KR102232559B1 - Dressing composition for salad containing rubus coreanum vinegar - Google Patents
Dressing composition for salad containing rubus coreanum vinegar Download PDFInfo
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- KR102232559B1 KR102232559B1 KR1020180048967A KR20180048967A KR102232559B1 KR 102232559 B1 KR102232559 B1 KR 102232559B1 KR 1020180048967 A KR1020180048967 A KR 1020180048967A KR 20180048967 A KR20180048967 A KR 20180048967A KR 102232559 B1 KR102232559 B1 KR 102232559B1
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- bokbunja
- vinegar
- sugar
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- 239000004332 silver Substances 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
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- 229920001864 tannin Polymers 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 235000010384 tocopherol Nutrition 0.000 description 1
- 229960001295 tocopherol Drugs 0.000 description 1
- 229930003799 tocopherol Natural products 0.000 description 1
- 239000011732 tocopherol Substances 0.000 description 1
- 235000010692 trans-unsaturated fatty acids Nutrition 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 238000002525 ultrasonication Methods 0.000 description 1
- 235000019156 vitamin B Nutrition 0.000 description 1
- 239000011720 vitamin B Chemical group 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 1
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/60—Salad dressings; Mayonnaise; Ketchup
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12J—VINEGAR; PREPARATION OR PURIFICATION THEREOF
- C12J1/00—Vinegar; Preparation or purification thereof
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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Abstract
본 발명은 복분자 식초가 함유된 샐러드용 드레싱 조성물에 관한 것으로, 더욱 상세하게는 정제수, 카놀라유, 복분자 식초, 당혼합물, 양조식초, 복분자 즙, 조미료 및 증점제로 이루어진다.
상기의 성분으로 이루어지는 샐러드용 드레싱 조성물은 복분자 식초가 함유되어 탄수화물, 유기산, 비타민 및 폴리페놀 등과 같은 영양성분이 풍부하며, 우수한 항산화효과를 나타낸다.The present invention relates to a dressing composition for salads containing bokbunja vinegar, and more specifically, purified water, canola oil, bokbunja vinegar, sugar mixture, brewed vinegar, bokbunja juice, seasoning and thickener.
Salad dressing composition consisting of the above ingredients contains bokbunja vinegar, rich in nutrients such as carbohydrates, organic acids, vitamins and polyphenols, and exhibits excellent antioxidant effects.
Description
본 발명은 복분자 식초가 함유된 샐러드용 드레싱 조성물에 관한 것으로, 더욱 상세하게는 복분자 식초가 함유되어 탄수화물, 유기산, 비타민 및 폴리페놀 등과 같은 영양성분이 풍부하며, 우수한 항산화효과를 나타내는 복분자 식초가 함유된 샐러드용 드레싱 조성물에 관한 것이다.The present invention relates to a salad dressing composition containing bokbunja vinegar, and more specifically, bokbunja vinegar is contained, rich in nutrients such as carbohydrates, organic acids, vitamins and polyphenols, and contains bokbunja vinegar showing excellent antioxidant effect. It relates to a dressing composition for salad.
복분자(Rubus coreanus Miquel)는 장미과에 속하는 낙엽 활엽관목으로 높이는 2-3 m에 달하고 줄기 끝은 자주색 또는 적색이고 흰색 분말로 덮여있는 산딸기 일종이다. 5-6월에 흰색의 꽃이 피고 7-8월에 반구형의 검붉은 색 열매를 맺는 다년생 식물로 한반도 황해도 이남지방과 중국, 일본의 해발 50-1,000 m 지역 산기슭 양지에서 야생하고 있다(Yuk CS, 1990). Rubus coreanus Miquel is a deciduous broad-leaved shrub belonging to the Rosaceae family. It reaches 2-3 m in height, and its stem end is purple or red, and is a kind of raspberry covered with white powder. It is a perennial plant that blooms white flowers in May-June and bears hemispherical dark red fruits in July-August. It is wild in the southern part of the Hwanghae-do region of the Korean peninsula and 50-1,000 m above sea level in China and Japan. , 1990).
또한 복분자 열매에는 탄수화물, 유기산, 비타민 B군, 비타민 C, 무기성분과 quercetin, ellagic acid, sanguiin H-5 등의 phenol성 화합물이 함유되어 있다(Lee JH et al., 2006, Pang GC et al., 1996). 복분자 열매의 항산화 활성을 지닌 Quercetin의 분리 및 동정 (Yoon et al., 2003), 복분자의 유산균 발효 및 생리활성 효과 등을 보고되고 있다(Park YS et al., 2003). 그 외에도 복분자 추출조건에 따른 페놀성 화합물의 특성 변화 (Yoon et al., 2003), 복분자의 항산화 활성(Yoon et al., 1995), 미숙 복분자로부터 가수분해된 tannin의 분리 (Lee & Lee, 1995), 미숙 복분자 분말을 첨가한 건면의 품질특성 등 다양한 생리활성이 있는 것으로 보고되고 있다(Lee et al., 2000). 복분자는 과실의 크기가 작으며 수분함량이 많아 부패하기 쉽고 저장이 어려워 복분자를 이용한 가공 식품개발에 관한 연구는 미흡한 수준이며, 기능성 식품 소재로서 활용가치가 크게 기대되고 있으나 아직 연구는 미비한 수준으로 이에 대한 활용도 잘 이루어지지 않고 있는 실정이다(Kim AJ et al., 2007b). In addition, bokbunja fruit contains carbohydrates, organic acids, vitamin B group, vitamin C, inorganic components and phenolic compounds such as quercetin, ellagic acid, and sanguiin H-5 (Lee JH et al., 2006, Pang GC et al. , 1996). Isolation and identification of Quercetin with antioxidant activity from bokbunja fruit (Yoon et al., 2003), lactic acid bacteria fermentation and physiological effects of bokbunja have been reported (Park YS et al., 2003). In addition, changes in properties of phenolic compounds according to extraction conditions of bokbunja (Yoon et al., 2003), antioxidant activity of bokbunja (Yoon et al., 1995), separation of hydrolyzed tannin from unripe bokbunja (Lee & Lee, 1995) ), it has been reported that there are various physiological activities such as quality characteristics of dried noodles added with unripe bokbunja powder (Lee et al., 2000). Raspberry fruit is small in size and has a high moisture content, which makes it easy to perish and storage. Therefore, research on the development of processed food using bokbunja is insufficient, and its application value as a functional food material is expected to be high, but research is still insufficient. The use of Korea is not well done (Kim AJ et al., 2007b).
샐러드는 대표적인 채소의 조리방법으로 주 요리 자체로 많이 이용되며, 이에 따라 샐러드의 맛을 더해 주는 드레싱의 이용률도 증가하고 있다(Choi SN et al., 2009). 드레싱은 식사 전 식욕을 돋우어 주고 음식의 맛과 향을 증진시키며 (Kim HD et al., 2002), 색상을 부여하는 등의 역할과 육류 위주의 서구식 식단에서 영양적 균형을 맞추는 역할, 부재료 첨가로 영양가를 높이고 소화 작용을 도와주는 기능을 가지고 있다(Kim MH, 2003; Kim YH, 2007; Lee KI, 2004). Salad is a typical vegetable cooking method and is widely used as the main dish itself, and accordingly, the use of dressings that add flavor to the salad is increasing (Choi SN et al., 2009). Dressing arouses appetite before meals, improves taste and aroma of food (Kim HD et al., 2002), plays a role in imparting color, and balances nutrition in a meat-oriented Western diet, and additives are added. It has the function of increasing nutritional value and helping digestion (Kim MH, 2003; Kim YH, 2007; Lee KI, 2004).
