NZ521121A - Wireless communication using well casing - Google Patents

Wireless communication using well casing

Info

Publication number
NZ521121A
NZ521121A NZ521121A NZ52112101A NZ521121A NZ 521121 A NZ521121 A NZ 521121A NZ 521121 A NZ521121 A NZ 521121A NZ 52112101 A NZ52112101 A NZ 52112101A NZ 521121 A NZ521121 A NZ 521121A
Authority
NZ
New Zealand
Prior art keywords
formation
piping structure
induction choke
casing
downhole
Prior art date
Application number
NZ521121A
Inventor
Harold J Vinegar
Robert Rex Burnett
William Mountjoy Savage
Frederick Gordon Carl
Llya Emil Berchenko
Original Assignee
Shell Int Research
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shell Int Research filed Critical Shell Int Research
Publication of NZ521121A publication Critical patent/NZ521121A/en

Links

Classifications

    • EFIXED CONSTRUCTIONS
    • E21EARTH DRILLING; MINING
    • E21BEARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B17/00Drilling rods or pipes; Flexible drill strings; Kellies; Drill collars; Sucker rods; Cables; Casings; Tubings
    • E21B17/003Drilling rods or pipes; Flexible drill strings; Kellies; Drill collars; Sucker rods; Cables; Casings; Tubings with electrically conducting or insulating means
    • EFIXED CONSTRUCTIONS
    • E21EARTH DRILLING; MINING
    • E21BEARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B34/00Valve arrangements for boreholes or wells
    • E21B34/06Valve arrangements for boreholes or wells in wells
    • E21B34/066Valve arrangements for boreholes or wells in wells electrically actuated
    • EFIXED CONSTRUCTIONS
    • E21EARTH DRILLING; MINING
    • E21BEARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B34/00Valve arrangements for boreholes or wells
    • E21B34/06Valve arrangements for boreholes or wells in wells
    • E21B34/08Valve arrangements for boreholes or wells in wells responsive to flow or pressure of the fluid obtained
    • EFIXED CONSTRUCTIONS
    • E21EARTH DRILLING; MINING
    • E21BEARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B34/00Valve arrangements for boreholes or wells
    • E21B34/16Control means therefor being outside the borehole
    • EFIXED CONSTRUCTIONS
    • E21EARTH DRILLING; MINING
    • E21BEARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B43/00Methods or apparatus for obtaining oil, gas, water, soluble or meltable materials or a slurry of minerals from wells
    • E21B43/14Obtaining from a multiple-zone well
    • EFIXED CONSTRUCTIONS
    • E21EARTH DRILLING; MINING
    • E21BEARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B47/00Survey of boreholes or wells
    • E21B47/12Means for transmitting measuring-signals or control signals from the well to the surface, or from the surface to the well, e.g. for logging while drilling
    • E21B47/13Means for transmitting measuring-signals or control signals from the well to the surface, or from the surface to the well, e.g. for logging while drilling by electromagnetic energy, e.g. radio frequency

Abstract

A petroleum well having a borehole extending into a formation is provided. A piping structure is positioned within the borehole, and an induction choke is positioned around the piping structure downhole. A communication system is provided along the piping structure between a surface of the well and the induction choke. A downhole module is positioned on an exterior surface of the piping structure and is configured to measure characteristics of the formation. The formation characteristics, such as pressure and resistivity, are communicated to the surface of the well along the piping structure.

