KR850004704A - 탈유 대두박으로 부터 유용한 생성물의 회수방법. - Google Patents
탈유 대두박으로 부터 유용한 생성물의 회수방법. Download PDFInfo
- Publication number
- KR850004704A KR850004704A KR1019840004399A KR840004399A KR850004704A KR 850004704 A KR850004704 A KR 850004704A KR 1019840004399 A KR1019840004399 A KR 1019840004399A KR 840004399 A KR840004399 A KR 840004399A KR 850004704 A KR850004704 A KR 850004704A
- Authority
- KR
- South Korea
- Prior art keywords
- product
- free
- residue
- coal
- liquid
- Prior art date
Links
- 235000019764 Soybean Meal Nutrition 0.000 title claims 2
- 239000004455 soybean meal Substances 0.000 title claims 2
- 238000011084 recovery Methods 0.000 title 1
- 238000000034 method Methods 0.000 claims description 10
- 239000000047 product Substances 0.000 claims 13
- 239000007788 liquid Substances 0.000 claims 8
- 239000003245 coal Substances 0.000 claims 5
- 150000001413 amino acids Chemical class 0.000 claims 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 4
- FGUUSXIOTUKUDN-IBGZPJMESA-N C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 Chemical compound C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 FGUUSXIOTUKUDN-IBGZPJMESA-N 0.000 claims 3
- 239000000203 mixture Substances 0.000 claims 3
- 102000004169 proteins and genes Human genes 0.000 claims 3
- 108090000623 proteins and genes Proteins 0.000 claims 3
- 239000011347 resin Substances 0.000 claims 3
- 229920005989 resin Polymers 0.000 claims 3
- 239000007790 solid phase Substances 0.000 claims 3
- GNFTZDOKVXKIBK-UHFFFAOYSA-N 3-(2-methoxyethoxy)benzohydrazide Chemical compound COCCOC1=CC=CC(C(=O)NN)=C1 GNFTZDOKVXKIBK-UHFFFAOYSA-N 0.000 claims 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims 2
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 claims 2
- 239000004472 Lysine Substances 0.000 claims 2
- 239000002253 acid Substances 0.000 claims 2
- 239000003463 adsorbent Substances 0.000 claims 2
- 238000009835 boiling Methods 0.000 claims 2
- 238000001035 drying Methods 0.000 claims 2
- 238000010438 heat treatment Methods 0.000 claims 2
- 238000000108 ultra-filtration Methods 0.000 claims 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims 1
- 239000004475 Arginine Substances 0.000 claims 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims 1
- COLNVLDHVKWLRT-QMMMGPOBSA-N L-phenylalanine Chemical compound OC(=O)[C@@H](N)CC1=CC=CC=C1 COLNVLDHVKWLRT-QMMMGPOBSA-N 0.000 claims 1
- OUYCCCASQSFEME-QMMMGPOBSA-N L-tyrosine Chemical compound OC(=O)[C@@H](N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-QMMMGPOBSA-N 0.000 claims 1
- 238000005903 acid hydrolysis reaction Methods 0.000 claims 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims 1
- ODKSFYDXXFIFQN-UHFFFAOYSA-N arginine Natural products OC(=O)C(N)CCCNC(N)=N ODKSFYDXXFIFQN-UHFFFAOYSA-N 0.000 claims 1
- 150000001720 carbohydrates Chemical class 0.000 claims 1
- 235000014633 carbohydrates Nutrition 0.000 claims 1