샐러드를 먹기 위해서 사용되는 드레싱은 식품공전(2008)에서 “식품을 제조·가공·조리함에 있어 식품의 풍미를 돋우기 위한 목적으로 사용되는 것으로, 식용유, 식초 등을 주원료로 하여 식염, 당류, 향신료, 알류 또는 식품첨가물을 가하고 유화시키거나 분리액상으로 제조한 것 또는 이에 채소류, 과일류 등을 가한 것으로 드레싱, 마요네즈를 말한다”고 정의하고 있다. Dressings used to eat salads are used for the purpose of enhancing the flavor of foods in manufacturing, processing, and cooking foods in the Food Code (2008). It is defined as "dressing, mayonnaise," which is made by adding eggs or food additives and emulsifying or prepared in the form of a separated liquid, or adding vegetables, fruits, etc. to it.
일반적으로 드레싱이란 대개 차가운 종류의 소스로 주로 차가운 채소에 뿌려 먹는 것을 말하며 드레싱의 종류로는 기름과 식초의 혼합 드레싱, 마요네즈가 들어간 드레싱, 조리된 드레싱의 3종류가 있고 사용하는 재료의 질에 따라 그 풍미와 물성이 좌우 된다 (Sharon, 1990). In general, dressing is usually a cold type of sauce, which is mainly sprinkled on cold vegetables, and there are three types of dressings: mixed dressing of oil and vinegar, dressing with mayonnaise, and cooked dressing, depending on the quality of the ingredients used. Its flavor and properties depend (Sharon, 1990).
드레싱은 주재료로 기름 및 산이 이용되고 맛과 유화작용을 돕는 향신료와 과일 등이 부재료로 혼입되기도 하는데, 이때 향신료 과일 등은 드레싱의 항산화와 항균성을 증가시키는 것으로 보고되고 있다(Frutos, M.J. et al., 2005). Oil and acid are used as main ingredients for dressings, and spices and fruits that help taste and emulsification are mixed as subsidiary materials. At this time, spices and fruits have been reported to increase the antioxidant and antibacterial properties of the dressing (Frutos, MJ et al. , 2005).
최근 건강에 대한 관심이 증가하면서 기존의 드레싱에 다양한 천연소재를 첨가한 연구가 보고되고 있으며, 이에 관한 연구로는 표고버섯 샐러드 드레싱 (Jung HA et al., 2011), 오미자 샐러드 드레싱 (Yim SB et al., 2012), 블루베리즙 요구르트드레싱 (Lee WG et al., 2012), 생강 샐러드 드레싱 (Jung HA et al., 2013), 복분자즙 요구르트드레싱 (Park JY et al., 2013), 오디즙 요구르트 드레싱 (Park KB, 2014), 머루 분말 샐러드 드레싱 (Bing DJ et al., 2015), 아로니아즙 요구르트 드레싱 (Park KB et al., 2015) 등이 보고된바 있다.Recently, as interest in health has increased, studies in which various natural ingredients are added to existing dressings have been reported, and studies on this include shiitake mushroom salad dressing (Jung HA et al., 2011), Schisandra chinensis salad dressing (Yim SB et al. al., 2012), blueberry juice yogurt dressing (Lee WG et al., 2012), ginger salad dressing (Jung HA et al., 2013), bokbunja juice yogurt dressing (Park JY et al., 2013), mulberry juice Yogurt dressing (Park KB, 2014), berry powder salad dressing (Bing DJ et al., 2015), aronia juice yogurt dressing (Park KB et al., 2015) have been reported.
따라서 본 연구 사업에서는 기능성이 입증된 복분자를 이용한 식초를 제조한 후 이를 이용한 샐러드용 드레싱 조성물을 개발하여 이화학적 특성 및 기능성 성분을 분석하여 기능성이 부합된 복분자 식초가 함유된 샐러드용 드레싱 조성물을 개발하고자 한다.Therefore, in this research project, after preparing vinegar using bokbunja with proven functionality, we developed a salad dressing composition using it, analyzed physicochemical properties and functional ingredients, and developed a salad dressing composition containing bokbunja vinegar with matching functionality. I want to.
본 발명의 목적은 복분자 식초가 함유되어 탄수화물, 유기산, 비타민 및 폴리페놀 등과 같은 영양성분이 풍부하며, 우수한 항산화효과를 나타내는 복분자 식초가 함유된 샐러드용 드레싱 조성물을 제공하는 것이다.It is an object of the present invention to provide a salad dressing composition containing bokbunja vinegar, rich in nutrients such as carbohydrates, organic acids, vitamins and polyphenols, and exhibiting excellent antioxidant effects.
본 발명의 목적은 정제수, 카놀라유, 복분자 식초, 당혼합물, 양조식초, 복분자 즙, 조미료 및 증점제로 이루어지는 것을 특징으로 하는 복분자 식초가 함유된 샐러드용 드레싱 조성물을 제공함에 의해 달성된다.An object of the present invention is achieved by providing a salad dressing composition containing bokbunja vinegar, characterized in that it consists of purified water, canola oil, bokbunja vinegar, sugar mixture, brewed vinegar, bokbunja juice, seasoning and thickener.
본 발명의 바람직한 특징에 따르면, 상기 복분자식초를 이용한 샐러드용 드레싱 조성물은 정제수 100 중량부, 카놀라유 60 내지 70 중량부, 복분자 식초 30 내지 35 중량부, 당혼합물 60 내지 65 중량부, 양조식초 30 내지 35 중량부, 복분자 즙 10 내지 15 중량부, 조미료 20 내지 25 중량부 및 증점제 0.1 내지 0.5 중량부로 이루어지는 것으로 한다.According to a preferred feature of the present invention, the dressing composition for salad using bokbunja vinegar is 100 parts by weight of purified water, 60 to 70 parts by weight of canola oil, 30 to 35 parts by weight of bokbunja vinegar, 60 to 65 parts by weight of sugar mixture, 30 to brewed vinegar. It shall consist of 35 parts by weight, 10 to 15 parts by weight of bokbunja juice, 20 to 25 parts by weight of seasoning, and 0.1 to 0.5 parts by weight of a thickener.
본 발명의 더 바람직한 특징에 따르면, 상기 복분자 식초는 복분자와 설탕을 혼합하여 당도가 23 내지 25 brix가 되도록 혼합물을 제조한 후에, 상기 혼합물 100 중량부에 효모 0.5 내지 1.5 중량부를 투입하고, 20 내지 30℃에서 8 내지 12일간 1차 발효한 후에, 고형분을 제거하고 효모 0.05 내지 0.15 중량부를 추가로 투입하고 24 내지 26℃에서 28 내지 32일간 2차 발효하여 제조되는 것으로 한다.According to a more preferred feature of the present invention, the bokbunja vinegar is mixed with bokbunja and sugar to prepare a mixture so that the sugar content is 23 to 25 brix, and then 0.5 to 1.5 parts by weight of yeast is added to 100 parts by weight of the mixture, and 20 to After the first fermentation at 30° C. for 8 to 12 days, solids are removed, 0.05 to 0.15 parts by weight of yeast are additionally added, and secondary fermentation is performed at 24 to 26° C. for 28 to 32 days.