Description

521121 WIRELESS COMMUNICATION IN A PETROLEUM WELL BACKGROUND OF THE INVENTION Field of the Invention The present invention relates in general to petroleum wells, and in particular to a petroleum well having a 5 casing which is used as a conductive path to transmit wireless spread spectrum communications between surface equipment and a downhole module used to measure physical characteristics of a petroleum formation or condition of well structures.
Description of Related Art Several methods have been devised to place electronics, sensors, or controllable valves downhole along an oil production tubing string, but all such known devices typically use an internal or external cable along 15 the tubing string to provide power and communications downhole. It is, of course, highly undesirable and in practice difficult to use a cable along the tubing string either integral to the tubing string or spaced in the annulus between the tubing string and the casing. The use 20 of a cable presents difficulties for well operators while assembling and inserting the tubing string into a borehole. Additionally, the cable is subjected to corrosion and heavy wear due to movement of the tubing string within the borehole. An example of a downhole 25 communication system using a cable is shown in PCT/EP97/01621.
U. S. Patent No. 4,839,644 describes a method and system for wireless two-way communications in a cased borehole having a tubing string. However, this system INTELLECTUAL PROPERTY UH=1(5E| OF M-Z 21 JAN 2005 RECEIVED describes a communication scheme for coupling electromagnetic energy in a TEM mode using the annulus between the casing and the tubing. This inductive coupling requires a substantially nonconductive fluid 5 such as crude oil in the annulus between the casing and the tubing.
Therefore, the invention described in U. S. Patent No. 4,839,644 has not been widely adopted as a practical scheme for downhole two-way communication. Another system 10 for downhole communication using mud pulse telemetry is described in U. S. Patent Nos. 4,648,471 and 5,887,657. Although mud pulse telemetry can be successful at low data rates, it is of limited usefulness where high data rates are required or where it is undesirable to have 15 complex, mud pulse telemetry equipment downhole. Other methods of communicating within a borehole are described in U.S. Patent Nos. 4,468,665; 4,578,675; 4,739,325; ,130,706; 5,467,083; 5,493,288; 5,576,703; 5,574,374; and 5,883,516. Similarly, several permanent downhole 20 sensors and control systems have been described in U.S.
Pat. Nos. 4,972, 704; 5,001,675; 5,134,285; 5,278,758; 5,662,165; 5,730,219; 5,934,371; and 5,941,307.
Due to the limited success of wireless communication within a borehole, the current use of downhole 25 measurement and control equipment is minimal. A lack of downhole measurement and control restricts the ability to maximize economic return by optimizing production of the well.
It would, therefore, be a significant advance in the operation of petroleum wells if an alternate means for providing communications within a well were provided.
More specifically, it would be advantageous if downhole physical characteristics of the formation could be easily..
INTELLECTUAL °R0PERTv QFICE Of -s\7. 2 1 JAN 2005 RECEIVED communicated to the surface of the well. This information could then be used to increase the aggregate recovery of formation reserves, and would thereby optimize production of the well.
BRIEF SUMMARY OF THE INVENTION The problems associated with communicating in the borehole of a petroleum well are solved by the present invention.
A petroleum well according to the invention 10 comprises: a borehole extending into a formation; a piping structure including a casing positioned within the borehole; a downhole module positioned on the outside of the 15 casing for collecting formation characteristic data of the formation; a communication system operably coupled to the piping structure and module such that the formation characteristic data can be communicated along the piping 20 structure as a time-varying signal; and an induction choke positioned concentrically around the piping structure; wherein the formation characteristic data is communicated along the piping structure between a current 25 supply point and the induction choke.
In a petroleum well having a borehole extending into a formation and having a piping structure positioned within the borehole, a method for assessing the formation in accordance with the invention comprises the steps of: 3 0 sensing a formation characteristic of the formation using sensors external to the piping structure; and rr 2 1 JAN 2005 RECEIVED communicating the formation characteristic along the piping structure as a time varying signal applied to the piping structure, wherein the communicating step further 5 comprises: providing an induction choke positioned concentrically around the piping structure; and communicating the formation characteristic along the piping structure between a current supply point and the 10 induction choke.