- 125000002091 cationic group Chemical group 0.000 claims 1
- 229920002678 cellulose Polymers 0.000 claims 1
- 239000001913 cellulose Substances 0.000 claims 1
- 238000001816 cooling Methods 0.000 claims 1
- 239000008367 deionised water Substances 0.000 claims 1
- 229910021641 deionized water Inorganic materials 0.000 claims 1
- 239000000706 filtrate Substances 0.000 claims 1
- 238000004108 freeze drying Methods 0.000 claims 1
- 229910001385 heavy metal Inorganic materials 0.000 claims 1
- HNDVDQJCIGZPNO-UHFFFAOYSA-N histidine Natural products OC(=O)C(N)CC1=CN=CN1 HNDVDQJCIGZPNO-UHFFFAOYSA-N 0.000 claims 1
- 229910052742 iron Inorganic materials 0.000 claims 1
- 150000002632 lipids Chemical class 0.000 claims 1
- 239000012071 phase Substances 0.000 claims 1
- COLNVLDHVKWLRT-UHFFFAOYSA-N phenylalanine Natural products OC(=O)C(N)CC1=CC=CC=C1 COLNVLDHVKWLRT-UHFFFAOYSA-N 0.000 claims 1
- OUYCCCASQSFEME-UHFFFAOYSA-N tyrosine Natural products OC(=O)C(N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-UHFFFAOYSA-N 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
- 238000010586 diagram Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
- A23J1/14—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from leguminous or other vegetable seeds; from press-cake or oil-bearing seeds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J3/00—Working-up of proteins for foodstuffs
- A23J3/30—Working-up of proteins for foodstuffs by hydrolysis
- A23J3/32—Working-up of proteins for foodstuffs by hydrolysis using chemical agents
- A23J3/34—Working-up of proteins for foodstuffs by hydrolysis using chemical agents using enzymes
- A23J3/346—Working-up of proteins for foodstuffs by hydrolysis using chemical agents using enzymes of vegetable proteins
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Peptides Or Proteins (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제1도는 본 발명에 따른 방법에 있어 바람직한 단계들의 개략도이고,
제2도는 본 발명에 따른 이용을 위해 바람직한 장치의 개략도이다.
Claims (22)
- a)60-95℃의 온도 범위에서 수성액체로 탈유 대두박 잔사를 추출하고; b) 상기 잔사로부터; a)단계로 부터의 액체추출물을 분리하고; c)상기 b)단계로 부터의 상기 잔사를 수성의 산성 가수분해 조건으로 주입하고; d) 상기 잔사로부터 상기 c)단계의 혼합물로부터 액체층을 분리하고; e) 상기 액체층을 양이온성 술폰화 수지로 접촉시키고; f) 상기 수지로 부터의 아미노산을 수성염기로 용출하고; g)상기 f)단계의 용출물을 한외 여과에 주입하고; h) 상기 g)단계의 여액을 탄소성 흡착제 상에서 정제하고; i) 상기 탄소성 흡착제로부터 액체를 함유하는 아미노산을 분리시키는 단계로 구성됨을 특징으로 하는 탈유 대두박으로부터 유용한 생성물을 회수하는 방법.
- 상기 1항에 있어, c')상기 b)단계로부터 상기 액체 추출물을 비등시키고; d')상기 c) 단계의 생성물을 냉각시켜 액체 및 고체상을 형성시키고; e')상기 d')단계에 있어 상기 상들을 분리시키고; f') 상기 e')단계로부터 액체층을 냉동 건조시키는 단계로 구성된 상기의 방법.
- 상기 1항에 있어, e″) 상기 d)단계로부터 상기 잔사를 세척하고; f″) 상기 e″) 단계로부터 상기 잔사를 건조시키는 단계로 구성된 상기의 방법.
- 상기 2항에 있어, e')단계 이후의 고체상을 수집하고 건조시키는 단계로 구성된 상기의 방법.
- 상기 1항에 있어, 상기 c)단계는 150℃까지의 온도에서 수성염산으로 상기 잔사를 접촉시키는 것을 특징으로 하는 상기의 방법.
- 상기 5항에 있어, 상기 산의 농도는 5-25%범위내인 상기의 방법.
- 상기 6항에 있어, 상기 온도는 110℃이고 상기 산농도는 15%인 상기의 방법.
- 상기 1항에 있어, 상기 f)단계는 2% 수성암모니아 및 물로 상기 수지를 연속적으로 용출시킴을 특징으로 하는 상기의 방법.