본 발명의 더욱 바람직한 특징에 따르면, 상기 당혼합물은 설탕과 올리고당이 1:0.7 내지 0.8 중량부로 혼합되어 이루어지는 것으로 한다.According to a more preferred feature of the present invention, the sugar mixture is made by mixing sugar and oligosaccharides in an amount of 1:0.7 to 0.8 parts by weight.
본 발명의 더욱 더 바람직한 특징에 따르면, 상기 조미료는 겨자씨, 소금, 건조마늘 및 후추로 이루어지는 것으로 한다.According to an even more preferred feature of the present invention, the seasoning is to be made of mustard seeds, salt, dry garlic and pepper.
본 발명의 더욱 더 바람직한 특징에 따르면, 상기 증점제는 잔탄검으로 이루어지는 것으로 한다.According to a further preferred feature of the present invention, the thickener is made of xanthan gum.
본 발명에 따른 복분자 식초가 함유된 샐러드용 드레싱 조성물은 복분자 식초가 함유되어 탄수화물, 유기산, 비타민 및 폴리페놀 등과 같은 영양성분이 풍부하며, 우수한 항산화효과를 나타내는 샐러드용 드레싱 조성물을 제공한다.The dressing composition for salads containing bokbunja vinegar according to the present invention is rich in nutrients such as carbohydrates, organic acids, vitamins and polyphenols by containing bokbunja vinegar, and provides a salad dressing composition exhibiting excellent antioxidant effect.
도 1은 본 발명에 실시예 1을 통해 제조된 복분자 식초가 함유된 샐러드용 드레싱 조성물을 촬영하여 나타낸 사진이다.
도 2는 본 발명의 실시예 1을 통해 제조된 복분자 식초가 함유된 샐러드용 드레싱 조성물을 보관용기에 투입한 상태를 촬영하여 나타낸 사진이다.1 is a photograph showing a salad dressing composition containing bokbunja vinegar prepared through Example 1 in the present invention.
2 is a photograph showing a state in which a dressing composition for salad containing bokbunja vinegar prepared through Example 1 of the present invention is put into a storage container.
이하에는, 본 발명의 바람직한 실시예와 각 성분의 물성을 상세하게 설명하되, 이는 본 발명이 속하는 기술분야에서 통상의 지식을 가진 자가 발명을 용이하게 실시할 수 있을 정도로 상세하게 설명하기 위한 것이지, 이로 인해 본 발명의 기술적인 사상 및 범주가 한정되는 것을 의미하지는 않는다.Hereinafter, a preferred embodiment of the present invention and the physical properties of each component will be described in detail, but this is for explaining in detail enough that one of ordinary skill in the art can easily carry out the invention, This does not mean that the technical spirit and scope of the present invention are limited.
본 발명에 따른 복분자 식초가 함유된 샐러드용 드레싱 조성물은 정제수, 카놀라유, 복분자 식초, 당혼합물, 양조식초, 복분자 즙, 조미료 및 증점제로 이루어지며, 정제수 100 중량부, 카놀라유 60 내지 70 중량부, 복분자 식초 30 내지 35 중량부, 당혼합물 60 내지 65 중량부, 양조식초 30 내지 35 중량부, 복분자 즙 10 내지 15 중량부, 조미료 20 내지 25 중량부 및 증점제 0.1 내지 0.5 중량부로 이루어지는 것이 바람직하다.The dressing composition for salads containing bokbunja vinegar according to the present invention consists of purified water, canola oil, bokbunja vinegar, sugar mixture, brewed vinegar, bokbunja juice, seasoning and thickener, 100 parts by weight of purified water, 60 to 70 parts by weight of canola oil, bokbunja It is preferable to consist of 30 to 35 parts by weight of vinegar, 60 to 65 parts by weight of sugar mixture, 30 to 35 parts by weight of brewed vinegar, 10 to 15 parts by weight of bokbunja juice, 20 to 25 parts by weight of seasoning, and 0.1 to 0.5 parts by weight of thickener.
상기 복분자 식초는 복분자와 설탕을 혼합하여 당도가 23 내지 25 brix가 되도록 혼합물을 제조한 후에, 상기 혼합물 100 중량부에 효모 0.5 내지 1.5 중량부를 투입하고, 20 내지 30℃에서 8 내지 12일간 1차 발효한 후에, 고형분을 제거하고 효모 0.05 내지 0.15 중량부를 추가로 투입하고 24 내지 26℃에서 28 내지 32일간 2차 발효하여 제조된다.The bokbunja vinegar is mixed with bokbunja and sugar to prepare a mixture so that the sugar content is 23 to 25 brix, and then 0.5 to 1.5 parts by weight of yeast is added to 100 parts by weight of the mixture, and the first for 8 to 12 days at 20 to 30°C After fermentation, the solid content is removed, and 0.05 to 0.15 parts by weight of yeast are additionally added, followed by secondary fermentation at 24 to 26°C for 28 to 32 days.
또한, 상기 당혼합물은 설탕과 올리고당이 1:0.7 내지 0.8 중량부로 혼합되어 이루어진다.In addition, the sugar mixture is made by mixing sugar and oligosaccharides in an amount of 1:0.7 to 0.8 parts by weight.
또한, 상기 조미료는 겨자씨, 소금, 건조마늘 및 후추로 이루어지며, 겨자씨 12 내지 14 중량부, 소금 4.5 내지 5.5 중량부, 건조마늘 3 내지 3.5 중량부 및 후추 1 내지 2 중량부로 이루어진다.In addition, the seasoning consists of mustard seeds, salt, dry garlic and pepper, and consists of 12 to 14 parts by weight of mustard seeds, 4.5 to 5.5 parts by weight of salt, 3 to 3.5 parts by weight of dry garlic, and 1 to 2 parts by weight of pepper.
또한, 상기 증점제는 잔탄검으로 이루어지는 것이 바람직하다.In addition, the thickener is preferably made of xanthan gum.
상기의 성분으로 이루어지는 복분자 식초가 함유된 샐러드용 드레싱 조성물은 정제수 100 중량부, 카놀라유 60 내지 70 중량부, 복분자 식초 30 내지 35 중량부, 당혼합물 60 내지 65 중량부, 복분자 즙 10 내지 15 중량부, 조미료 20 내지 25 중량부 및 증점제 0.1 내지 0.5 중량부를 균질기에 투입하고 교반하여 균질화 한 후에 균질화된 혼합물을 살균기로 100℃의 온도에서 50 내지 70초 동안 살균하여 살균처리한 후에 보관용기에 투입하여 보관하게 된다.The dressing composition for salad containing bokbunja vinegar consisting of the above ingredients is 100 parts by weight of purified water, 60 to 70 parts by weight of canola oil, 30 to 35 parts by weight of bokbunja vinegar, 60 to 65 parts by weight of sugar mixture, 10 to 15 parts by weight of bokbunja juice , 20 to 25 parts by weight of seasoning and 0.1 to 0.5 parts by weight of a thickener were added to a homogenizer, stirred to homogenize, and then the homogenized mixture was sterilized with a sterilizer at a temperature of 100° C. for 50 to 70 seconds and then put into a storage container. Will be kept.