BRIEF DESCRIPTION OF THE DRAWINGS Figure 1 A is a schematic of a petroleum well having a downhole module attached to a casing, the downhole module being configured to measure formation 15 characteristics according to the present invention. 4 WO 01/65066 ' PCT/US01/06907 DESCRIPTION OF THE PREFERRED EMBODIMENTS As used in the present application, a "piping structure" can be one single pipe, a tubing string, a well casing, a pumping rod, a series of interconnected pipes, rods, rails, trusses, lattices, supports, a branch or lateral extension of a well, a network of interconnected pipes, or other structures known to one of ordinary skill in the art The preferred embodiment makes use of the 10 invention in the context of an oil well where the piping structure comprises tubular, metallic, electrically-conductive pipe or tubing strings, but the invention is not so limited. For the present invention, at least a portion of the piping structure needs to be electrically conductive, such electrically conductive portion may be the entire piping structure (e.g., steel pipes, copper pipes) or a longitudinal extending electrically conductive portion combined with a longitudinally 15 extending non-conductive portion. In other words, an electrically conductive piping structure is one that provides an electrical conducting path from one location where a power source is electrically connected to another location where a device and/or electrical return is electrically connected. The piping structure will typically be conventional round metal tubing, but the cross-sectional geometry of the piping structure, or any portion thereof, can vary in shape (e.g., round, 20 rectangular, square, oval) and size (e.g., length, diameter, wall thickness) along any portion of the piping structure.
A "valve" is any device that functions to regulate the flow of a fluid. Examples of valves include, but are not limited to, sub-surface safety valves used to control fluid flow in well tubulars, and bellows-type gas-lift valves and controllable gas-lift valves each of which may be 25 used to regulate the flow of lift gas into a tubing string of a well. The internal workings of valves can vary greatly, and in the present application, it is not intended to limit the valves described to any particular configuration, so long as the valve functions to regulate flow. Some of the various types of flow regulating mechanisms include, but are not limited to, ball valve configurations, needle valve configurations, gate valve configurations, and cage valve 30 configurations. Valves can be mounted downhole in a well in many different ways, some of which include tubing conveyed mounting configurations, side-pocket mandrel configurations, or permanent mounting configurations such as mounting the valve in an enlarged tubing pod.
The term "modem" is used generically herein to refer to any communications device for transmitting and/or receiving electrical communication signals via an electrical conductor (e.g., 35 metal). Hence, the term is not limited to the acronym for a modulator (device that converts a voice or data signal into a form that can be transmitted)/demodulator (a device that recovers an original signal after it has modulated a high frequency carrier). Also, the term 'modem'ias-used- JTRLECTUAL PROPERS OF^CE 0?' fti.7 2 1 JAN 2005 DECEIVED WO 01/65066 PCT/USO1/06907 herein is not limited to conventional computer modems that convert digital signals to analog signals and vice versa (e.g., to send digital data signals over the analog Public Switched Telephone Network). For example, if a sensor outputs measurements in an analog format, then such measurements may only need to be modulated (e.g., spread spectrum modulation) and transmitted—hence no analog-to-digital conversion is needed. As another example, a 10 relay/slave modem or communication device may only need to identify, filter, amplify, and/or retransmit a signal received.
The term "processor" is used in the present application to denote any device that is capable of performing arithmetic and/or logic operations. The processor may optionally include a control unit, a memory unit, and an arithmetic and logic unit.
The term "sensor" as used in the present application refers to any device that detects, determines, monitors, records, or otherwise senses the absolute value of or a change in a physical quantity. Sensors as described in the present application can be used to measure temperature, pressure (both absolute and differential), flow rate, seismic data, acoustic data, pH level, salinity levels, valve positions, or almost any other physical data.
