KR20080015406A - 중축합에서 유래한 응축물의 처리방법 - Google Patents
중축합에서 유래한 응축물의 처리방법 Download PDFInfo
- Publication number
- KR20080015406A KR20080015406A KR1020077026506A KR20077026506A KR20080015406A KR 20080015406 A KR20080015406 A KR 20080015406A KR 1020077026506 A KR1020077026506 A KR 1020077026506A KR 20077026506 A KR20077026506 A KR 20077026506A KR 20080015406 A KR20080015406 A KR 20080015406A
- Authority
- KR
- South Korea
- Prior art keywords
- condensate
- condenser
- collection tank
- product
- condensation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000006068 polycondensation reaction Methods 0.000 title claims description 10
- 239000000178 monomer Substances 0.000 claims abstract description 37
- 238000000034 method Methods 0.000 claims abstract description 24
- 238000004519 manufacturing process Methods 0.000 claims abstract description 15
- 150000002989 phenols Chemical class 0.000 claims abstract description 11
- 230000008707 rearrangement Effects 0.000 claims abstract description 8
- VPWNQTHUCYMVMZ-UHFFFAOYSA-N 4,4'-sulfonyldiphenol Chemical class C1=CC(O)=CC=C1S(=O)(=O)C1=CC=C(O)C=C1 VPWNQTHUCYMVMZ-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229930185605 Bisphenol Natural products 0.000 claims abstract description 7
- 150000007522 mineralic acids Chemical class 0.000 claims abstract description 7
- 150000007524 organic acids Chemical class 0.000 claims abstract description 7
- 125000000217 alkyl group Chemical group 0.000 claims abstract description 6
- 238000004821 distillation Methods 0.000 claims abstract description 6
- 150000007860 aryl ester derivatives Chemical class 0.000 claims abstract description 5
- 239000000047 product Substances 0.000 claims description 66
- 238000000354 decomposition reaction Methods 0.000 claims description 27
- 238000009833 condensation Methods 0.000 claims description 13
- 230000005494 condensation Effects 0.000 claims description 13
- 238000005886 esterification reaction Methods 0.000 claims description 11
- 239000002253 acid Substances 0.000 claims description 6
- 230000032050 esterification Effects 0.000 claims description 5
- 229920000642 polymer Polymers 0.000 claims description 5
- 229920001577 copolymer Polymers 0.000 claims description 4
- 239000002699 waste material Substances 0.000 claims description 4
- 150000007513 acids Chemical class 0.000 claims description 3
- 239000007795 chemical reaction product Substances 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 238000002425 crystallisation Methods 0.000 claims description 2
- 230000008025 crystallization Effects 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 2
- 238000005979 thermal decomposition reaction Methods 0.000 claims description 2
- 230000015556 catabolic process Effects 0.000 abstract 1
- 238000006731 degradation reaction Methods 0.000 abstract 1
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 17
- 238000009835 boiling Methods 0.000 description 15
- 238000006243 chemical reaction Methods 0.000 description 14
- -1 polyethylene terephthalate Polymers 0.000 description 10
- 238000003908 quality control method Methods 0.000 description 9
- 239000003054 catalyst Substances 0.000 description 8
- ROORDVPLFPIABK-UHFFFAOYSA-N diphenyl carbonate Chemical compound C=1C=CC=CC=1OC(=O)OC1=CC=CC=C1 ROORDVPLFPIABK-UHFFFAOYSA-N 0.000 description 6
- 229920000515 polycarbonate Polymers 0.000 description 6
- 239000004417 polycarbonate Substances 0.000 description 6
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 5
- 239000007857 degradation product Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 229920001230 polyarylate Polymers 0.000 description 4
- 238000010517 secondary reaction Methods 0.000 description 4
- 239000006227 byproduct Substances 0.000 description 3
- 230000006835 compression Effects 0.000 description 3
- 238000007906 compression Methods 0.000 description 3
- 229920006351 engineering plastic Polymers 0.000 description 3
- 150000002148 esters Chemical class 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- QUUSLJRWTDZCBF-UHFFFAOYSA-N 2,3-dihydroindene-1,1-diol Chemical compound C1=CC=C2C(O)(O)CCC2=C1 QUUSLJRWTDZCBF-UHFFFAOYSA-N 0.000 description 2
