KR101496759B1 - Functional soap - Google Patents

Functional soap Download PDF

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Publication number
KR101496759B1
KR101496759B1 KR20130103732A KR20130103732A KR101496759B1 KR 101496759 B1 KR101496759 B1 KR 101496759B1 KR 20130103732 A KR20130103732 A KR 20130103732A KR 20130103732 A KR20130103732 A KR 20130103732A KR 101496759 B1 KR101496759 B1 KR 101496759B1
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soap
silver
purity
organic
germanium
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KR20130103732A
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Korean (ko)
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정구완
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나노폴리(주)
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/06—Inorganic compounds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/23—Sulfur; Selenium; Tellurium; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/10—Washing or bathing preparations
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B3/00—Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/38—Products in which the composition is not well defined
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/41—Particular ingredients further characterized by their size
    • A61K2800/413—Nanosized, i.e. having sizes below 100 nm

Abstract

The present invention relates to a functional soap, which comprises a nano-sized platinum, gold, silver, organic germanium, and organic selenium and which is manufactured by adding functions like antibiosis, sterilization, reducing stimulation on skin, and keeping moisture on skin of the platinum, gold, silver, organic germanium and organic selenium to the cleaning effect of an existing soap.

Description

기능성 비누{Functional soap}Functional soap {Functional soap}

본 발명은 비누에 관한 것으로서, 항균, 살균, 피부자극완화, 피부 보습기능을 갖는 비누에 관한 것이다.The present invention relates to a soap, and more particularly, to a soap having antibacterial, antiseptic, skin irritation, and skin moisturizing functions.

일반적으로 비누는 피부의 유지방 제거 및 피부의 노폐물을 제거하기 위해 사용된다.In general, soap is used to remove the milking water of the skin and to remove the waste matter of the skin.

기존의 비누는 피부의 동물성 오일 또는 식물성 오일을 주원료로 하여 만들어 진다. Conventional soaps are made mainly from animal or vegetable oils of the skin.

상기 기존의 비누는 피부의 유지방 및 노폐물을 제거하지만 피부에 발생한 트러블 및 피부에 존재하는 세균에 대한 항균, 살균, 피부자극완화 기능을 갖지 못한다. 또한 피부가 건조하거나 가려운 증상 또는 아토피 등의 증상으로 피부를 긁게 되면 피부는 더욱 거칠어지고 세균에 노출될 수 있다. 이 경우 일반 세정용 비누를 사용할 경우 피부질환에 도움을 주기가 쉽지 않다. 본 발명의 비누는 이러한 피부질환으로부터 오는 세균성 2차 감염을 예방하거나 완화시키는데 도움을 줄 수 있는 나노크기의 입자화된 유효 성분을 함유하는 기능성 비누를 제조하는 기술에 관한 것이다.Conventional soap does not have the functions of removing skin oil and waste products, but has trouble in skin and antibacterial, sterilizing, and skin irritation mitigation against germs present in the skin. In addition, when the skin is dry or itchy, or when the skin is scratched by symptoms such as atopy, the skin may become rougher and exposed to bacteria. In this case, general cleaning soap is not easy to help with skin diseases. The soaps of the present invention are directed to techniques for making functional soaps containing nanosized particulate active ingredients that can help prevent or mitigate bacterial secondary infections resulting from such skin conditions.

대한민국 특허출원 제90-4016호, 대한민국 특허출원 제99-6005호Korean Patent Application No. 90-4016, Korean Patent Application No. 99-6005

본 발명은 상기한 사정을 감안하여 창출된 것으로서, 비누를 사용하여 세안 또는 몸을 세정시 각종 세균으로부터 피부를 보호하고 항균, 살균, 피부자극완화, 피부 보습기능 갖는 나노크기의 입자화된 유효 성분을 함유하는 기능성 비누를 제공함에 기술적 목적이 있다.The present invention has been made in view of the above circumstances, and it is an object of the present invention to provide a nano-sized granular active ingredient having antibacterial, antiseptic, skin irritation alleviation and skin moisturizing function, which protects skin from various bacteria when cleansing or cleansing the body using soap To a functional soap.

