MY133690A - A method for preparing mixed amorphous vanadium oxides and their use as electrodes in rechargeable lithium cells - Google Patents
A method for preparing mixed amorphous vanadium oxides and their use as electrodes in rechargeable lithium cellsInfo
- Publication number
- MY133690A MY133690A MYPI97003089A MYPI9703089A MY133690A MY 133690 A MY133690 A MY 133690A MY PI97003089 A MYPI97003089 A MY PI97003089A MY PI9703089 A MYPI9703089 A MY PI9703089A MY 133690 A MY133690 A MY 133690A
- Authority
- MY
- Malaysia
- Prior art keywords
- formula
- metal oxide
- amorphous
- vanadium metal
- lithiated
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 4
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 title 1
- XHCLAFWTIXFWPH-UHFFFAOYSA-N [O-2].[O-2].[O-2].[O-2].[O-2].[V+5].[V+5] Chemical class [O-2].[O-2].[O-2].[O-2].[O-2].[V+5].[V+5] XHCLAFWTIXFWPH-UHFFFAOYSA-N 0.000 title 1
- 229910052744 lithium Inorganic materials 0.000 title 1
- 229910001935 vanadium oxide Inorganic materials 0.000 title 1
- -1 VANADIUM METAL OXIDE Chemical class 0.000 abstract 6
- 229910044991 metal oxide Inorganic materials 0.000 abstract 6
- 229910052720 vanadium Inorganic materials 0.000 abstract 6
- 229910003206 NH4VO3 Inorganic materials 0.000 abstract 2
- 229910002651 NO3 Inorganic materials 0.000 abstract 2
- 239000007864 aqueous solution Substances 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 2
- ALTWGIIQPLQAAM-UHFFFAOYSA-N metavanadate Chemical class [O-][V](=O)=O ALTWGIIQPLQAAM-UHFFFAOYSA-N 0.000 abstract 2
- 150000002823 nitrates Chemical class 0.000 abstract 2
- 230000001376 precipitating effect Effects 0.000 abstract 2
- 239000000243 solution Substances 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 1
- 239000011149 active material Substances 0.000 abstract 1
- 238000004090 dissolution Methods 0.000 abstract 1
- 239000003792 electrolyte Substances 0.000 abstract 1
- 238000009830 intercalation Methods 0.000 abstract 1
- 230000002687 intercalation Effects 0.000 abstract 1
- 229910003002 lithium salt Inorganic materials 0.000 abstract 1
- 159000000002 lithium salts Chemical class 0.000 abstract 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/485—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G31/00—Compounds of vanadium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G51/00—Compounds of cobalt
- C01G51/80—Compounds containing cobalt, with or without oxygen or hydrogen, and containing one or more other elements
- C01G51/82—Compounds containing cobalt, with or without oxygen or hydrogen, and containing two or more other elements
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G53/00—Compounds of nickel
- C01G53/80—Compounds containing nickel, with or without oxygen or hydrogen, and containing one or more other elements
- C01G53/82—Compounds containing nickel, with or without oxygen or hydrogen, and containing two or more other elements
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/02—Amorphous compounds
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/40—Electric properties
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Battery Electrode And Active Subsutance (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Secondary Cells (AREA)
Abstract