본 발명에서 사용되는 복분자의 일반성분을 분석하였고, 비교군으로 오디를 사용하여 함께 분석하여 아래 표 1에 나타내었다.General components of bokbunja used in the present invention were analyzed, and analyzed together using Audi as a comparative group, and are shown in Table 1 below.
아래 표 1에 나타낸 바와 같이 복분자와 오디의 수분함량은 86.35±1.43과 88.90±0.20로 측정되었고, 단백질은 1.34±0.01과 0.64±0.22로 오디에 비해 복분자가 약 2배 더 높게 측정되었다. 지질은 0.10±0.01과 0.42±0.51로 각각 측정되었는데 오디가 복분자에 비해 약 4배 더 높게 측정되었다. 회분은 0.63±0.05와 0.53±0.01 로 각각 확인되었다.As shown in Table 1 below, the moisture content of bokbunja and Audi was measured as 86.35±1.43 and 88.90±0.20, and the protein was 1.34±0.01 and 0.64±0.22, which was about 2 times higher than that of Audi. Lipids were measured at 0.10±0.01 and 0.42±0.51, respectively, but Audi was measured 4 times higher than that of bokbunja. Ash content was found to be 0.63±0.05 and 0.53±0.01, respectively.
<표 1><Table 1>
또한, 본분자의 DPPH-free radical 소거활성 측정하였는데, DPPH는 아스코르빈산 및 토코페롤, polyhydroxy 방향족 화합물, 방향족 아민류에 의해 전자나 수소를 받아 불가역적으로 안정한 분자를 형성하여 환원됨에 따라 짙은 자색이 탈색되는 원리를 이용하여 다양한 천연소재로부터 항산화 물질을 탐색하기 위해 많이 이용되고 있으며 인체 내에서 특히 지방질의 산화과정에서 생성되는 free radical들은 세포의 노화를 촉진시키고 생체세포의 방어기전을 저하시킬 뿐만 아니라 세포활성을 저해하므로 이들 free radical의 생성을 근본적으로 억제하거나 이미 생성된 free radical들의 안정화를 통해 생체세포를 보호할 필요가 있다. 전자공여작용은 이러한 생물활성 free radical에 전자를 공여하여 세포 성분의 산화를 억제시킨다. 복분자와 비교하기 위하여 고창에서 많이 재배되고 있는 오디와 함께 DPPH(2,2-diphenyl-1-picryl-hydrazyl) radical 소거활성을 측정하였고 그 결과 값은 아래 표 2에 나타내었다.In addition, DPPH-free radical scavenging activity of this molecule was measured. DPPH is irreversibly received by electrons or hydrogens from ascorbic acid, tocopherol, polyhydroxy aromatic compounds, and aromatic amines to form a stable molecule, resulting in decolorization of dark purple. It is widely used to search for antioxidants from various natural materials by using the principle. In the human body, in particular, free radicals generated during the oxidation of fats promote cell aging and degrade the defense mechanisms of living cells, as well as cell activity. Therefore, it is necessary to fundamentally inhibit the generation of these free radicals or to protect living cells by stabilizing the free radicals that have already been generated. The electron donating action inhibits the oxidation of cellular components by donating electrons to these biologically active free radicals. To compare with bokbunja, DPPH (2,2-diphenyl-1-picryl-hydrazyl) radical scavenging activity was measured with mulberry grown in Gochang, and the results are shown in Table 2 below.
<표 2><Table 2>
위에 표 2에 나타낸 것처럼, 두 베리의 DPPH-free radical 소거활성의 IC50 값은 각각 6.19와 5.59로 복분자가 오디에 비해 약간 높은 값을 나타내었다. As shown in Table 2 above, the IC 50 values of the DPPH-free radical scavenging activity of the two berries were 6.19 and 5.59, respectively, indicating a slightly higher value than that of Mulberry.
또한, 본 발명에 사용되는 복분자와 오디의 ABTS radical 소거활성을 측정한 결과는 아래 표 3에 나타내었다.In addition, the results of measuring the ABTS radical scavenging activity of bokbun and mulberry used in the present invention are shown in Table 3 below.
ABTS[2,2'-azinbis-(3-ethyl-benzothiazoline-6-sulfonic acid)]는 비교적 안정한 free radical로서 DPPH 방법과 함께 항산화활성을 스크리닝하는데 많이 이용되고 있다. 또한 lipophilic 또는 hydrophilic 항산화 물질의 측정에 적용 가능한 방법으로 알려져 있다. ABTS는 양이온 라디칼을DPPH는 음이온 라디칼을 소거하는 활성을 흡광도로 측정하는 방법으로 두 방법에 대한 기질과 반응물질과의 결합정도가 달라 추출물을 이용한 라디칼 소거활성 측정값에서 차이가 나타날 수 있다ABTS[2,2'-azinbis-(3-ethyl-benzothiazoline-6-sulfonic acid)] is a relatively stable free radical and is widely used for screening antioxidant activity along with the DPPH method. It is also known as a method applicable to the measurement of lipophilic or hydrophilic antioxidants. ABTS is a method to measure the activity of scavenging cationic radicals and DPPH is an anionic radical by absorbance. The degree of binding between the substrate and the reactant is different between the two methods, so there may be a difference in the measured value of the radical scavenging activity using the extract.
<표 3><Table 3>
위에 표 3에 나타낸 것처럼, 두 베리의 ABTs radical 소거활성의 IC50 값은 각각 11.36과 16.13으로 오디가 복분자에 비해 높은 값을 나타내었다. As shown in Table 3 above, the IC 50 values of the ABTs radical scavenging activity of the two berries were 11.36 and 16.13, respectively, and Audi showed higher values than bokbunja.
또한, 본 발명에 사용되는 복분자의 총 플라보노이드 성분을 분석하였는데, 폴라보노이드는 주로 anthocyanidins, flavonols, flavones, cathechins 및 flavanones 등으로 구성되어 있으며, 식물에 다량 존재하는 플라보노이드는 항산화 작용, 순환기 질환 예방, 항염, 항알러지, 항균, 항바이러스, 면역증강 등 다양한 기능성 생리활성 효과를 보인다고 보고하였다(Kawaguchi K 1997, Middleton E 1997, Nakagawa M 1974). 복분자와 오디의 총 플라보노이드 함량은 아래 표 4에 나타내었다.In addition, the total flavonoid components of bokbunja used in the present invention were analyzed, and the polaronoids are mainly composed of anthocyanidins, flavonols, flavones, cathechins and flavanones, and flavonoids present in a large amount in plants have antioxidant activity, prevention of circulatory diseases, It has been reported that it exhibits various functional physiological effects such as anti-inflammatory, anti-allergic, antibacterial, antiviral, and immunity enhancement (Kawaguchi K 1997, Middleton E 1997, Nakagawa M 1974). The total flavonoid contents of bokbunja and mulberry are shown in Table 4 below.