본 발명의 실시 예에 따른 기능성 비누는 비누 원료에 나노입자 형성된 백금, 금, 은, 유기 게르마늄, 유기셀레늄이 함유된 것을 특징으로 한다.The functional soap according to the embodiment of the present invention is characterized in that the raw material for soap contains platinum, gold, silver, organic germanium, and organic selenium, which are formed of nanoparticles.

또한, 상기 백금은 순도 99.9%의 백금으로 그 입자 직경이 1-50nm이며 비누 원료에 0.2-10ppm 혼합되며, 상기 금은 순도 99.9%의 금으로 그 입자 직경이 1-9nm 크기이며 비누 원료에 0.5-20ppm 혼합되며, 상기 은은 순도 99.9%의 은으로 그 입자 직경이 1-9nm 크기이며 비누 원료에 0.5-20ppm 혼합되며, 상기 유기게르마늄은 순도 99.9%의 유기 게르마늄으로 그 입자 직경이 5-50nm이며 비누 원료에 0.1-10ppm 혼합되며, 상기 유기셀레늄은 순도 99.9%의 유기 셀레늄으로 그 입자 직경이 1-20nm 이며 비누 원료에 0.1-10ppm 혼합되는 것을 특징으로 한다.The platinum is platinum having a purity of 99.9%, and has a particle diameter of 1-50 nm and is mixed with 0.2-10 ppm of the raw material of the soap. The gold has a purity of 99.9%, its particle diameter is 1-9 nm, The silver is silver of 99.9% purity and has a particle diameter of 1-9 nm and is mixed with 0.5-20 ppm of the raw material of soap. The organic germanium is organic germanium having a purity of 99.9% and its particle diameter is 5-50 nm The organic selenium is organic selenium having a purity of 99.9%, its particle diameter is 1-20 nm, and the soap raw material is mixed with 0.1-10 ppm.

상기한 본 발명에 의하면 비누에 백금, 금, 은, 유기 셀레늄, 유기 게르마늄의 나노입자가 함유됨으로 인해 비누를 사용하여 세안 또는 세정시 항균, 살균, 피부자극완화, 피부 보습기능 갖는 기능성 비누를 제공할 수 있게 된다.According to the present invention, since the nanoparticles of platinum, gold, silver, organic selenium and organic germanium are contained in the soap, antibacterial, sterilizing, skin irritation mitigation and skin moisturizing functional soaps are provided when using soap .

도 1은 나노 백금입자의 TEM(전자현미경이미지) 사진이다.
도 2는 나노 금입자의 TEM(전자현미경이미지) 사진이다.
도 3은 나노 은입자의 TEM(전자현미경이미지) 사진이다.
도 4는 나노 유기 게르마늄 입자의 TEM(전자현미경이미지) 사진이다.
도 5는 나노 유기 셀레늄 입자의 TEM(전자현미경이미지) 사진이다.1 is a TEM (electron microscope image) photograph of nanoparticle particles.
2 is a TEM (electron microscope image) photograph of nano gold particles.
3 is a TEM (Electron Microscopic Image) photograph of nano silver particles.
4 is a TEM (electron micrograph) photograph of nanoparticulate germanium particles.
5 is a TEM (electron microscope image) photograph of nano-organic selenium particles.

이하, 본 발명에 따른 실시 예를 설명한다. 단, 이하에서 설명하는 실시 예는 본 발명에 대한 하나의 바람직한 구현 예를 예시적으로 나타낸 것으로서, 이러한 실시예의 예시는 본 발명의 권리범위를 제한하기 위한 것이 아니다. 본 발명은 그 기술적 사상을 벗어나지 않는 범위 내에서 다양하게 변형시켜 실시할 수 있다.Hereinafter, embodiments according to the present invention will be described. It should be noted, however, that the embodiments described below are illustrative of one preferred embodiment of the present invention, and examples of such embodiments are not intended to limit the scope of the present invention. The present invention can be variously modified without departing from the technical idea thereof.

