NZ740209A - Refined oil compositions and methods for making - Google Patents

Refined oil compositions and methods for making

Info

Publication number
NZ740209A
NZ740209A NZ740209A NZ74020916A NZ740209A NZ 740209 A NZ740209 A NZ 740209A NZ 740209 A NZ740209 A NZ 740209A NZ 74020916 A NZ74020916 A NZ 74020916A NZ 740209 A NZ740209 A NZ 740209A
Authority
NZ
New Zealand
Prior art keywords
oil
fatty acid
less
acid ester
microorganism
Prior art date
Application number
NZ740209A
Other versions
NZ740209B2 (en
Inventor
Nasrin Tabayehnejad
Michael Lenn Stefanski
Chris Connor Luigart
Original Assignee
Dsm Ip Assets Bv
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dsm Ip Assets Bv filed Critical Dsm Ip Assets Bv
Publication of NZ740209A publication Critical patent/NZ740209A/en
Publication of NZ740209B2 publication Critical patent/NZ740209B2/en

Links

Classifications

    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS OR COOKING OILS
    • A23D9/00—Other edible oils or fats, e.g. shortenings or cooking oils
    • A23D9/02—Other edible oils or fats, e.g. shortenings or cooking oils characterised by the production or working-up
    • A23D9/04—Working-up
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING OR TREATMENT THEREOF
    • A23C9/00—Milk preparations; Milk powder or milk powder preparations
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING OR TREATMENT THEREOF
    • A23C9/00—Milk preparations; Milk powder or milk powder preparations
    • A23C9/152—Milk preparations; Milk powder or milk powder preparations containing additives
    • A23C9/1528—Fatty acids; Mono- or diglycerides; Petroleum jelly; Paraffine; Phospholipids; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS OR COOKING OILS
    • A23D9/00—Other edible oils or fats, e.g. shortenings or cooking oils
    • A23D9/02—Other edible oils or fats, e.g. shortenings or cooking oils characterised by the production or working-up
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K50/00—Feeding-stuffs specially adapted for particular animals
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K50/00—Feeding-stuffs specially adapted for particular animals
    • A23K50/80—Feeding-stuffs specially adapted for particular animals for aquatic animals, e.g. fish, crustaceans or molluscs
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/52—Adding ingredients
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/115—Fatty acids or derivatives thereof; Fats or oils
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/40—Complete food formulations for specific consumer groups or specific purposes, e.g. infant formula
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36—Carboxylic acids; Salts or anhydrides thereof
    • A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/10—Refining fats or fatty oils by adsorption
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/12—Refining fats or fatty oils by distillation
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/16—Refining fats or fatty oils by mechanical means
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/80—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in fisheries management
    • Y02A40/81—Aquaculture, e.g. of fish
    • Y02A40/818—Alternative feeds for fish, e.g. in aquacultures

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Polymers & Plastics (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Food Science & Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Microbiology (AREA)
  • Nutrition Science (AREA)
  • Mycology (AREA)
  • Birds (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Mechanical Engineering (AREA)
  • Zoology (AREA)
  • Animal Husbandry (AREA)
  • Epidemiology (AREA)
  • Pediatric Medicine (AREA)
  • Biophysics (AREA)
  • Insects & Arthropods (AREA)
  • Marine Sciences & Fisheries (AREA)
  • Emergency Medicine (AREA)
  • Dermatology (AREA)
  • Fats And Perfumes (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Dairy Products (AREA)
  • Edible Oils And Fats (AREA)
  • Lubricants (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

A refined oil comprising at least one polyunsaturated fatty acid (PUFA), wherein the oil has a fatty acid ester of monochloropropanediol, epoxypropanol, and mixtures thereof in an amount of 10 ppm or less, and processes for producing the oil. The oil is preferably a microbial or marine oil.

Claims (19)

