is removed from the cavity of this device without any special difficulties.

"Comfortable" conditions for dismantling the previously obtained in the device of this crystalline structure are provided, first of all, by the fact that between the inner side surface of the hole formed at its center and the core-seed 7 is an intermediate loose layer "G" (see figure 2), entirely consisting of slag waste accumulated in this area.

After removing the “I” single crystal from the device, the finely dispersed slags partially filling the central bore hole contained in it are easily shaken out when even a “minor” mechanical effect is applied to them.

The processing cycle on this can be considered completely completed. It should also be emphasized on the fact that the power supplies (not shown) that are capable of supplying winding coils of the coil 13 generators 11 pulses are equipped with corresponding electronic circuits, with the help of which these signals are formed in the form of a “saw tooth” and are assembled in a kind stacked packets, (as if in a pseudophase), the components of which the elements have corresponding angular displacements relative to similar neighboring ones (see Fig. 5), and the latter also have additional contours that provide the possibility adjusting the magnitude of tension and oscillation frequency in a zone processing sawtooth magnetic fields (i.e., the magnitude of current, voltage, frequency supplied electric signals).

As noted earlier, by performing the above changes in the main technological parameters of the process of processing the same mixture from the starting raw materials, it is guaranteed to obtain finished products represented by intermetallic compounds with a very different structural formula and, accordingly, having different physicochemical properties.

The technical and economic indicators characterizing the degree of efficiency of the processing performed with its use, recorded during the use to achieve the above goals when applying this type of design of the proposed device, made it possible to determine the following:

With a device length of 1.5 meters and its width, taking into account the dimensions of the systems serving its operation of 1.2 m, as well as with a case diameter of 0.44 m, and if it is operated in 3 shift modes, it is ensured production of 0.7–0.8 tons of metal intermetallic alloys consisting of titanium, iron and aluminum within one day. Electricity consumption per ton of multicomponent alloy obtained in accordance with the proposed technology is 2.7-3.2 thousand kW / h.

Given all of the above, we can come to the following conclusion. Using the proposed method for producing alloys based on titanium, iron and aluminum, as well as the device used to implement this technology, provides a significant reduction in the cost of electric energy required for processing the feedstock into a finished final product. That is, the application of the proposed technical solutions creates the conditions for reducing its consumption by 8-15 times in relation to the amount that is necessary to obtain a similar product, carried out using the melts constituting the latter, metals formed in addition to involving this goals, rather complex technical systems containing various kinds of melting units.

In addition, if the processing process is carried out in accordance with the proposed method, the latter proceeds during only one technological transition, and no harmful substances are emitted into the surrounding equipment, which inevitably accompanies the methods of obtaining the same in accordance with the “classical” scheme the end product itself.

It should also be noted that the metal alloy itself, which is completely ready for subsequent use, is formed in the form of a continuous columnar ring single crystal with a practically unchanged intrinsic configuration and including titanium, iron, and aluminum intermetallic compounds obtained from the raw materials used, the content of which in the volume of this structure itself is 99.9999% -99.99999%.

All varieties made besides using the same starting raw material and the alloys listed above have a sufficiently low specific bulk density and have a sufficiently high refractoriness.

Obtained using the proposed technology, columnar ring single crystals based on titanium, iron and aluminum can be quite successfully used to meet the relevant needs of existing industrial production without any additional operations for their “final” refinement.

The introduction of the proposed processing process, as well as the device used during its implementation, does not require significant investment and is not associated with the need to use significant labor costs, as well as the long lead times required for the preparation of production.

The choice of materials and components included in the composition of the proposed device was made taking into account the possibility of using them as the latter similar, widespread and used in equipment designed to perform technologies similar to the above. This proposed device itself is characterized by a high degree of simplicity of its design, and as a result, it has good performance with respect to its own operational reliability.

Claims (2)

1. A method of producing an alloy based on titanium from an aqueous suspension of ore particles containing titanium compounds, including the generation of magnetic fields applied to portions of the processed raw material, the recovery of metals from ores with continuous mixing of the raw material, followed by accumulation and formation of the product in the form of an annular single crystal consisting of an intermetallic compound selected from TiAl _3, TiFeAl _2, TiAl ₂ Fe, TiFe _3, and its discharging at the same time as the original feed mass, an aqueous slurry comprising ore material particles with the dispersion in the range 0,001-0,008 mm and in an amount of 40-70% by volume of an aqueous suspension, wherein the magnetic fields as used sawtooth magnetic field with intensity 3 × 10 ⁴ ÷ 1,5 · 10 ⁵ A / m and a frequency oscillations of 20-80 units of impulses within one minute, which form clusters in the form of field lines having a configuration as close as possible to the outline of the spatial formation obtained by rotating a elongated rectangle that rotates relative to its own longitudinal axis and symmetry, while the process of restoration and formation of the aforementioned single crystal is carried out on a metal rod located in a sealed mobile working chamber installed in the housing and performing reciprocating movements while the housing is making angular rotations relative to its own longitudinal axis of symmetry, with gas supply to the raw material layers jets consisting of compressed atmospheric air and carbon as a reducing agent present in the composition of compressed gases, and mixing iem original feed mass by transferring it in the inner volume of the working chamber, crushing and subsequent extrusion separate microportions feedstock flowing under the influence of shocks produced by intersecting streams of compressed air supplied under overpressure 0,4-6,0 kg / cm ^2. 2. Device for producing an alloy based on titanium from an aqueous suspension of ore particles containing titanium compounds, comprising a housing consisting of two parts, one of which is removable and made in the form of a cap removable cap connected by ring flat flanges with its fixed base in the form of a cylindrical shell, with the formation of a prefabricated unit, while the length of the fixed base of the prefabricated unit is 80-85% of its entire length, and a sealed mobile working chamber is installed in the cavity of the housing, which the second is made with the possibility of reciprocating movement, and the housing is made to rotate relative to its own longitudinal axis of symmetry, while the working chamber is equipped with left and right cheeks in the form of pistons mounted on the roller, and a metal rod is mounted between them through the walls of the fixed base of the prefabricated assembly, focusing magnetic nozzles were generated, generating clusters of magnetic field lines, mounting sleeves and blowing nozzles intended for entering the polo case of compressed air jets and having both radial and tangential angles of inclination of 30-45 ° relative to the surface of the body, and in the left and right halves of the fixed base of the assembly, exhaust pipes are installed to output excess accumulated in the working chamber into the external atmosphere gas volumes, and in the upper part of the removable cap there is a feed hopper of raw materials, the volume of which through the through hatch available in this part of the housing is in communication with the cavity of the working chamber located under it.