- 상기 1항에 있어, 상기 g)단계는 1000MW 절단한외 여과기로 상기 용출액을 접촉시키는 것을 특징으로 하는 상기의 방법.
- 상기 1항에 있어, i)단계에 따라 얻어진 생성물.
- 상기 10항에 있어, 13.9% 유리로이신, 0.42% 유리티로신, 2.7% 유리페닐아란닌, 10.4% 유리라이신, 3.02% 유리히스티딘, 0.66% 유리알기닌, 0.15% 유리드립토판으로 구성된 생성물.
- 상기 2항에 있어, f')단계에 따른 생성물.
- 상기 12항에 있어, 17-22% 단백질매, 30-35% 탄수화물, 12-15%회분(무기물)으로 구성된 생성물.
- 상기 13항에 따라 얻어진 생성물.
- 상기 14항에 있어, 14-15% 단백질 및 15%회분(무기물)로 구성되어 얻어진 생성물.
- 상기 4항에 따라 얻어진 생성물.
- 상기 16항에 있어, 3-4% 단백질, 6-8% 회분(무기물), 70% 셀룰로스로 구성되어 얻어진 생성물.
- 상기 9항에 따라 얻어진 생성모류물.
- 상기 10항에 있어, 중량으로, 지질 0.11%, 전체환원당 0.12%, 전체아미노산 95.1%(91.3% 유리아미노산), 회분 0.7%, 염화물200ppm 이하, 중금속 20ppm이하, 철 200ppm 이하, 물 대략 4%로 구성된 생성물.
- 상기 11항에 있어 무게로으로 구성된 생성물
- 무게로
- a)석탄의 중량으로 약2배의 물의 양으로, 석탄을 탈이온수와 혼합하고; b)상기 a)단계의 혼합물을 비등시키고; c)상기 b)단계의 혼합물로부터 석탄을 냉각 분리시키고; d) 약 2시간동안 약 2000℃로 상기 c)단계로부터의 석탄을 가열하고; e)약 4시간동안 약 1000℃로 상기 d)단계로부터의 석탄을 가열시키는 단계로 구성됨을 특징으로 하는 석탄으로부터 활성탄을 제조하는 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US51628583A | 1983-07-22 | 1983-07-22 | |
| US516285 | 1983-07-22 | ||
| US58783884A | 1984-03-12 | 1984-03-12 | |
| US587838 | 1984-03-12 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| KR850004704A true KR850004704A (ko) | 1985-07-27 |
Family
ID=27058781
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019840004399A KR850004704A (ko) | 1983-07-22 | 1984-07-24 | 탈유 대두박으로 부터 유용한 생성물의 회수방법. |
Country Status (9)
| Country | Link |
|---|---|
| KR (1) | KR850004704A (ko) |
| AU (1) | AU3058084A (ko) |
| FR (1) | FR2549351A1 (ko) |
| GB (1) | GB2143828B (ko) |
| IN (1) | IN162583B (ko) |
| IT (1) | IT8421989A0 (ko) |
| MX (1) | MX7589E (ko) |
| PH (1) | PH21335A (ko) |
| WO (1) | WO1985000502A1 (ko) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61295219A (ja) * | 1985-06-21 | 1986-12-26 | Eiichi Sato | 活性炭 |
Family Cites Families (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3001875A (en) * | 1956-05-28 | 1961-09-26 | Griffith Laboratories | Method of extracting protein from defatted soybean material |
| US2991309A (en) * | 1957-12-30 | 1961-07-04 | Internat Minerals & Chemicals | Protein hydrolysis |
| GB931016A (en) * | 1960-12-22 | 1963-07-10 | Distillers Co Yeast Ltd | Amino acids concentrate and intravenous preparations thereof |
| US3185675A (en) * | 1963-03-28 | 1965-05-25 | Bristol Myers Co | Peptide |
| US3701666A (en) * | 1968-02-14 | 1972-10-31 | Morton Norwich Products Inc | Process for making amino acid composition |
| US3697287A (en) * | 1969-01-28 | 1972-10-10 | Morton Norwich Products Inc | Amino acid food composition |
| US3698912A (en) * | 1969-07-01 | 1972-10-17 | Morton Norwich Products Inc | Process for making nutrient composition |
| IL36482A0 (en) * | 1970-04-04 | 1971-05-26 | Istituto Ricerche Biomediche | The manufacture of natural amino acid mixtures from protein material |
| US3778514A (en) * | 1970-10-09 | 1973-12-11 | Mayer & Co Inc O | Nutritional product of whey protein and collagen hydrolysate |