본 발명에 따른 비누에 사용되는 주 원료는 코코넛 커넬과 오일 성분이며 여기에 나노입자가 혼합되고 일반적인 비누 보조 성분으로 호호바오일, 그레이프씨드오일 등이 보조제로 사용된다. 본 발명의 기능성 비누는 상기 일반적으로 사용되는 식물성 비누원료에 나노입자 크기의 백금(Platinum), 금(Gold), 은(Silver), 유기셀레늄(Organic Germanium), 유기게르마늄(Organic Selenium)이 첨가된다.The main raw materials used in the soap according to the present invention are a coconut kernel and an oil component, and nano particles are mixed therein, and jojoba oil, grape seed oil and the like are used as an auxiliary agent as a general soap auxiliary component. The functional soap of the present invention is prepared by adding nanoparticle-sized platinum, gold, silver, organic selenium, and organic germanium to the generally used vegetable soap raw material .

도 1은 나노 백금입자의 TEM(전자현미경이미지) 사진이다.1 is a TEM (electron microscope image) photograph of nanoparticle particles.

백금은 순도 99.9%의 백금으로 그 입자 크기가 1-50nm이며 비누 원료에 0.2-10ppm 혼합된다. 백금은 항균, 살균 및 냄새제거 효과가 있다.Platinum is a platinum with a purity of 99.9% and its particle size is 1-50nm and it is mixed with 0.2-10ppm in soap raw material. Platinum has antibacterial, sterilizing and deodorizing effects.

도 2는 나노 금입자의 TEM(전자현미경이미지) 사진이다.2 is a TEM (electron microscope image) photograph of nano gold particles.

금은 순도 99.9%의 금으로 그 입자 크기가 1-9nm이며 비누 원료에 0.5-20ppm 혼합된다. 금은 항균, 살균 및 안정효과가 있는 것으로 알려져 있다.Gold has a purity of 99.9%, its particle size is 1-9nm, and it is mixed with 0.5-20ppm in soap raw material. Gold is known to have antibacterial, antiseptic and stabilizing effects.

도 3은 나노 은입자의 TEM(전자현미경이미지) 사진이다.3 is a TEM (Electron Microscopic Image) photograph of nano silver particles.

은은 순도 순도 99.9%의 은으로 그 입자 크기가 1-9nm이며 비누 원료에 0.5-20ppm 혼합된다. 은은 살균, 항균, 항곰팡이 효과가 있다. 은은 인체에 무해하고 탁월한 살균효과를 가지며 내성이 없는 천연 항생제로 잘 알려져 있다. Silver is silver with a purity of 99.9% and its particle size is 1-9nm and it is mixed with 0.5-20ppm in soap raw material. Silver has sterilization, antibacterial and antifungal effects. Silver is known to be a natural antibiotic that is harmless to the human body and has excellent sterilizing effect and no resistance.

도 4는 나노유기게르마늄 입자의 TEM(전자현미경이미지) 사진이다.4 is a TEM (electron micrograph) photograph of nanoparticulate germanium particles.

유기게르마늄은 순도 99.9%의 유기 게르마늄으로 그 입자 크기가 5-50nm 이며 비누 원료에 0.1-10ppm 혼합된다. 유기 게르마늄은 피부 보습과 노화방지 및 면역성 향상의 기능이 있는 것으로 알려져 있다.Organic germanium is organic germanium with a purity of 99.9%, its particle size is 5-50nm and it is mixed with 0.1-10ppm in soap raw material. Organic germanium is known to have the function of moisturizing skin, preventing aging and improving immunity.

도 5는 나노 유기셀레늄 입자의 TEM(전자현미경이미지) 사진이다.5 is a TEM (electron microscope image) photograph of nano-organic selenium particles.

유기 셀레늄은 순도 99.9%의 유기 셀레늄으로 그 입자 크기가 1-20nm 이며 비누 원료에 0.1-10ppm 혼합된다. 유기 셀레늄은 항곰팡이 및 항상화 효과가 있다.Organic selenium is organic selenium with a purity of 99.9%, its particle size is 1-20nm and it is mixed with 0.1-10ppm in soap raw material. Organic selenium has antifungal and anti-inflammatory effects.

특히, 글루타치온-퍼옥시다제(Glutathione-Peroxidase)라는 효소를 생성케 하여 활성산소 즉 슈퍼옥사이드(Superoxide)로부터 세포를 보호하여 노화를 방지하는 항산화 작용이 비타민C의 2,000배가 있다고 알려져 있다. In particular, it is known that the antioxidant activity that protects cells from active oxygen, Superoxide, by making an enzyme called glutathione-peroxidase, is 2,000 times as much as vitamin C.

