MX2016000621A - Proceso mejorado para preparar bifenilanilidas y bifenilanilinas cloradas. - Google Patents

Proceso mejorado para preparar bifenilanilidas y bifenilanilinas cloradas.

Info

Publication number
MX2016000621A
MX2016000621A MX2016000621A MX2016000621A MX2016000621A MX 2016000621 A MX2016000621 A MX 2016000621A MX 2016000621 A MX2016000621 A MX 2016000621A MX 2016000621 A MX2016000621 A MX 2016000621A MX 2016000621 A MX2016000621 A MX 2016000621A
Authority
MX
Mexico
Prior art keywords
formula
biphenylanilines
improved process
biphenylanilides
preparing chlorinated
Prior art date
Application number
MX2016000621A
Other languages
English (en)
Inventor
Lars Rodefeld
Michael Dockner
Jens Dietmar Heinrich
Original Assignee
Bayer Cropscience Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer Cropscience Ag filed Critical Bayer Cropscience Ag
Publication of MX2016000621A publication Critical patent/MX2016000621A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B37/00—Reactions without formation or introduction of functional groups containing hetero atoms, involving either the formation of a carbon-to-carbon bond between two carbon atoms not directly linked already or the disconnection of two directly linked carbon atoms
    • C07B37/04—Substitution
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/68—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/12—Preparation of carboxylic acid amides by reactions not involving the formation of carboxamide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C07C233/64—Carboxylic acid amides having carbon atoms of carboxamide groups bound to carbon atoms of six-membered aromatic rings
    • C07C233/66—Carboxylic acid amides having carbon atoms of carboxamide groups bound to carbon atoms of six-membered aromatic rings having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by halogen atoms or by nitro or nitroso groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/50—Organo-phosphines
    • C07F9/5004—Acyclic saturated phosphines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/50—Organo-phosphines
    • C07F9/5022—Aromatic phosphines (P-C aromatic linkage)
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/54—Quaternary phosphonium compounds
    • C07F9/5407—Acyclic saturated phosphonium compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/54—Quaternary phosphonium compounds
    • C07F9/5442—Aromatic phosphonium compounds (P-C aromatic linkage)

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Biochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Catalysts (AREA)

Abstract

La presente invención se relaciona con un proceso para preparar bifenilanilidas sustituidas de la fórmula (I) (Ver Fórmula) en la que R1 se selecciona de un grupo amino protegido, NO2, NH2 y NHR3, en la que un compuesto de la fórmula II (ver Fórmula) se hace reaccionar en presencia de una base y de una sal de paladio, en presencia de un ligando de fosfina de la fórmula (V) como ligando complejo (ver Fórmula) o una sal del mismo, en un solvente, con un compuesto organoboro de la fórmula (III) (ver Fórmula) en la que todos los sustituyentes son como se define en la descripción.
MX2016000621A 2013-07-23 2014-07-18 Proceso mejorado para preparar bifenilanilidas y bifenilanilinas cloradas. MX2016000621A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP13177583 2013-07-23
PCT/EP2014/065463 WO2015011032A1 (de) 2013-07-23 2014-07-18 Verbessertes verfahren zur herstellung von chlorierten biphenylaniliden und biphenylanilinen

Publications (1)

Publication Number Publication Date
MX2016000621A true MX2016000621A (es) 2016-05-26

Family

ID=48808249

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2016000621A MX2016000621A (es) 2013-07-23 2014-07-18 Proceso mejorado para preparar bifenilanilidas y bifenilanilinas cloradas.

Country Status (12)

Country Link
US (2) US9868694B2 (es)
EP (2) EP3418284A1 (es)
JP (2) JP6518242B2 (es)
KR (1) KR102310474B1 (es)
CN (1) CN105392791B (es)
BR (1) BR112016000968B1 (es)
DK (1) DK3024836T3 (es)
ES (1) ES2687950T3 (es)
IL (1) IL243680B (es)
MX (1) MX2016000621A (es)
TW (1) TWI658031B (es)
WO (1) WO2015011032A1 (es)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3500551B1 (en) * 2016-08-22 2021-11-10 Basf Se Process for preparing substituted biphenyls
ES2880323T3 (es) * 2017-02-14 2021-11-24 Basf Se Proceso para la preparación de bifenilos sustituidos
FR3064496A1 (fr) 2017-03-31 2018-10-05 Centre National De La Recherche Scientifique Utilisation de materiaux naturels d'origine vegetale riches en acides phenoliques pour la mise en oeuvre de reaction de chimie organique et le recyclage de catalyseurs
CN107556199A (zh) * 2017-09-24 2018-01-09 杨子辉 一种3,4‑二氯‑2‑氨基‑5‑氟联苯的制备方法
DE102018122708A1 (de) * 2018-09-17 2020-03-19 Novaled Gmbh Organische elektronische Vorrichtung, organisches halbleitendes Material und eine Boranverbindung
CA3118079A1 (en) 2018-10-29 2020-05-07 Stuart Licht Sustainable, facile separation of the molten carbonate electrolysis cathode product
EP3999488A1 (en) 2019-07-19 2022-05-25 Adama Makhteshim Ltd. Process for the preparation of biphenylamines
US20220042193A1 (en) 2020-08-06 2022-02-10 C2Cnt Llc Sustainable, facile separation of the molten carbonate electrolysis cathode product
WO2022243099A1 (en) 2021-05-19 2022-11-24 Basf Se Process for preparing substituted biphenyls via suzuki coupling of aryl-chlorides