<표 4><Table 4>
위에 표 4에 나타낸 것처럼, 복분자의 총 플라보노이드 함량은 0.62mg/mL 이었고 오디는 0.59mg/mL을 나타내었다. As shown in Table 4 above, the total flavonoid content of bokbunja was 0.62mg/mL and that of mulberry was 0.59mg/mL.
또한, 본 발명에 사용되는 복분자의 총 폴리페놀 함량을 측정하여 아래 표 5에 나타내었다.In addition, the total polyphenol content of bokbunja used in the present invention was measured and shown in Table 5 below.
식물체에 존재하는 페놀화합물은 2차 대사산물로서 분자 내에 하나 이상의 phenolic hydroxyl(OH)기를 가지고 있어서 단백질 및 거대분자들과 결합하는 성질이 있고 공명 안정화된 구조로써 전자를 수용하는 기작으로 항산화 반응에 직접적으로 기여하면서 다양한 식물계에서 발견되는 중요한 성분이다. 2가 금속이온과의 결합력이 우수하며 수소 공여 작용을 통해 free radical을 제거함으로써 콜레스테롤 저하, 고혈압이나 동맥경화 억제, 중성지질의 생성 억제에 의한 비만 방지 및 모세혈관의 저항?r 증진 등의 효과가 있으며 항산화 작용과 항암 등의 효과를 나타내는 것으로 알려져 있다.Phenolic compounds present in plants are secondary metabolites and have one or more phenolic hydroxyl (OH) groups in the molecule, so they bind to proteins and macromolecules, and have a resonance-stabilized structure that accepts electrons directly for antioxidant reactions. It is an important component found in various plant kingdoms while contributing to it. It has excellent binding power with divalent metal ions and has effects such as lowering cholesterol, inhibiting hypertension or arteriosclerosis by removing free radicals through hydrogen donating action, preventing obesity by inhibiting the production of neutral lipids, and enhancing resistance of capillaries. It is known to exhibit antioxidant and anti-cancer effects.
<표 5><Table 5>
이하에서는, 본 발명에 따른 복분자 식초가 함유된 샐러드용 드레싱 조성물의 제조방법 및 그 제조방법을 통해 제조된 샐러드용 드레싱 조성물의 물성을 실시예를 들어 설명하기로 한다.Hereinafter, a method of preparing a dressing composition for a salad containing bokbunja vinegar according to the present invention and physical properties of a dressing composition for a salad prepared through the method will be described with reference to examples.
<제조예 1><Production Example 1>
복분자와 설탕을 혼합하여 당도가 24 brix가 되도록 혼합물을 제조한 후에, 상기 혼합물 100 중량부에 효모 1.0 중량부를 투입하고, 5℃에서 10일간 1차 발효한 후에, 고형분을 제거하고 효모 0.1 중량부를 추가로 투입하고 25℃에서 30일간 2차 발효하여 복분자 식초를 제조하였다.After preparing a mixture so that the sugar content is 24 brix by mixing bokbun and sugar, 1.0 parts by weight of yeast was added to 100 parts by weight of the mixture, and after primary fermentation at 5°C for 10 days, the solids were removed and 0.1 parts by weight of yeast It was further added and fermented at 25° C. for 30 days to prepare bokbunja vinegar.
본 발명에서 원재료의 일반성분은 AOAC(2000)방법으로 분석하였다. 수분함량은 105℃ 오븐을 이용한 상압가열법을 이용하여 측정하였고, 조지질은 에테르를 용매로 사용한 속실렛법을 이용하여 속실렛장치(Extraction Unit E-816)를 이용하여 측정하였다. 단백질함량은 미량 켈달법, 회분은 550℃ 회화로를 이용한 직접 회화법으로 측정하였다.In the present invention, general components of raw materials were analyzed by the AOAC (2000) method. Moisture content was measured using an atmospheric pressure heating method using an oven at 105°C, and crude lipids were measured using a Soxhlet device (Extraction Unit E-816) using the Soxhlet method using ether as a solvent. The protein content was measured by the trace Keldahl method, and the ash was measured by the direct incineration method using a 550°C incinerator.
또한, DPPH(2,2-diphenyl-1-picryl-hydrazyl) radical 소거활성은 농도별로 조제한 시료액 100mL에 ethanol 200mL를 가하고 2×10-4M DPPH용액 300mL를 가한 후 5초간 vortex mixer로 혼합하여 실온에서 30분간 반응시키고 ELISA(Synergy HT, Biotec, Washington DC, USA)를 사용하여 517nm에서 흡광도를 측정하였음. 대조구는 시료 대신 ethanol을 첨가하여 실험하였다.In addition, for DPPH (2,2-diphenyl-1-picryl-hydrazyl) radical scavenging activity, 200 mL of ethanol was added to 100 mL of sample solution prepared by concentration, 300 mL of 2×10 -4 M DPPH solution was added, and then mixed with a vortex mixer for 5 seconds. After reacting at room temperature for 30 minutes, absorbance was measured at 517 nm using ELISA (Synergy HT, Biotec, Washington DC, USA). Control was experimented by adding ethanol instead of the sample.
DPPH radical scavenging activity(%)=(1 - 시료의 흡광도/대조구의 흡광도) ×100DPPH radical scavenging activity(%)=(1-absorbance of sample/absorbance of control) ×100
또한, ABTS radical을 이용한 항산화 활성의 측정은 potassium persulfate와의 반응에 의해 생성된 ABTS radical이 추출물 내의 항산화 물질에 의해 제거되어 radical 특유의 색인 청록색이 탈색되는 것을 이용한 방법으로 DPPH 방법과 함께 항산화 활성을 탐색하는데 자주 이용되고 있가. ABTS assay는 Art 등의 방법을 변형하여 측정하였다. 농도별 (1, 5, 10, 25, 50/mL)로 제조한 시료를 96well plate에 5mL를 취하고 pH 7.0으로 맞춘 2.45 mM ABTs 용액 195 mL를 넣은 후 잘 교반한 후 7 min동안 방치 한 다음 ELISA를 이용하여 734 nm에서 흡광도를 측정하였고, 대조구는 시료 대신 ethanol을 첨가하여 실험하였다.In addition, the measurement of antioxidant activity using ABTS radicals is a method using the fact that ABTS radicals generated by reaction with potassium persulfate are removed by antioxidants in the extract, and the characteristic color of the radical is decolorized, and the antioxidant activity is explored with the DPPH method. Is it used often? ABTS assay was measured by modifying methods such as Art. Take 5 mL of a sample prepared by concentration (1, 5, 10, 25, 50/mL) into a 96 well plate, add 195 mL of a 2.45 mM ABTs solution adjusted to pH 7.0, stir well, and leave for 7 min, then ELISA Absorbance was measured at 734 nm using, and ethanol was added instead of the sample for the control.