As used in the present application, "wireless" means the absence of a conventional, insulated wire conductor e.g. extending from a downhole device to the surface. Using the tubing and/or casing as a conductor is considered "wireless." The term "electronics module" in the present application refers to a control device. Electronics modules can exist in many configurations and can be mounted downhole in many 25 different ways. In one mounting configuration, the electronics module is actually located within a valve and provides control for the operation of a motor within the valve. Electronics modules can also be mounted external to any particular valve. Some electronics modules will be mounted within side pocket mandrels or enlarged tubing pockets, while others may be permanently attached to the tubing string. Electronics modules often are electrically connected 30 to sensors and assist in relaying sensor information to the surface of the well. It is conceivable that the sensors associated with a particular electronics module may even be packaged within the electronics module. Finally, the electronics module is often closely associated with, and may actually contain, a modem for receiving, sending, and relaying communications from and to the surface of the well. Signals that are received from the surface by the electronics module are 35 often used to effect changes within downhole controllable devices, such as valves. Signals sent or relayed to the surface by the electronics module generally contain information about downhole physical conditions supplied by the sensors.
INTELLECTUAL PR0PFRTv 0FICE OF ;\i.Z •jnni 21 WO 01/65066 PCT/USO1/06907 In accordance with conventional terminology of oilfield practice, the descriptors "upper," "lower," "uphole," and "downhole" as used herein are relative and refer to distance along hole depth from the surface, which in deviated or horizontal wells may or may not accord with vertical elevation measured with respect to a survey datum.
The term "formation" as used in the present application refers to a bed or deposit 10 composed throughout of substantially the same kinds of rock. A formation may or may not contain petroleum products.
Referring to FIG. 1 in the drawings, a petroleum well 10 having a wireless smart well casing 12 is illustrated. Petroleum well 10 includes a borehole 14 extending into a formation from a surface 16 to a production zone 18 that is located downhole. The casing 12 is disposed in 15 borehole 14 and includes a structure of the type conventionally employed in the oil and gas industry. The casing 12 is typically installed in sections and is secured in borehole 14 during well completion with cement 34. A tubing string, or production tubing, 26 is generally conventional comprising a plurality of elongated tubular pipe sections joined by threaded couplings at each end of the pipe sections. Oil or gas produced by petroleum well 10 is typically 20 delivered to surface 16 by tubing string 26.
A production platform 27 is located at surface 16 and includes a tubing hanger 28.
Tubing hanger 28 supports tubing string 26 such that the tubing string 26 is concentrically positioned within casing 12. As illustrated in FIG. 1 production platform 27 also includes a gas input throttle 30 to permit the input of compressed gas into an annular space 31 between casing 25 12 and tubing string 26. Conversely, an oulput valve 32 permits the expulsion of oil and gas bubbles from an interior of tubing string 26 during oil production. While FIG. 1 illustrates a gas lift well, the present invention is not so limited, and the gas input throttle valve 30 and its associated input tubing is therefore optional.
Well 10 includes a communication system 44 for providing power and two-way 30 communication signals downhole in well 10. Casing 12 acts as an electrical conductor for communication system 44. In accordance with the present invention, an induction choke 42 is positioned concentrically around casing 12 prior to securing the casing 12 within cement 34. Induction choke 42 serves as a series impedance to electric current flow along the casing 12. The size and material of lower induction choke 42 can be altered to vary the series impedance 35 value; however, the lower induction choke 42 is made of a ferromagnetic material. Induction choke 42 is mounted concentric and external to casing 12, and is typically hardened with epoxy to withstand rough handling.
INTETlect^ OF- Aj.? 2 1 JAN 2005 RECEIVED WO 01/65066 PCT/US01/06907 A means is provided to electrically insulate casing 12 and tubing string 26 from ground connection through surface ancillary tubing connected to valves 30 and 32. Insulators 40 provide this fimction as shown in FIG. 1, but alternative methods exist and will be clear to those of average skill in the art, such as the use of an insulated tubing hanger (not shown) in combination with an electrical isolation tubing joint (not shown). In alternative, another induction choke (not shown) can be placed about the casing above the electrical point of connection 49 of the surface power and communication equipment 44, or two such chokes may be placed individually about the production fluids tubing and the lift gas supply pipe. As noted in the related applications, inductive chokes such as 42 external to the casing act to impede current flow on both casing and tubing at the points where these pass through such inductive chokes.