본 발명의 기능성 비누에는 나노입자 크기의 백금, 금, 은, 유기게르마늄, 유기셀레늄을 포함하여 구성되게 되며 기존의 비누의 세정효과에 백금, 금, 은, 유기 게르마늄, 유기셀레늄이 갖고 있는 항균, 살균, 피부자극완화, 피부 보습기능이 비누에 함께 추가된다.The functional soap of the present invention is composed of nanoparticles of platinum, gold, silver, organic germanium and organic selenium. The antibacterial and antimicrobial properties of the soap, which have platinum, gold, silver, organic germanium, Sterilization, skin irritation mitigation and skin moisturizing are added to the soap.

이하에서는 본 발명의 기능성 비누의 실시 예에 따른 혼합 비율을 표로 표시하였다.Hereinafter, the mixing ratios according to the examples of the functional soap of the present invention are tabulated.

Figure 112013079346535-pat00001
Figure 112013079346535-pat00001

표1 에 표시된 성분의 특성은 다음과 같다.The characteristics of the components shown in Table 1 are as follows.

비누 주 원료는 코코넛 성분이며, 호호바오일, 알로에추출물, 카모마일 오일, 토코페롤, 식물성스쿠알렌, 포도씨오일 등의 성분이 백금, 금, 은, 유기게르마늄, 유기셀레늄의 나노입자가 함께 혼합되어 일반 비누제조공정을 거쳐 고형 비누를 형성한다.The soap raw material is a coconut ingredient and the nano particles of platinum, gold, silver, organic germanium, and organic selenium are mixed together with ingredients such as jojoba oil, aloe extract, chamomile oil, tocopherol, vegetable squalane and grape seed oil, To form a solid soap.

이상으로 본 발명에 따른 실시 예를 설명하였다. 그러나, 본 발명은 상기한 적용 예로 한정되지는 않고 발명의 기술적 요지 및 요점을 이탈하지 않는 범위 내에서 다양한 변경 및 변형실시가 가능함은 물론이다.The embodiments according to the present invention have been described above. However, it should be understood that the present invention is not limited to the above-described embodiments, and various changes and modifications may be made without departing from the spirit and scope of the invention.

상기 기능성 비누에 대해 항균성 시험을 시행한 결과에 따르면, 항균성 시험에 적용되는 사용공시균주로는 MRSA (Methicillin Resistance S. aureus, 메티실린내성 황색포도상구균, ATCC 33592)를 사용하고 'KS M 0146' 시험방법에 적합하게 하여 1분 후 살균력 시험을 하여 결과를 얻었다. 시료는 비누를 100배 희석한 농도가 되게 1%를 사용하였다. 정균감소율(％)은 '(Ma-Mc) / Mb] x 100' 으로부터 구해지고, 증가율(F)은 'Mb/Ma'이며, Ma는 대조편의 접종 직후의 생균수이고, 접종균 농도 (CFU/㎖) (여기서 CFU는 Colony Forming Unit를 의미함)는 1.3 x 10^5, Ma 1.3 x 10^5, Mb 1.4 x 10^5, Mc < 10, 정균 감소율 99.9%의 살균력이 있는 시험결과를 얻었다. According to the result of the antibacterial test on the functional soap, MRSA (Methicillin Resistance S. aureus, methicillin-resistant Staphylococcus aureus, ATCC 33592) was used as the test strain to be used for the antibacterial test and 'KS M 0146' The sterilization test was carried out after 1 minute in accordance with the test method, and the result was obtained. The sample used was 1% so that the concentration of soap was 100 times diluted. Ma is the number of viable bacteria immediately after inoculation of the control piece, and the inoculum concentration (CFU (ml) / ml) / Ml), where CFU stands for Colony Forming Unit, is 1.3 x 10 ^ 5, Ma 1.3 x 10 ^ 5, Mb 1.4 x 10 ^ 5, Mc <10 and a bactericidal reduction rate of 99.9% .