A METHOD FOR PREPARING AN AMORPHOUS TERNARY LITHIATED VANADIUM METAL OXIDE OF THE FORMULA LIXMYVZO(X+5Z-NY)/2, WHERE M IS A METAL, 0 < X < 3, 0 < Y < 3, 1 < Z < 4, AND N = 2 OR 3, COMPRISING THE STEPS OF CREATING AN AQUEOUS SOLUTION OF AT LEAST ONE METAVANADATE SALT SELECTED FROM THE GROUP CONSISTING OF NH4VO3 AND NAVO3, AND A NITRATE SALT OF THE FORMULA M(NO3')N CONTAINING A LARGE EXCESS OF A LITHIUM SALT; HEATING THE SOLUTION; ADDING A SUFFICIENT AMOUNT OF A BASE TO OBTAIN A SUITABLE PH; AND PRECIPITATING THE AMORPHOUS LITHIATED VANADIUM METAL OXIDE. A METHOD FOR PREPARING AN AMORPHOUS BINARY NON-LITHIATED VANADIUM METAL OXIDE OF THE FORMULA MYVZO(5Z+NY)/2, WHERE M IS A METAL, 0 < Y < 3, 1 < Z < 4, AND N = 2 OR 3, COMRPISING THE STEPS OF CREATING AN AQUEOUS SOLUTION OF AT LEAST ONE METAVANADATE SALT SELECTED FROM THE GROUP CONSISTING OF NH4VO3 AND NAVO3, AND A NITRATE SALT OF THE FORMULA M(NO3)N; HEATING THE SOLUTION; ADDING A SUFFICIENT AMOUNT OF AN ACID FOR DISSOLUTION; AND ADDING A SUFFICIENT AMOUNT OF A BASE TO OBTAIN A SUITABLE PH FOR PRECIPITATING THE AMORPHOUS BINARY NON-LITHIATED VANADIUM METAL OXIDE. A RECHARGEABLE LITHIATED INTERCALATION BATTERY CELL COMPRISING A POSITIVE ELECTRODE, A NEGATIVE ELECTRODE, AND AN ELECTROLYTE, WHEREIN THE ACTIVE MATERIAL OF THE NEGATIVE ELECTRODE IS AN AMORPHOUS TERNARY LITHIATED VANADIUM METAL OXIDE OF THE FORMULA LIXMYVZO(X+5Z+NY)/2 OR AN AMORPHOUS BINARY NON-LITHIATED VANADIUM METAL OXIDE OF THE FORMULA MYVZO(5Z+NY)/2, PREPARED ACCORDING TO THE METHODS OF THE PRESENT INVENTION.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/678,210 US5700598A (en) | 1996-07-11 | 1996-07-11 | Method for preparing mixed amorphous vanadium oxides and their use as electrodes in reachargeable lithium cells |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MY133690A true MY133690A (en) | 2007-11-30 |
Family
ID=24721854
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MYPI97003089A MY133690A (en) | 1996-07-11 | 1997-07-08 | A method for preparing mixed amorphous vanadium oxides and their use as electrodes in rechargeable lithium cells |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US5700598A (en) |
| EP (1) | EP0913007A1 (en) |
| JP (2) | JP2000503622A (en) |
| AU (1) | AU715258B2 (en) |
| CA (1) | CA2259590C (en) |
| ID (1) | ID17594A (en) |
| IL (1) | IL127707A (en) |
| MY (1) | MY133690A (en) |
| TW (1) | TW362296B (en) |
| WO (1) | WO1998002929A1 (en) |
Families Citing this family (39)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6277521B1 (en) | 1997-05-15 | 2001-08-21 | Fmc Corporation | Lithium metal oxide containing multiple dopants and method of preparing same |
| ZA983867B (en) * | 1997-05-16 | 1998-11-13 | Henkel Corp | Lithium and vanadium containing sealing composition and process therewith |
| DE69827700T2 (en) * | 1997-05-22 | 2005-10-06 | Matsushita Electric Industrial Co., Ltd., Kadoma | Secondary battery with non-aqueous electrolyte |
| US6017654A (en) * | 1997-08-04 | 2000-01-25 | Carnegie Mellon University | Cathode materials for lithium-ion secondary cells |
| US6517974B1 (en) * | 1998-01-30 | 2003-02-11 | Canon Kabushiki Kaisha | Lithium secondary battery and method of manufacturing the lithium secondary battery |
| US5980855A (en) * | 1998-05-26 | 1999-11-09 | Rentech, Inc. | Method for preparing lithiated metal oxides |
| US5939043A (en) * | 1998-06-26 | 1999-08-17 | Ga-Tek Inc. | Process for preparing Lix Mn2 O4 intercalation compounds |
| US6267943B1 (en) | 1998-10-15 | 2001-07-31 | Fmc Corporation | Lithium manganese oxide spinel compound and method of preparing same |
| DK1137598T3 (en) | 1998-11-13 | 2003-08-18 | Fmc Corp | Layered lithium metal oxides free of local cubic spinel-like structural phases and processes for making the same |
| EP1135334B1 (en) | 1998-11-20 | 2002-10-09 | Fmc Corporation | Multiple doped lithium manganese oxide compounds and methods of preparing same |