ABTS radical scavenging activity (%) = (1 - A/B) × 100ABTS radical scavenging activity (%) = (1-A/B) × 100
A: Absorbance of sampleA: Absorbance of sample
B: Absorbance of blankB: Absorbance of blank
또한, 플라보노이드 함량 또한 건강기능식품공전 방법을 이용하여 측정하였다. 즉 각각의 시료 0.5 mL에 ethanol 1.5 mL, 10% 질산알루미늄 0.1 mL, 1 M 초산칼슘 0.1 mL, 증류수 2.8 mL을 순서대로 가하고 vortex mixer로 혼합하여 암소에서 40분간 반응시키고 UV/VIS spectrophotometer(UV-2450, Shimadzu Co., Kyoto, Japan)를 사용하여 415nm에서 흡광도를 측정하였다. 이때 quercetin(Sigma-Aldrich Co., St. Louis, Mo, USA)을 표준물질로 사용하여 검량곡선을 작성하고 이로부터 총 폴리페놀 함량을 구하였다. In addition, the flavonoid content was also measured using the health functional food code method. That is, 1.5 mL of ethanol, 0.1 mL of 10% aluminum nitrate, 0.1 mL of 1 M calcium acetate, and 2.8 mL of distilled water were sequentially added to 0.5 mL of each sample, mixed with a vortex mixer, and reacted in the dark for 40 minutes, followed by UV/VIS spectrophotometer (UV- 2450, Shimadzu Co., Kyoto, Japan) was used to measure the absorbance at 415 nm. At this time, a calibration curve was prepared using quercetin (Sigma-Aldrich Co., St. Louis, Mo, USA) as a standard material, and the total polyphenol content was calculated from this.
또한, 총 폴리페놀 함량은 페놀성 물질인 phosphomolybdic acid와 반응하여 청색을 나타내는 원리를 이용한 Folin-Denis 방법을 이용하여 측정하였다. 시료액 1mL에 Folin-Ciocalteau’s phenol regent 1mL를 가하고 3 분간 반응시킨 다음 10% Na2CO3 1mL를 넣고 1 시간 동안 실온에서 반응시킨 후 UV/VIS spectrophotometer(UV-2450, Shimadzu Co., Kyoto, Japan)를 사용하여 700nm에서 비색정량 하였다. 이때 gallic acid(Sigma-Aldrich Co., St. Louis, Mo, USA)를 표준물질로 사용하여 검량곡선을 작성하고 이로부터 총 폴리페놀 함량을 구하였다.In addition, the total polyphenol content was measured using the Folin-Denis method using the principle of showing a blue color by reacting with phosphomolybdic acid, a phenolic substance. 1 mL of Folin-Ciocalteau's phenol regent was added to 1 mL of the sample solution, reacted for 3 minutes, 1 mL of 10% Na 2 CO 3 was added and reacted at room temperature for 1 hour, followed by UV/VIS spectrophotometer (UV-2450, Shimadzu Co., Kyoto, Japan) ) Was used to colorimetrically quantify at 700 nm. At this time, a calibration curve was prepared using gallic acid (Sigma-Aldrich Co., St. Louis, Mo, USA) as a standard material, and the total polyphenol content was calculated from this.
또한, 당도는 휴대용 당도계(Refractometer, PAL-1, Brix 0 to 53%, Atago, Japan)를 이용하여 시료 착즙액을 3회 반복 측정한 후 그 평균값으로 나타내었다.In addition, the sugar content was measured repeatedly three times using a portable sugar content meter (Refractometer, PAL-1, Brix 0 to 53%, Atago, Japan) and then expressed as the average value.
또한, pH 측정은 pH meter(SevenEasy, Mettler Toledo, Swiss)를 이용하여 3회 반복측정하였고, 산도는 자동산도계(Easy pH, METTLER TOLEDO, Swizerland)를 이용하여 측정하고 3번 반복 측정하여 평균값으로 나타내었다.In addition, the pH measurement was repeated three times using a pH meter (SevenEasy, Mettler Toledo, Swiss), and the acidity was measured using an automatic acidity meter (Easy pH, METTLER TOLEDO, Swizerland) and measured three times as an average value. Indicated.
또한, 색도 측정은 분광색차계(CM-5, Minolta, Osaka, Japan)를 사용하여 L(Lightness), a(Redness), b(Yellowness) 값으로 표시하였으며, 각 시료를 3회 반복 측정하여 그 평균값을 나타내었다. In addition, chromaticity measurement was expressed as L (Lightness), a (Redness), and b (Yellowness) values using a spectroscopic colorimeter (CM-5, Minolta, Osaka, Japan). The average value is shown.
또한, 아미노산 분석은 HPLC를 이용하여 분석하였으며, Borate buffer, OPA/MPA, FMOC 시약을 시료와 단계적으로 혼합한 후 반응이 완료되면 시료를 칼럼에 주입하여 분석하였음. HPLC 조건은 Dionex Ultimate 3000 (Thremo Dionex, USA)로 분석하였고, 칼럼은 VDSpher 100 C18-E (4.6mm x 150mm, 3.5um/VDS optilab, Germany)을 사용하였다.In addition, amino acid analysis was performed using HPLC. Borate buffer, OPA/MPA, and FMOC reagents were mixed with the sample in stages, and when the reaction was completed, the sample was injected into the column for analysis. HPLC conditions were analyzed with Dionex Ultimate 3000 (Thremo Dionex, USA), and a column was used as VDSpher 100 C18-E (4.6mm x 150mm, 3.5um/VDS optilab, Germany).
또한, 무기성분은 Osborne & Voogt (1981)의 방법에 따라 시료를 질산과 과산화수소, 증류수를 이용하여 마이크로웨이브 분해기(Ultrawave, Milestone, Italy)로 시료를 분해하였고, 냉각 후 소량의 증류수로 희석한 후 50 mL 정용플라스크로 옮겨 서 증류수로 정용하였다. 이 용액을 ICP-OES(Agilent 720-ES, Melbourne, Australia)로 분석하여 무기성분의 함량을 구하였다. 분석조건은 power의 경우 1.20 kw, analysis pump rate는 15 rpm, rinse time은 10 sec로 하였다.In addition, for inorganic components, the sample was decomposed using a microwave digester (Ultrawave, Milestone, Italy) using nitric acid, hydrogen peroxide, and distilled water according to the method of Osborne & Voogt (1981). After cooling, the sample was diluted with a small amount of distilled water. Transfer to a 50 mL diaphragm flask and diaphragm with distilled water. This solution was analyzed by ICP-OES (Agilent 720-ES, Melbourne, Australia) to determine the content of inorganic components. Analysis conditions were 1.20 kw for power, 15 rpm for analysis pump rate, and 10 sec for rinse time.
또한, 유기산 분석은 시료를 호모게나이저로 고르게 균질화한 후 10 g을 100 mL 용량 플라스크에 취한 후 증류수로 표시선까지 정확히 채우고, 초음파로 1시간 추출하였음. 5℃의 원심분리기 3,000 rpm에서 30분간 원심분리한 후 상등액을 취한 다음, membrane filter (0.45 μm)로 여과 후 HPLC (Dionex Ultimate 3000 (USA)로 분석하였으며, 표준 유기산의 각 retention time을 확인하였고, 그 때의 표준 유기산 면적과 시료의 면적으로부터 함량을 계산하였다. In addition, for organic acid analysis, after homogenizing the sample evenly with a homogenizer, 10 g was taken into a 100 mL volumetric flask, accurately filled with distilled water to the indicated line, and extracted for 1 hour by ultrasonication. After centrifuging for 30 minutes at 3,000 rpm in a centrifuge at 5°C, the supernatant was taken, filtered with a membrane filter (0.45 μm) and analyzed by HPLC (Dionex Ultimate 3000 (USA), and each retention time of the standard organic acid was confirmed. The content was calculated from the area of the standard organic acid and the area of the sample at that time.