By electrically isolating a section of casing 12, power and communications signals can be supplied downhole along the casing 12 and tubing 26. While it is not an ideal electrical insulator, the cement 20 can be of low electrical conductivity and provides a degree of electrical isolation between casing 12 and the formation surrounding the well. Induction choke 42 further 20 impedes current flow along casing 12 and tubing 26, thereby allowing the signals to be passed between induction choke 42 and the surface of the well. It is important to note that electrical contact between casing 12 and tubing string 26 does not short circuit the signals travelling along casing 12. Since tubing string 26 is also located within the annulus of induction choke 42, the choke 42 has the same electrical impedance effect on tubing string 26 as on casing 12. More 25 specifically, current travelling down tubing string 26 is effectively blocked from travelling further downhole to a potential ground. Similar protection is provided at the top of tubing string 26 by insulating tubing joints 40. In practice the majority of the current conveyed into the well by the embodiment illustrated in FIG. 1 is carried on the casing, and the tubing contributes negligibly to the conveyance of power to depth in the well.
A computer and power source 44 including a power supply 46 and a spread spectrum communications device (e.g. modem) 48 is disposed outside of borehole 14 at surface 16. The computer and power source 44 is electrically connected to casing 12 at a current supply point 49 for supplying time varying current to the casing 12. Computer and power source 44 is grounded to surface 16. In operation the use of casing 12 as a conductor is lossy because of the imperfect 35 electrical isolation provided by the cement 20. However, the spread-spectrum communications technique is tolerant of noise and low signal levels, and can operate effectively even with losses as high as-lOOdb. mTFllSCTUAL PROPERTV OFFICE OF AL7 2 1 JAN 2005 | RECEIVED WO 01/65066 PCT/US01/06907 As shown in FIG. 1, downhole electronics module 50 is positioned proximate to an exterior surface of the casing 12 prior to completion of the well. Downhole module 50 includes a plurality of sensors 70,72,74, for assessing formation characteristics (i.e. physical characteristics) about the formation that surrounds the well. These sensors could include resistivity sensors, pressure sensors, temperature sensors, flow rate sensors, corrosion sensors, or geophones. Each of these sensors can be used to obtain information about the characteristics of the formation. Additionally, hydrophones could be used to measure acoustic waves in well fluids within casing 12.
It is not obvious that sensors 70 - 74 would be able to measure formation characteristics such as pressure or resistivity, since they are embedded within cement 34 and not in direct 15 connection with formation 18. However, while the permeability of cement 34 is low, it does not provide an absolute hydraulic seal. Since the flow of formation fluids through the cement is prevented by the casing 12, the pressure of fluids in the pore spaces of the cement 34 equilibrates with the pressure in the formation. Rapid changes in formation pressure cannot be measured, but slow changes can be measured, and it is data from slow changes as the reservoir is 20 depleted that are valuable as an indication of reservoir condition.
The same considerations apply to other physical characteristics of the formation 18, such as fluid composition, which would be reflected in resistivity changes. The interpretation of such resistivity data differs from that for a conventional resistivity log of a well as measured by open-hole logging tools. Open-hole resistivity logs reveal the spatial variation of resistivity over the 25 logged section of the formation, measured at essentially a single instant of time. The resistivity log acquired by the methods of the present invention is derived from a locationally static single sensor, but over an extended period of time. In both cases, changes in the resistivity are the features which reveal the condition of the formation: in the open-hole log, these are spatial changes, in the present invention, the changes are a function of time rather than spatial 30 variations.
Downhole module 50 is configured to be mechanically connected to the casing 12 either above or below induction choke 42. Electrical connections to the downhole module 50 are provided by jumpers. Power is received at the downhole module 50 by a jumper connected to casing 12 above the induction choke 42. A ground return jumper is provided that connects 35 downhole module 50 to casing 12 below induction choke 42.
Downhole module 50 also includes a spread spectrum transceiver (not shown) for communicating with modem 48 at the surface of the well 10. The' ■ OFFICE or t\i.7 2 1 JAN 2005 RECEIVE data representing the formation characteristics to be transmitted to the surface of the well 10 for use in optimizing production of the well 10. If multiple downhole modules 50 are positioned on the casing 12, the transceiver in each downhole module is able to communicate with transceivers in the other downhole modules, thereby allowing transceivers to relay signals and providing redundancy in the event of a failure of one of the downhole modules 50.
After positioning induction choke 42 and downhole module 50 on casing 12, the casing 12 is run into borehole 14. Cement 34 is injected into the annulus between the borehole and casing 12 to secure the casing within the borehole 14. The cement 34 also further secures the positioning of the induction choke 42 and the downhole module 50 relative to casing 12.
INTELLECTUAL PROPPRTV OFFICE OF iM7 2 1 JAN 2005 RECEIVED