THE CLAIMS DEFINING THE INVENTION ARE AS FOLLOWS:
1. A refined microbial oil or marine oil comprising at least 35% of at least one polyunsaturated fatty acid (PUFA), wherein the PUFA is selected from arachidonic acid (ARA), eicosapentaenoic acid (EPA), docosahexaenoic acid (DHA), and mixtures thereof, wherein the oil has a fatty acid ester of monochloropropanediol, epoxypropanol, and mixtures thereof in an amount of 10 ppm or less, and an anisidine value (AnV) of less than 20.
2. The oil of claim 1, wherein the fatty acid ester of monochloropropanediol is bound 2- monochloropropane-1,2-diol (2-MCPD) and/or bound 3-monochloropropane-1,2-diol (3- MCPD), and/or the fatty acid ester of epoxypropanol is bound 2,3-epoxypropanol.
3. The oil according to claims 1 or 2, wherein the fatty acid ester is in an amount of 1 ppm or less, preferably in an amount 0.3 ppm or less, preferably in an amount of 0.1 ppm or less.
4. The oil according to any one of claims 1-3, wherein the oil has an anisidine value (AnV) of less than 10.
5. The oil according to any one of claims 1-4, comprising at least 40% of the PUFA.
6. The oil according to claim any one of claims 1-5, wherein the oil has been produced by a microorganism, wherein the microorganism is selected from the group comprising microalgae, bacteria, fungi and protists, preferably wherein; (i) the microorganism is of the genus Crypthecodinium, preferably of the species Crypthecodinium cohnii, (ii) the microorganism is of the genus Thraustochytrium, preferably of the species Schizochytrium sp, (iii) the microorganism is of the genus Mortierella, preferably of the species Mortierella alpina, and/or wherein the oil is produced by a genetically modified organism.
7. The oil according to any one of claims 1-6, wherein a second oil is added to the oil, preferably wherein (i) the second oil is a vegetable oil and/or (ii) the second oil has a fatty acid ester of monochloropropanediol, epoxypropanol, and mixtures thereof in an amount of 3 ppm or less, preferably, wherein the second oil has a fatty acid ester of monochloropropanediol, epoxypropanol, and mixtures thereof in an amount of 1 ppm or less.
8. The oil according to any one of claims 1-7, wherein the oil has been subjected to a process comprising treating the oil with a silica, a bleaching earth, an activated carbon, and combinations thereof, and deodorizing the oil, in which the oil is subject to steam under heat.
9. A food product, cosmetic or pharmaceutical composition for a non-human or human, comprising the oil of any one of claims 1-8, preferably, (i) the food product is an infant formula, (ii) the food product is a milk, a beverage, a therapeutic drink, a nutritional drink, or a combination thereof, or (iii) the food product is a dietary supplement.
10. A process for reducing and/or preventing the formation, or decreasing the level of, at least one fatty acid ester in a microbial oil or a marine oil comprising: (a) treating the oil with a combination of a silica, and an activated carbon, and optionally, a bleaching earth; and (b) deodorizing the oil, in which the oil is subjected to steam under heat, wherein the temperature of the deodorization is 170-190 C; wherein the fatty acid ester is a fatty acid ester of monochloropropanediol, epoxypropanol, and mixtures thereof, and wherein the microbial or marine oil comprises (i) at least 35% of at least one polyunsaturated fatty acid (PUFA), wherein the PUFA is selected from arachidonic acid (ARA), eicosapentaenoic acid (EPA), docosahexaenoic acid (DHA), and mixtures thereof; and (ii) and an anisidine value (AnV) of less than 20, and wherein the fatty acid ester is in an amount of 10 ppm or less.
11. The process of claim 10, wherein the rate of steam is 1-10 wt.%.
12. The process according to claim 10 or 11, wherein the deodorization is performed using a short path distillation apparatus, a wiped-film evaporator, a thin-film evaporator, or a rotating packed bed deodorizer.
13. The process according to any one of claims 10-12, wherein the residence time of the oil during the deodorization process is less than two minutes.
14. The process according to any one of claims 10-13, wherein the fatty acid ester of monochloropropanediol is bound 2-monochloropropane-1,2-diol (2-MCPD) and/or bound 3- monochloropropane-1,2-diol (3-MCPD) and/or the fatty acid ester of epoxypropanol is bound 2,3-epoxypropanol.
15. The process according to any one of claims 10-14, wherein the fatty acid ester is in an amount less than 5 ppm, preferably in an amount less than 1 ppm, preferably in an amount less than 0.3 ppm.
16. The process according to any one of claims 10-15, wherein the oil has an anisidine value (AnV) of less than 10.
17. The process according to any one of claim 10-16, wherein oil comprises at least 40% of the desired PUFA.
18. The process according to any one of claims 10-17, wherein the oil has been produced by a microorganism, wherein the microorganism is selected from the group comprising microalgae, bacteria, fungi and protists, preferably: (i) the microorganism is of the genus Crypthecodinium, preferably of the species Crypthecodinium cohnii; (ii) the microorganism is of the genus Thraustochytrium, preferably of the species Schizochytrium sp; or (iii) the microorganism is of the genus Mortierella.
19. The process according to claim 18, wherein the microorganism is of the species Mortierella alpina, and/or wherein the oil is produced by a genetically modified organism.
NZ740209A 2016-08-25 Refined oil compositions and methods for making NZ740209B2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201562209505P 2015-08-25 2015-08-25
PCT/US2016/048781 WO2017035403A1 (en) 2015-08-25 2016-08-25 Refined oil compositions and methods for making

Publications (2)

Publication Number Publication Date
NZ740209A true NZ740209A (en) 2024-11-29
NZ740209B2 NZ740209B2 (en) 2025-03-04

Family

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Also Published As

Publication number Publication date
US11672258B2 (en) 2023-06-13
US20180242609A1 (en) 2018-08-30
AU2021201384A1 (en) 2021-03-18
KR102716618B1 (en) 2024-10-14
EP4595778A3 (en) 2025-10-22
RU2018110375A (en) 2019-09-26
RU2747879C2 (en) 2021-05-17
MX390089B (en) 2025-03-20
US20230270129A1 (en) 2023-08-31
CA2996526A1 (en) 2017-03-02
EP3341457B1 (en) 2025-11-05
CN108138079A (en) 2018-06-08
KR20180048715A (en) 2018-05-10
EP4595778A2 (en) 2025-08-06
WO2017035403A1 (en) 2017-03-02
BR112018003578A2 (en) 2018-09-25
RU2018110375A3 (en) 2020-02-21
MY204082A (en) 2024-08-06
HK1257691A1 (en) 2019-10-25
MX2018002297A (en) 2018-06-06
SG10202001800WA (en) 2020-04-29
AU2016310503A1 (en) 2018-03-22
EP3341457A1 (en) 2018-07-04
EP3341457A4 (en) 2019-05-01
AU2021201384B2 (en) 2023-04-27
PH12018500410A1 (en) 2018-08-29

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Free format text: PATENT RENEWED FOR 1 YEAR UNTIL 25 AUG 2026 BY ABHISHEK KUMAR - CPA-PTO PAYMENTS

Effective date: 20250710