또한, 유리당 분석은 시료 5 g에 증류수 50 mL를 정용하여 30℃ 수욕조에서 30분간 진탕한 후 15,000 rpm에서 20분간 원심분리 한 다음 25 mL로 정용하고 0.45 μm syring filter로 여과시킨 것을 HPLC ystems (Waters 2695, Milford, CT, USA)로 분석하였음. HPLC 조건으로 칼럼은 carbohydrate analysis (4.6×150 mm, TST, Waters, Newcastle, DE, USA)를 사용하였고, 용매는 acetonitrile-water (75:25v/v), 유속은 1.5 mL/min으로 분석하였고, 유리당 함량은 시료 중의 각 유리당과 동일한 표준물질 (Sigma Chemical Co., St. Louis, MO, USA)을 이용하여 작성한 검량선으로부터 계산하였다.In addition, for the analysis of free sugar, 50 mL of distilled water was added to 5 g of a sample, shaken for 30 minutes in a water bath at 30°C, centrifuged at 15,000 rpm for 20 minutes, and then measured at 25 mL and filtered with a 0.45 μm syring filter. Waters 2695, Milford, CT, USA). As HPLC conditions, the column was carbohydrate analysis (4.6×150 mm, TST, Waters, Newcastle, DE, USA), the solvent was acetonitrile-water (75:25v/v), and the flow rate was analyzed at 1.5 mL/min, The free sugar content was calculated from a calibration curve prepared using the same standard material as each free sugar in the sample (Sigma Chemical Co., St. Louis, MO, USA).
상기 제조예 1을 통해 제조된 복분자 식초의 당도, 산도, pH를 측정하여 아래 표 6에 나타내었다.The sugar content, acidity, and pH of the bokbunja vinegar prepared through Preparation Example 1 were measured and shown in Table 6 below.
<표 6><Table 6>
위에 표 6에 나타낸 것처럼, 복분자 식초의 당도는 10°Brix 였고 산도와 pH는 각각 5.05 %와 3.32를 나타냈다.As shown in Table 6 above, the sugar content of bokbunja vinegar was 10°Brix, and the acidity and pH were 5.05% and 3.32, respectively.
또한, 상기 제조예 1을 통해 제조된 복분자 식초의 색도를 측정하여 아래 표 7에 나타내었다.In addition, the chromaticity of the bokbunja vinegar prepared through Preparation Example 1 was measured and shown in Table 7 below.
<표 7><Table 7>
위에 표 7에 나타낸 것처럼, 복분자 식초의 명도 값을 나타내는 L 값은 24.49±0.09를 나타냈고 적색도인 a 값은 43.61±0.02를 나타냈으며 황색도 값인 b 값은 41.58±0.16을 나타내었다.As shown in Table 7 above, the L value representing the brightness value of bokbunja vinegar was 24.49±0.09, the redness a value was 43.61±0.02, and the yellowness value b was 41.58±0.16.
또한, 상기 제조예 1을 통해 제조된 복분자 식초의 아미노산을 분석하여 아래 표 8에 나타내었다.In addition, the amino acids of bokbunja vinegar prepared through Preparation Example 1 were analyzed and shown in Table 8 below.
<표 8><Table 8>
위에 표 8에 나타낸 것처럼, 아미노산 중 proline이 58.71 mg/L로 가장 높은 값을 나타내었고, 그 다음은 alanine으로 56.94 mg/L 순이었으며, histidine이 1.97 mg/L로 가장 낮은 값을 나타내었다.As shown in Table 8 above, proline among amino acids showed the highest value at 58.71 mg/L, followed by alanine in the order of 56.94 mg/L, and histidine at 1.97 mg/L, showing the lowest value.
또한, 상기 제조예 1을 통해 제조된 복분자 식초의 무기성분을 분석하여 아래 표 9에 나타내었다.In addition, the inorganic components of the bokbunja vinegar prepared through Preparation Example 1 were analyzed and shown in Table 9 below.
<표 9><Table 9>
위에 표 9에 나타낸 것처럼, 복분자 식초의 무기성분은 K가 1351.453 mg/L로 가장 높은 함량을 나타냈으며 Mg이 126.416 mg/L, Ca가 107.547 mg/L 순으로 높게 나타났다.As shown in Table 9 above, the inorganic component of bokbunja vinegar showed the highest content of K at 1351.453 mg/L, followed by 126.416 mg/L of Mg and 107.547 mg/L of Ca.
또한, 상기 제조예 1을 통해 제조된 복분자 식초의 유기산 성분을 분석하여 아래 표 10에 나타내었다.In addition, the organic acid component of bokbunja vinegar prepared through Preparation Example 1 was analyzed and shown in Table 10 below.
<표 10><Table 10>
위에 표 10에 나타낸 것처럼, 복분자 식초의 주요 유기산은 Acetic acid이었으며 그 함량은 38931.442 mg/L로 나타났다. 이어서 Citric acid, Lactic acid로 각각 1905.739 mg/L, 854.529 mg/L 로 높았으며 Malic acid가 231.095 mg/L로 가장 낮은 값을 나타냈다.As shown in Table 10 above, the main organic acid of bokbunja vinegar was Acetic acid, and its content was 38931.442 mg/L. Subsequently, citric acid and lactic acid were high at 1905.739 mg/L and 854.529 mg/L, respectively, and malic acid was the lowest at 231.095 mg/L.
또한, 상기 제조예 1을 통해 제조된 복분자 식초의 유리당 성분을 분석하여 아래 표 11에 나타내었다.In addition, the free sugar component of bokbunja vinegar prepared through Preparation Example 1 was analyzed and shown in Table 11 below.
<표 11><Table 11>
위에 표 11에 나타낸 것처럼, 복분자 식초의 주요 유리당 성분은 fructose 와 glucose로 나타났으며, 그 함량은 각각 7879.217와 6506.876mg/L이었다.As shown in Table 11 above, the main free sugar components of bokbunja vinegar were fructose and glucose, and the contents were 7879.217 and 6506.876mg/L, respectively.
<실시예 1><Example 1>
정제수 30g, 카놀라유 20g, 상기 제조예 1을 통해 제조된 복분자식초 10g, 설탕 11g, 올리고당 8, 양조식초 10g, 복분자 즙 4g, 겨자씨 3.9g, 소금 1.5g, 건조마늘 1g, 후추 0.5g, 잔탄검 0.1g을 균질기에 투입하고 30분 동안 균질화한 후에, 균질화된 혼합물을 살균기에 투입하고 100℃의 온도에서 60초 동안 살균하여 복분자 식초가 함유된 샐러드용 드레싱 조성물을 제조하였다.Purified water 30g, canola oil 20g, bokbunja vinegar 10g, sugar 11g, oligosaccharide 8, brewed vinegar 10g, bokbunja juice 4g, mustard seed 3.9g, salt 1.5g, dry garlic 1g, pepper 0.5g, xanthan gum After 0.1 g was added to a homogenizer and homogenized for 30 minutes, the homogenized mixture was put into a sterilizer and sterilized at a temperature of 100° C. for 60 seconds to prepare a salad dressing composition containing bokbunja vinegar.