상기한 시험결과로부터 알 수 있는 바와 같이, 본 발명에 따른 항균 기능의 나노 입자가 혼합된 비누로 우수한 항균성을 나타낼 수 있게 된다.As can be seen from the above test results, the antimicrobial nanoparticles according to the present invention can exhibit excellent antibacterial properties with soap mixed with them.

Claims (2)

비누 원료에 나노 크기의 백금, 금, 은, 유기게르마늄, 유기셀레늄이 함유되며, 상기 백금은 순도 99.9%, 입자크기 1-50nm, 혼합량이 0.2-10ppm이며, 상기 금은 순도 99.9%, 입자크기 1-9nm, 혼합량이 0.5-20ppm이며, 상기 은은 순도 99.9%, 입자크기 1-9nm, 혼합량이 0.5-20ppm이며, 상기 유기게르마늄은 순도 99.9%, 입자크기 5-50nm, 혼합량이 0.1-10ppm이며, 상기 유기셀레늄은 순도 99.9%, 입자크기 1-20nm, 혼합량이 0.1-10ppm 인 것을 특징으로 하는 비누에 있어서,
상기 비누 원료는 주원료로서 코코넛 커넬과 오일성분을 포함하며,
상기 주원료에 혼합되는 상기 백금, 금, 은, 유기게르마늄, 유기셀레늄의 나노입자를 포함하며,
상기 주원료에 혼합되는 나노입자에 보조제로서 혼합되는 호호바오일, 알로에추출물, 카모마일 오일, 토코페롤, 식물성스쿠알렌, 포도씨오일 성분을 포함하는 것을 특징으로 하는 비누.Wherein the raw material of the soap contains nano-sized platinum, gold, silver, organic germanium and organic selenium, the platinum has a purity of 99.9%, a particle size of 1-50 nm, a mixing amount of 0.2-10 ppm, a silver purity of 99.9% The silver germanium has a purity of 99.9%, a particle size of 5 to 50 nm, and a mixing amount of 0.1 to 10 ppm. The silver germanium has a purity of 99.9%, a particle size of 1-9 nm and a mixing amount of 0.5-20 ppm. , The organic selenium has a purity of 99.9%, a particle size of 1 to 20 nm, and a mixing amount of 0.1 to 10 ppm,
The soap raw material includes a coconut kernel and an oil component as main ingredients,
Gold, silver, organic germanium, or organic selenium mixed in the main raw material,
Characterized in that it contains Jojoba oil, aloe extract, chamomile oil, tocopherol, vegetable squalane and grape seed oil components which are mixed as an adjuvant in nanoparticles mixed with the above-mentioned raw materials. 삭제delete
KR20130103732A 2013-08-30 2013-08-30 Functional soap KR101496759B1 (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106963658A (en) * 2017-03-26 2017-07-21 广州市花安堂生物科技有限公司 A kind of cosmetic composition containing nanometer platinum
KR101966046B1 (en) * 2018-04-24 2019-08-13 금마유기공예 주식회사 method of manufacturing a silver, selenium bronze soap
KR102006167B1 (en) * 2018-04-24 2019-10-21 금마유기공예주식회사 Manufacturing method of bronze soap

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KR20080108714A (en) * 2007-06-11 2008-12-16 나노폴리(주) Manufactur method of wet-tissue with antimicrobial and anti-fungus function
KR20100019652A (en) * 2008-08-11 2010-02-19 서경대학교 산학협력단 Cleansing composition comprising nano-rized precious metals and method of producing the same

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20080108714A (en) * 2007-06-11 2008-12-16 나노폴리(주) Manufactur method of wet-tissue with antimicrobial and anti-fungus function
KR20100019652A (en) * 2008-08-11 2010-02-19 서경대학교 산학협력단 Cleansing composition comprising nano-rized precious metals and method of producing the same

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106963658A (en) * 2017-03-26 2017-07-21 广州市花安堂生物科技有限公司 A kind of cosmetic composition containing nanometer platinum
KR101966046B1 (en) * 2018-04-24 2019-08-13 금마유기공예 주식회사 method of manufacturing a silver, selenium bronze soap
KR102006167B1 (en) * 2018-04-24 2019-10-21 금마유기공예주식회사 Manufacturing method of bronze soap

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