- WUQYBSRMWWRFQH-UHFFFAOYSA-N 2-prop-1-en-2-ylphenol Chemical compound CC(=C)C1=CC=CC=C1O WUQYBSRMWWRFQH-UHFFFAOYSA-N 0.000 description 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 238000012696 Interfacial polycondensation Methods 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 238000005194 fractionation Methods 0.000 description 2
- PQNFLJBBNBOBRQ-UHFFFAOYSA-N indane Chemical compound C1=CC=C2CCCC2=C1 PQNFLJBBNBOBRQ-UHFFFAOYSA-N 0.000 description 2
- 238000011068 loading method Methods 0.000 description 2
- 229920000139 polyethylene terephthalate Polymers 0.000 description 2
- 239000005020 polyethylene terephthalate Substances 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- XKZQKPRCPNGNFR-UHFFFAOYSA-N 2-(3-hydroxyphenyl)phenol Chemical compound OC1=CC=CC(C=2C(=CC=CC=2)O)=C1 XKZQKPRCPNGNFR-UHFFFAOYSA-N 0.000 description 1
- 125000004203 4-hydroxyphenyl group Chemical group [H]OC1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 125000005907 alkyl ester group Chemical group 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 238000003776 cleavage reaction Methods 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 230000000593 degrading effect Effects 0.000 description 1
- 150000001991 dicarboxylic acids Chemical class 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 125000005027 hydroxyaryl group Chemical group 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 125000005498 phthalate group Chemical class 0.000 description 1
- 229920001748 polybutylene Polymers 0.000 description 1
- 229920001707 polybutylene terephthalate Polymers 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 230000007017 scission Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- MDCWDBMBZLORER-UHFFFAOYSA-N triphenyl borate Chemical compound C=1C=CC=CC=1OB(OC=1C=CC=CC=1)OC1=CC=CC=C1 MDCWDBMBZLORER-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/20—General preparatory processes
- C08G64/30—General preparatory processes using carbonates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/78—Preparation processes
- C08G63/785—Preparation processes characterised by the apparatus used
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
- B01D3/148—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step in combination with at least one evaporator
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/20—General preparatory processes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
- C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
- C08G63/16—Dicarboxylic acids and dihydroxy compounds
- C08G63/18—Dicarboxylic acids and dihydroxy compounds the acids or hydroxy compounds containing carbocyclic rings
- C08G63/19—Hydroxy compounds containing aromatic rings
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyesters Or Polycarbonates (AREA)
- Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)
- Closing And Opening Devices For Wings, And Checks For Wings (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102005017427.2 | 2005-04-15 | ||
| DE102005017427A DE102005017427A1 (de) | 2005-04-15 | 2005-04-15 | Verfahren zur Aufbereitung von Kondensaten aus der Polykondensation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| KR20080015406A true KR20080015406A (ko) | 2008-02-19 |
Family
ID=36581737
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020077026506A Withdrawn KR20080015406A (ko) | 2005-04-15 | 2006-02-27 | 중축합에서 유래한 응축물의 처리방법 |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US20090114523A1 (https=) |
| EP (1) | EP1869102A1 (https=) |
| JP (1) | JP2008535980A (https=) |
| KR (1) | KR20080015406A (https=) |
| CN (1) | CN101160341A (https=) |
| DE (1) | DE102005017427A1 (https=) |
| WO (1) | WO2006108469A1 (https=) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5110238B2 (ja) * | 2004-05-11 | 2012-12-26 | Jsr株式会社 | 絶縁膜形成用組成物およびその製造方法、ならびにシリカ系絶縁膜およびその形成方法 |
| US7946665B2 (en) * | 2008-11-11 | 2011-05-24 | Dueperthal Sicherheitstechnik GmbH | Safety cabinet with multipanel folding door |
| CN102126958B (zh) * | 2010-12-30 | 2013-12-04 | 江苏淮河化工有限公司 | 精馏与结晶耦合制备高纯度间(对)硝基甲苯的装置及方法 |
| US8727459B2 (en) * | 2011-07-08 | 2014-05-20 | SSI Schäfer Noell GmbH Lager- und Systemtechnik | Multiple-door switchgear cabinet |