상기 실시예 1을 통해 제조된 복분자 식초가 함유된 샐러드용 드레싱 조성물의 당도, 산도, pH를 측정하여 아래 표 12에 나타내었다.The sugar content, acidity, and pH of the salad dressing composition containing bokbunja vinegar prepared through Example 1 were measured and shown in Table 12 below.
단, 당도는 휴대용 당도계(Refractometer, PAL-1, Brix 0 to 53%, Atago, Japan)를 이용하여 시료 착즙액을 3회 반복 측정한 후 그 평균값으로 나타내었다.However, the sugar content was measured repeatedly 3 times using a portable sugar content meter (Refractometer, PAL-1, Brix 0 to 53%, Atago, Japan) and then expressed as the average value.
또한, 산도는 자동산도계(Easy pH, METTLER TOLEDO, Swizerland)를 이용하여 측정하고 3번 반복 측정하여 평균값으로 나타내었다.In addition, the acidity was measured using an automatic acidity meter (Easy pH, METTLER TOLEDO, Swizerland) and measured three times and expressed as an average value.
또한, pH 측정은 pH meter(SevenEasy, Mettler Toledo, Swiss)를 이용하여 3회 반복측정하였다. In addition, the pH measurement was repeated three times using a pH meter (SevenEasy, Mettler Toledo, Swiss).
<표 12><Table 12>
또한, 상기 실시예 1을 통해 제조된 복분자 식초가 함유된 샐러드용 드레싱 조성물의 점도를 측정하여 아래 표 13에 나타내었다.In addition, the viscosity of the salad dressing composition containing bokbunja vinegar prepared through Example 1 was measured and shown in Table 13 below.
단, 점도는 Viscometer (brookfield, LVDV Ⅱ, USA) 이용하여 100 rpm으로 spindle LV2룰 사용하여 상온에서 측정하였으며 spindel이 돌기 시작한 후 1분 정도 되는 순간의 점도를 cP(centi poise)단위로 읽었다. However, the viscosity was measured at room temperature using a spindle LV2 rule at 100 rpm using a Viscometer (brookfield, LVDV II, USA), and the viscosity at the moment about 1 minute after the spindel started to protrude was read in cP (centi poise) units.
<표 13><Table 13>
또한, 상기 실시예 1을 통해 제조된 복분자 식초가 함유된 샐러드용 드레싱 조성물의 색도를 측정하여 아래 표 14에 나타내었다.In addition, the chromaticity of the salad dressing composition containing bokbunja vinegar prepared through Example 1 was measured and shown in Table 14 below.
단, 색도는 분광색차계(CM-5, Minolta, Osaka, Japan)를 사용하여 L(Lightness), a(Redness), b(Yellowness) 값으로 표시하였으며, 각 시료를 3회 반복 측정하여 그 평균값을 나타내었다. However, chromaticity was expressed as L (Lightness), a (Redness), b (Yellowness) values using a spectrochromometer (CM-5, Minolta, Osaka, Japan), and the average value of each sample was measured three times. Shown.
<표 14><Table 14>
또한, 상기 실시예 1을 통해 제조된 복분자 식초가 함유된 샐러드용 드레싱 조성물의 영양성분을 분석하여 아래 표 15에 나타내었다.In addition, the nutritional components of the salad dressing composition containing bokbunja vinegar prepared through Example 1 were analyzed and shown in Table 15 below.
단, 영양성분 분석은 ㈜ 세스코 시험분석센터에 의뢰하여 분석하였다. 분석 내용으로는 9대 영양성분인 나트륨, 당류, 열량, 조단백질, 조지방, 콜레스테롤, 탄수화물, 트랜스지방 및 포화지방 항목을 분석하였다.However, the analysis of nutrients was conducted by requesting the CESCO Test Analysis Center. As for the analysis, the nine major nutrients such as sodium, sugar, calories, crude protein, crude fat, cholesterol, carbohydrates, trans fat and saturated fat were analyzed.
<표 15><Table 15>
위에 표 15에 나타낸 것처럼, 본 발명의 실시예 1을 통해 제조된 복분자 식초가 함유된 샐러드용 드레싱 조성물은 1회 제공량 100ml로 탄수화물은 영양소 기준치 7%, 당류는 18%, 단백질은 1%, 지방은 41%, 포화지방은 7% 및 나트륨은 36%를 나타냈다.As shown in Table 15 above, the salad dressing composition containing bokbunja vinegar prepared through Example 1 of the present invention is 100ml per serving, with 7% of the nutrient standard for carbohydrates, 18% for sugars, 1% for protein, and fat. Silver was 41%, saturated fat was 7% and sodium was 36%.
본 발명에 따른 복분자 식초가 함유된 샐러드용 드레싱 조성물은 복분자 식초가 함유되어 탄수화물, 유기산, 비타민 및 폴리페놀 등과 같은 영양성분이 풍부하며, 우수한 항산화효과를 나타낸다.The dressing composition for salads containing bokbunja vinegar according to the present invention contains bokbunja vinegar, rich in nutrients such as carbohydrates, organic acids, vitamins and polyphenols, and exhibits an excellent antioxidant effect.
Claims (6)
상기 복분자식초는,
복분자와 설탕을 혼합하여 당도가 24 brix가 되도록 혼합물을 제조한 후에, 상기 혼합물 100 중량부에 효모 1.0 중량부를 투입하고, 5℃에서 10일간 1차 발효한 후에, 고형분을 제거하고 효모 0.1 중량부를 추가로 투입하고 25℃에서 30일간 2차 발효하여 제조하며,
상기 조미료는,
겨자씨 12 내지 14 중량부, 소금 4.5 내지 5.5 중량부, 건조마늘 3 내지 3.5 중량부 및 후추 1 내지 2 중량부로 이루어지고,
상기 증점제는, 잔탄검으로 이루어지며,
상기 당혼합물은,
설탕과 올리고당이 1:0.7 내지 0.8 중량부로 혼합되어 이루어지는 복분자 식초가 함유된 샐러드용 드레싱 조성물.100 parts by weight of purified water, 60 to 70 parts by weight of canola oil, 30 to 35 parts by weight of bokbunja vinegar, 60 to 65 parts by weight of sugar mixture, 30 to 35 parts by weight of brewed vinegar, 10 to 15 parts by weight of bokbunja juice, 20 to 25 parts by weight of seasoning And 0.1 to 0.5 parts by weight of a thickener is added to a homogenizer, stirred to homogenize, and then the homogenized mixture is sterilized with a sterilizer at a temperature of 100° C. for 50 to 70 seconds,
The bokbunja vinegar,
After preparing a mixture so that the sugar content is 24 brix by mixing bokbun and sugar, 1.0 parts by weight of yeast was added to 100 parts by weight of the mixture, and after primary fermentation at 5° C. for 10 days, solids were removed and 0.1 parts by weight of yeast It is prepared by adding additionally and second fermentation at 25°C for 30 days,
The seasoning is,
12 to 14 parts by weight of mustard seeds, 4.5 to 5.5 parts by weight of salt, 3 to 3.5 parts by weight of dry garlic, and 1 to 2 parts by weight of pepper,
The thickener is made of xanthan gum,
The sugar mixture,
Salad dressing composition containing bokbunja vinegar made by mixing sugar and oligosaccharides in an amount of 1:0.7 to 0.8 parts by weight.
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