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1163452C (zh) 1996-03-13 2004-08-25 巴斯福股份公司 硝基联苯的制备方法
CA2281525A1 (en) * 1997-02-18 1998-08-20 Neurocrine Biosciences, Inc. Biazacyclic crf antagonists
US6307087B1 (en) * 1998-07-10 2001-10-23 Massachusetts Institute Of Technology Ligands for metals and improved metal-catalyzed processes based thereon
FR2801884A1 (fr) 1999-12-06 2001-06-08 Rhodia Chimie Sa Procede de preparation d'un compose polyaromatique
CN1628122B (zh) * 2002-02-04 2010-06-09 北兴化学工业株式会社 制备具有大体积烃基团的叔膦的方法
DE10215292A1 (de) 2002-02-19 2003-08-28 Bayer Cropscience Ag Disubstitutierte Pyrazolylcarbocanilide
DE10252273A1 (de) * 2002-11-11 2004-05-27 Bayer Ag Polyhalogenalkylaryle
CN100548948C (zh) * 2002-12-09 2009-10-14 麻省理工学院 金属配体以及以此为基础的改良的金属催化方法
DK1581467T3 (en) 2002-12-09 2016-11-28 Massachusetts Inst Technology LIGANDS FOR METALS AND IMPROVED METAL CATALYZED PROCEDURES BASED ON THERE
EP1688424B1 (en) * 2003-11-28 2016-01-13 Hokko Chemical Industry Co., Ltd. Phosphonium borate compound and method of using the same
AR052930A1 (es) 2005-03-02 2007-04-11 Basf Ag Procedimiento para la preparacion de bifenilos sustituidos
DE102005022362B4 (de) * 2005-05-10 2016-12-15 Studiengesellschaft Kohle Mbh Verfahren zur decarboxylierenden C-C Verknüpfung von Carbonsäuren mit Kohlenstoffelektrophilen
WO2007138089A1 (en) 2006-06-01 2007-12-06 Basf Se Process for preparing substituted biphenyls
CN101374799B (zh) * 2006-06-01 2012-05-23 巴斯夫欧洲公司 制备取代联苯的方法
EP2008991A1 (de) 2007-06-29 2008-12-31 Bayer CropScience AG Verfahren zur Herstellung von Biarylen
EP2119697A1 (en) * 2008-05-09 2009-11-18 Bayer CropScience AG Process for preparing substituted biphenylanilides
KR101751249B1 (ko) * 2009-08-31 2017-06-27 바이엘 인텔렉쳐 프로퍼티 게엠베하 테트라아릴보레이트를 사용한 치환된 비페닐의 제조 방법
EP2563759B1 (en) * 2010-04-27 2022-04-06 Calcimedica, Inc. Compounds that modulate intracellular calcium

Also Published As

Publication number Publication date
KR102310474B1 (ko) 2021-10-07
CN105392791A (zh) 2016-03-09
JP6518242B2 (ja) 2019-05-22
US20160280635A1 (en) 2016-09-29
BR112016000968B1 (pt) 2021-05-18
ES2687950T3 (es) 2018-10-30
IL243680B (en) 2020-06-30
EP3418284A1 (de) 2018-12-26
TWI658031B (zh) 2019-05-01
US20180093942A1 (en) 2018-04-05
TW201546031A (zh) 2015-12-16
IL243680A0 (en) 2016-04-21
JP2019108352A (ja) 2019-07-04
US9868694B2 (en) 2018-01-16
EP3024836A1 (de) 2016-06-01
BR112016000968A2 (pt) 2017-08-29
CN105392791B (zh) 2019-02-22
JP2016525526A (ja) 2016-08-25
KR20160033702A (ko) 2016-03-28
WO2015011032A1 (de) 2015-01-29
EP3024836B1 (de) 2018-07-11
DK3024836T3 (en) 2018-10-08

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