Claims (15)

WHAT WE CLAIM IS:
1. A petroleum well comprising: a borehole extending into a formation; a piping structure including a casing positioned within the borehole; a downhole module positioned on the outside of the casing for collecting formation characteristic data of the formation; a communication system operably coupled to the piping structure and module such that the formation characteristic data can be communicated along the piping structure as a time-varying signal; and an induction choke positioned concentrically around the piping structure; wherein the formation characteristic data is communicated along the piping structure between a current supply point and the induction choke. *
2. The petroleum wel^according to claim 1, wherein the downhole module includes a pressure sensor.
3. The petroleum well according to claim 1, wherein the downhole module includes a flow rate sensor.
4. The petroleum well according to claim 1, wherein the downhole module includes a temperature sensor.
5. The petroleum well according to claim 1, wherein the downhole module includes a sensor for determining a resistivity value for the formation. iNTFl'i FC'TuAl (V Aiy 11 2 1 JAN 2005 R E C E S V £ i
6. The petroleum well according to claim 1, wherein the downhole module includes a geophone for measuring acoustic waves.
7. The petroleum well according to any one of claims 1 to 6, wherein the induction choke comprises: an upper induction choke positioned concentrically around the piping structure; and a lower induction choke positioned concentrically around the piping structure; and wherein the formation characteristic data is communicated along the piping structure between the upper induction choke and the lower induction choke.
8. In a petroleum well having a borehole extending into a formation and having a piping structure positioned within the borehole, a method for assessing the formation comprising the steps of: sensing a formation characteristic of the formation using sensors external to the piping structure; and communicating the formation characteristic along the piping structure as a time varying signal applied to the piping structure, wherein the communicating step further comprises: providing an induction choke positioned concentrically around the piping structure; and communicating the formation characteristic along the piping structure between a current supply point and the induction choke. 12 INTELLECTUAL PROPERTY OFTceI Of i\!.Z 2 1 JAN 2005 RECE IV ED
9. The method according to claim 8, wherein the sensed formation characteristic is a formation fluid pressure.
10. The method according to claim 8, wherein the sensed formation characteristic is a formation resistivity.
11. The method according to claim 8, wherein the sensed formation characteristic is a formation fluid flow.
12. The method according to claim 8, wherein the sensed formation characteristic is a formation temperature.
13. The method according to any one of claims 8 to 12, wherein the induction choke comprises: an upper induction choke positioned concentrically around the piping structure; and a lower induction choke positioned concentrically around the piping structure; and wherein the communicating step further comprises: communicating the formation characteristic along the piping structure between the upper induction choke and the lower induction choke.
14. A method according to any one of claims 8 to 13, substantially as herein described.
15. A petroleum well according to any one of claims 1 to 7, substantially as herein described. 13 INTELLECTUAL PROPERTV OFFICE 0r i\L/. 21 JAN 2005 RECEIVED
NZ521121A 2000-03-02 2001-03-02 Wireless communication using well casing NZ521121A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US18650300P 2000-03-02 2000-03-02
PCT/US2001/006907 WO2001065066A1 (en) 2000-03-02 2001-03-02 Wireless communication using well casing

Publications (1)

Publication Number Publication Date
NZ521121A true NZ521121A (en) 2005-03-24

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Country Status (5)

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AU (1) AU2001243405A1 (en)
CA (1) CA2401723C (en)
GB (1) GB2376968B (en)
NZ (1) NZ521121A (en)
WO (1) WO2001065066A1 (en)

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Publication number Publication date
GB0220347D0 (en) 2002-10-09
GB2376968A (en) 2002-12-31
WO2001065066A1 (en) 2001-09-07
CA2401723C (en) 2009-06-09
CA2401723A1 (en) 2001-09-07
GB2376968B (en) 2004-03-03
AU2001243405A1 (en) 2001-09-12

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