| DE102012105296A1 (de) * | 2012-06-19 | 2013-12-19 | Epc Engineering Consulting Gmbh | Verfahren und Anlage zur Herstellung von Polycarbonat |
| DE102013210180A1 (de) * | 2013-05-31 | 2014-12-04 | Aquafil Engineering Gmbh | Verfahren zur Aufarbeitung eines bei Polykondensationsprozessen anfallenden Gemisches und eine Anlage zur Durchführung des Verfahrens |
| CN104109101B (zh) * | 2013-06-06 | 2016-12-28 | 上海志诚化工有限公司 | 一种半导体用超纯电子级化学试剂纯化装置 |
| US9243437B1 (en) * | 2013-10-30 | 2016-01-26 | Austin Hardware And Supply, Inc. | Door sequencer |
| USD797475S1 (en) * | 2016-06-23 | 2017-09-19 | Cosmocube, Inc. | Cabinet |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2820514A (en) | 1955-08-26 | 1958-01-21 | John P Travis | Folding flue window |
| NL288080A (https=) | 1962-01-24 | |||
| DE1495730B2 (de) | 1963-07-24 | 1971-03-18 | Farbenfabriken Bayer AG, 5090 Le verkusen | Verfahren zum herstellen thermoplastischer polykondensations produkte |
| US3516198A (en) * | 1969-01-21 | 1970-06-23 | Robert J Lyons | Emergency release latch mechanism for smoke hatch |
| JPS5036877B2 (https=) | 1972-04-24 | 1975-11-28 | ||
| US3888826A (en) * | 1972-07-10 | 1975-06-10 | Mitsubishi Gas Chemical Co | Process for preparing aromatic polycarbonates |
| GB1474524A (https=) | 1973-07-06 | 1977-05-25 | ||
| US4262448A (en) * | 1979-06-20 | 1981-04-21 | Justrite Manufacturing Company | Safety storage cabinet |
| US4294994A (en) * | 1980-04-21 | 1981-10-13 | General Electric Company | Purification of bisphenol-A |
| US4619076A (en) * | 1985-04-15 | 1986-10-28 | Justrite Manufacturing Company | Safety cabinet latching system |
| US5061022A (en) * | 1990-06-11 | 1991-10-29 | The Louis Berkman Company | Door closing mechanism |
| US5722202A (en) * | 1996-04-26 | 1998-03-03 | Safe-T-Way | Sequential door closing mechanism |
| US5944399A (en) * | 1998-07-06 | 1999-08-31 | Eagle Manufacturing Company | Safety cabinet with self-closing and sequencing door mechanism |
| US5992098A (en) * | 1998-12-09 | 1999-11-30 | Justrite Manufacturing Company, Llc | Safety cabinet latching system |
| EP1018529B1 (en) * | 1999-01-06 | 2004-03-24 | Teijin Limited | Process for producing polycarbonates |
| EP1081174B1 (en) * | 1999-03-03 | 2005-05-11 | Ube Industries, Ltd. | Process for producing polycarbonate |
| DE10059616A1 (de) * | 2000-12-01 | 2002-06-06 | Zimmer Ag | Verfahren zum Erzeugen von Polycarbonaten |
| US6729701B2 (en) * | 2001-06-29 | 2004-05-04 | Justrite Manufacturing Company Llc | Safety cabinet |
| DE10316656B8 (de) | 2003-04-11 | 2004-09-16 | Asecos Gmbh Sicherheit Und Umweltschutz | Sicherheitsschrank |
| DE202004004855U1 (de) | 2004-03-25 | 2004-08-12 | Asecos Gmbh | Sicherheitsschrank |
| DE102004021912A1 (de) | 2004-03-25 | 2005-10-13 | Asecos Gmbh | Sicherheitsschrank |
-
2005
- 2005-04-15 DE DE102005017427A patent/DE102005017427A1/de not_active Withdrawn
-
2006
- 2006-02-27 JP JP2008505746A patent/JP2008535980A/ja not_active Withdrawn
- 2006-02-27 WO PCT/EP2006/001772 patent/WO2006108469A1/de not_active Ceased
- 2006-02-27 CN CNA2006800126037A patent/CN101160341A/zh active Pending
- 2006-02-27 US US11/918,636 patent/US20090114523A1/en not_active Abandoned
- 2006-02-27 KR KR1020077026506A patent/KR20080015406A/ko not_active Withdrawn
- 2006-02-27 EP EP06707287A patent/EP1869102A1/de not_active Withdrawn
-
2008
- 2008-11-11 US US12/268,516 patent/US8029079B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| US20090114523A1 (en) | 2009-05-07 |
| CN101160341A (zh) | 2008-04-09 |
| JP2008535980A (ja) | 2008-09-04 |
| US20090134756A1 (en) | 2009-05-28 |
| WO2006108469A1 (de) | 2006-10-19 |
| US8029079B2 (en) | 2011-10-04 |
| DE102005017427A1 (de) | 2006-10-19 |
| EP1869102A1 (de) | 2007-12-26 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0105 | International application |
Patent event date: 20071114 Patent event code: PA01051R01D Comment text: International Patent Application |
|
| PG1501 | Laying open of application | ||
| PC1203 | Withdrawal of no request for examination | ||
| WITN | Application deemed withdrawn, e.g. because no request for examination was filed or no examination fee was paid |