| US6322928B1 (en) * | 1999-09-23 | 2001-11-27 | 3M Innovative Properties Company | Modified lithium vanadium oxide electrode materials and products |
| AU1951601A (en) | 1999-12-10 | 2001-06-18 | Fmc Corporation | Lithium cobalt oxides and methods of making same |
| EP1251575A1 (en) * | 2000-04-19 | 2002-10-23 | Japan Storage Battery Co., Ltd. | Positive electrode active material for secondary cell, method for producing the same and nonaqueous electrolyte secondary cell comprising the same |
| EP1164649A1 (en) * | 2000-06-13 | 2001-12-19 | Japan Storage Battery Company Limited | Positive active material for secondary battery, process for preparation thereof and non-aqueous secondary battery comprising same |
| DE10296692T5 (en) * | 2002-03-28 | 2004-04-29 | Council Of Scientific And Industrial Research | Combustion process for the production of LiCoVO4 |
| US20030235761A1 (en) * | 2002-04-26 | 2003-12-25 | Prabaharan S.R. Sahaya | Rechargeable lithium-containing battery employing brannerite type LiVMoO5.5 cathode and method of preparing same |
| US20040048157A1 (en) * | 2002-09-11 | 2004-03-11 | Neudecker Bernd J. | Lithium vanadium oxide thin-film battery |
| US8026003B2 (en) * | 2003-08-21 | 2011-09-27 | Samsung Sdi Co., Ltd. | Negative active material for a non-aqueous electrolyte battery, and a non-aqueous electrolyte battery comprising the same |
| US7682746B2 (en) * | 2005-03-31 | 2010-03-23 | Panasonic Corporation | Negative electrode for non-aqueous secondary battery |
| US7399457B2 (en) * | 2005-04-12 | 2008-07-15 | Conocophillips Company | Process for the removal of heavy metals from gases, and compositions therefor and therewith |
| KR100759410B1 (en) * | 2006-11-20 | 2007-09-19 | 삼성에스디아이 주식회사 | Anode active material for lithium secondary battery, manufacturing method thereof and lithium secondary battery comprising same |
| KR100778450B1 (en) * | 2006-11-22 | 2007-11-28 | 삼성에스디아이 주식회사 | Anode active material for lithium secondary battery, preparation method thereof and lithium secondary battery comprising same |
| KR100814880B1 (en) * | 2006-11-22 | 2008-03-18 | 삼성에스디아이 주식회사 | Anode active material for lithium secondary battery, preparation method thereof and lithium secondary battery comprising same |
| JP5270089B2 (en) * | 2006-12-18 | 2013-08-21 | 三星エスディアイ株式会社 | Method for producing negative electrode material for non-aqueous secondary battery and method for producing non-aqueous secondary battery using the same |
| EP1935850A3 (en) * | 2006-12-18 | 2008-07-02 | Samsung SDI Co., Ltd. | Composition for negative electrodes and non-aqueous rechargeable battery prepared using Same |
| KR100805123B1 (en) * | 2007-02-15 | 2008-02-21 | 삼성에스디아이 주식회사 | Lithium secondary battery |
| KR100953615B1 (en) * | 2007-04-13 | 2010-04-20 | 삼성에스디아이 주식회사 | Anode active material for lithium secondary battery, manufacturing method thereof and lithium secondary battery comprising same |
| JP5511128B2 (en) * | 2007-06-07 | 2014-06-04 | 三星エスディアイ株式会社 | Anode material for non-aqueous secondary battery and non-aqueous secondary battery |
| KR100918048B1 (en) | 2007-09-07 | 2009-09-22 | 삼성에스디아이 주식회사 | Lithium secondary battery |
| KR100898291B1 (en) * | 2007-09-12 | 2009-05-18 | 삼성에스디아이 주식회사 | Lithium secondary battery |
| TW201002623A (en) * | 2008-05-30 | 2010-01-16 | Basf Se | Process for preparing lithium vanadium oxides and their use as cathode material |
| KR101208910B1 (en) | 2010-09-29 | 2012-12-06 | 전자부품연구원 | Manufacturing method of negative composition for Lithium secondary battery using lithium vanadium oxide substituted other metal |