| US3951856A (en) * | 1972-10-02 | 1976-04-20 | Westvaco Corporation | Process for making activated carbon from agglomerative coal |
| US3876505A (en) * | 1972-12-08 | 1975-04-08 | Calgon Corp | Manufacture of activated carbon from sized coal |
| JPS5545485B2 (ko) * | 1973-01-05 | 1980-11-18 | ||
| IT1018766B (it) * | 1974-07-30 | 1977-10-20 | Orban S | Procedimento per la preparazione di concentrati proteici vegetali prodotti ottenuti e mangimi sostitutivi del latte che li contengono |
| US3950547A (en) * | 1974-08-26 | 1976-04-13 | Syntex (U.S.A.) Inc. | Dietary composition and methods of preparing |
| US4107084A (en) * | 1975-06-09 | 1978-08-15 | Westvaco Corporation | Process for activating carbonaceous material |
| US3976597A (en) * | 1975-06-09 | 1976-08-24 | Westvaco Corporation | Fluidized bed process for making activated carbon including heating by conduction through the distributor plate |
| US3995071A (en) * | 1975-06-23 | 1976-11-30 | Mead Johnson & Company | Aqueous purified soy protein and beverage |
| US4091120A (en) * | 1976-11-15 | 1978-05-23 | Mead Johnson & Company | Liquid dietary product containing soy protein membrane isolate |
| CH620347A5 (ko) * | 1977-03-17 | 1980-11-28 | Maggi Ag | |
| US4130555A (en) * | 1977-09-06 | 1978-12-19 | Nippi Incorporated | Peptide mixtures derived from collagenous material or gelatin |
| US4268417A (en) * | 1977-09-26 | 1981-05-19 | American Minechem Corporation | Method of making activated carbon |
| US4172828A (en) * | 1977-09-30 | 1979-10-30 | Anderson, Clayton & Co. | Method for processing soy protein and composition of matter |
| US4273619A (en) * | 1979-11-19 | 1981-06-16 | Angelo Ii James F | Apparatus for continuously carbonizing and activating carbonaceous materials |
-
1984
- 1984-07-12 IN IN503/CAL/84A patent/IN162583B/en unknown
- 1984-07-13 GB GB08417924A patent/GB2143828B/en not_active Expired
- 1984-07-13 AU AU30580/84A patent/AU3058084A/en not_active Abandoned
- 1984-07-20 WO PCT/US1984/001137 patent/WO1985000502A1/en unknown
- 1984-07-20 IT IT8421989A patent/IT8421989A0/it unknown
- 1984-07-20 FR FR8411548A patent/FR2549351A1/fr not_active Withdrawn
- 1984-07-20 PH PH31016A patent/PH21335A/en unknown
- 1984-07-20 MX MX84101974U patent/MX7589E/es unknown
- 1984-07-24 KR KR1019840004399A patent/KR850004704A/ko not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| MX7589E (es) | 1989-12-20 |
| GB8417924D0 (en) | 1984-08-15 |
| IN162583B (ko) | 1988-06-11 |
| IT8421989A0 (it) | 1984-07-20 |
| GB2143828B (en) | 1987-05-13 |
| GB2143828A (en) | 1985-02-20 |
| AU3058084A (en) | 1985-01-24 |
| FR2549351A1 (fr) | 1985-01-25 |
| WO1985000502A1 (en) | 1985-02-14 |
| PH21335A (en) | 1987-10-13 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A201 | Request for examination | ||
| E902 | Notification of reason for refusal | ||
| E601 | Decision to refuse application |