| RU2453014C1 (en) * | 2010-11-23 | 2012-06-10 | Государственное образовательное учреждение высшего профессионального образования Самарский государственный технический университет | Electrolyte for chemical current source |
| KR101418060B1 (en) * | 2012-02-20 | 2014-07-10 | 경북대학교 산학협력단 | Preparation method of a positive active for a lithium secondary battery |
| US10297855B2 (en) | 2012-05-29 | 2019-05-21 | Nutech Ventures | Rechargeable multi-cell battery |
| CN103268964B (en) * | 2013-05-09 | 2015-08-05 | 西安交通大学 | A kind of method of sodium vanadate assembling aqueous solution lithium ion battery |
| ES2974780T3 (en) * | 2020-02-26 | 2024-07-01 | Lg Energy Solution Ltd | Irreversible additive, positive electrode including the irreversible additive, and secondary lithium battery including the positive electrode |
| JP2024055325A (en) * | 2022-10-07 | 2024-04-18 | 日本ケミコン株式会社 | Method for producing lithium vanadium oxide crystal, lithium vanadium oxide crystal, electrode material and power storage device |
| KR102907969B1 (en) * | 2023-11-28 | 2026-01-02 | 경북대학교 산학협력단 | Vanadium oxide-based negative electrode active material and method for manufacturing the same |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4675260A (en) * | 1984-11-12 | 1987-06-23 | Nippon Telegraph And Telephone Corporation | Lithium battery including vanadium pentoxide base amorphous cathode active material |
| IT1231750B (en) * | 1989-05-12 | 1991-12-21 | Consiglio Nazionale Ricerche | HIGH ENERGY AND POWER LITHIUM ACCUMULATORS AND RELATED PRODUCTION METHOD |
| US5284721A (en) * | 1990-08-01 | 1994-02-08 | Alliant Techsystems Inc. | High energy electrochemical cell employing solid-state anode |
| FR2685129B1 (en) * | 1991-12-13 | 1994-03-25 | Centre Nal Etudes Spatiales | USE OF VANADIUM OXIDE BRONZES WITH IRON AND / OR ALUMINUM AS CATHODE MATERIAL IN ELECTROCHEMICAL GENERATORS. |
| US5334334A (en) * | 1993-03-30 | 1994-08-02 | Valence Technology, Inc. | Method of preparing lithium battery electrode compositions |
| JPH07122275A (en) * | 1993-05-25 | 1995-05-12 | Wilson Greatbatch Ltd | Cathode for electrochemical cell, method for its preparation and electrochemical cell |
-
1996
- 1996-07-11 US US08/678,210 patent/US5700598A/en not_active Expired - Lifetime
-
1997
- 1997-06-27 WO PCT/US1997/011285 patent/WO1998002929A1/en not_active Ceased
- 1997-06-27 IL IL12770797A patent/IL127707A/en not_active IP Right Cessation
- 1997-06-27 AU AU36443/97A patent/AU715258B2/en not_active Ceased
- 1997-06-27 CA CA002259590A patent/CA2259590C/en not_active Expired - Fee Related
- 1997-06-27 JP JP10506049A patent/JP2000503622A/en active Pending
- 1997-06-27 EP EP97933196A patent/EP0913007A1/en not_active Withdrawn
- 1997-07-08 MY MYPI97003089A patent/MY133690A/en unknown
- 1997-07-10 ID IDP972381A patent/ID17594A/en unknown
- 1997-07-11 TW TW086109800A patent/TW362296B/en active
-
2002
- 2002-08-22 JP JP2002242077A patent/JP2003142096A/en active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| US5700598A (en) | 1997-12-23 |
| CA2259590C (en) | 2005-10-25 |
| EP0913007A1 (en) | 1999-05-06 |
| WO1998002929A1 (en) | 1998-01-22 |
| JP2000503622A (en) | 2000-03-28 |
| AU715258B2 (en) | 2000-01-20 |
| IL127707A (en) | 2002-05-23 |
| CA2259590A1 (en) | 1998-01-22 |
| AU3644397A (en) | 1998-02-09 |
| TW362296B (en) | 1999-06-21 |
| ID17594A (en) | 1998-01-15 |
| JP2003142096A (en) | 2003-05-16 |
| IL127707A0 (en) | 1999-10-28 |
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