KR101112783B1 - Germicide containing natural ingredients - Google Patents

Abstract

PURPOSE: An insecticidal composition containing natural ingredients is provided to void effect to human body, livestock, and environment and to enhance convenience. CONSTITUTION: An insecticidal composition contains 0.9-1.4 wt% of mineral, 7-13 wt% of sulfur, and remaining amount of water. The mineral includes 0.9-1.1 wt% of sulfur ion, 0.090-0.17 wt% of water soluble iron, 0.09-0.17 wt% of nitrogen, 0.005-0.015 wt% of water soluble magnesium, 0.0054-0.0076 wt% of water soluble potassium, 0.005-0.007 wt% of manganese, 0.003-0/005 wt% of sodium, 0.0005-0.0007 wt% of cobalt, 0.0003-0.0005 wt% of phosphorus, 0.0003-0.0005 wt% of zinc, and 0.00005-0.0002 wt% of water soluble phosphoric acid.

Description

Sterilizing composition containing natural ingredients {GERMICIDE CONTAINING NATURAL INGREDIENTS}

The present invention relates to a sterilizing composition, and more particularly to a sterilizing composition comprising a natural component.

In recent years, due to excessive use of chemical pesticides, environmental problems such as soil and water pollution, and ecosystem disturbance due to soil microorganisms and natural enemies are emerging as a major social issue. Chemical pesticides, which have been used for decades, are resistant to pests and can only be controlled by using more pesticides or more lethal pesticides over time. I'm making it. In addition, pesticide residues in crops are acting as a lethal hazard for humans who consume them.

Accordingly, researches on low-toxic, non-toxic and pollution-free biological pesticides to replace chemical pesticides are being actively conducted. Biological pesticides include microbial pesticides, biochemical pesticides and pesticides using natural enemies. Microbial pesticides are agricultural microbial control agents that use living microorganisms such as fungi, bacteria, viruses, and protozoa. Biochemical pesticides are used to extract and use natural compounds produced in nature, or agricultural biomaterials using non-toxic biological methods. Substance or herbal medicine. On the other hand, biochemical pesticides include natural pesticides composed of natural ingredients such as animals and plants, pheromones, enzymes, and minerals, and pesticides produced by plants by genes introduced into plants. Such biopesticides can be used as a substitute for chemical pesticides because they are non-residual and have no impact on humans and the environment. However, in the case of such environmentally friendly pesticides, the handling of raw materials is generally not easy, and the control value is lower than that of chemical pesticides, which impairs commercialization and limits generalization.

In addition, most biopesticides and natural pesticides are economically and ineffective due to their high price, and have a weak control effect or extremely limited effect, and the efficacy of the drug is not an immediate effect but a efficacious effect. It has not been well received and has not succeeded as a substitute for chemical pesticides to realize eco-friendly agriculture. Therefore, there is a demand for the development of a fungicide that is harmless to humans and plants and is environmentally friendly, easy to handle, low in production price, and high in controllability.

The present invention has been proposed to solve the above problems of the conventionally proposed methods, by using a material and active ionized minerals that can be easily extracted from soil and natural plants, while avoiding the impact on the stocking and environment It is an object of the present invention to provide a sterilizing composition comprising a natural component having high economical efficiency and convenience.

Another object of the present invention is to provide a sterilizing composition containing a natural component having high control effect and high practicality by producing a water-soluble solvent, sulfur and mineral in a specific ratio.

In addition, it is another object of the present invention to provide a sterilizing composition comprising natural ingredients, which can be rapidly absorbed into the interior of the plant by constructing it in an extremely small particle size.

Sterilizing composition comprising a natural component according to the characteristics of the present invention for achieving the above object,

Mineral 0.9-1.4 wt%;

7-13 weight percent sulfur; and

Including the residual amount of water is characterized by its configuration.

Preferably, the mineral is,

Sulfate, water soluble iron, nitrogen, water soluble earth, water soluble potassium, manganese, sodium, cobalt, phosphorus, zinc, water soluble phosphoric acid.

Preferably, the mineral is,

0.9 ~ 1.1 wt% sulfate sulfate, 0.09 ~ 0.17 wt% water soluble, 0.09 ~ 0.17 wt% nitrogen, 0.005 ~ 0.015 wt% water soluble earth, 0.0054 ~ 0.0076 wt% water soluble potassium, manganese 0.005 ~ 0.007 % By weight, sodium 0.003-0.005% by weight, cobalt 0.0005-0.0007, phosphorus 0.0003-0.0005% by weight, zinc 0.0003-0.0005% by weight, water-soluble phosphoric acid 0.00005-0.0002% by weight.

Preferably, the eco-friendly fungicide,

The particle size may be characterized by 1 to 4 nm.

Preferably,

It can be used to control at least one disease among powdery mildew and mildew.

According to the bactericidal composition comprising the natural component proposed in the present invention, using materials and active ionized minerals that can be easily extracted from the soil and natural plants, while not affecting the shrinkage and the environment, economical and convenience Can increase.

In addition, according to the present invention, by producing a water-soluble solvent, sulfur and minerals in a specific ratio, the control effect is high, the practicality can be improved.

In addition, according to the present invention, by configuring the micro particle size, it can be quickly absorbed into the interior of the plant.

1 is a view showing the composition ratio of the sterilizing composition comprising a natural component according to an embodiment of the present invention.
Figure 2 is a view showing a comparison of the results of using a sterilizing composition containing natural ingredients according to an embodiment of the present invention for powdery mildew control.
Figure 3 is a view showing a comparison of the results of using a bactericidal composition containing natural ingredients according to an embodiment of the present invention for powdery mildew disease control.

Hereinafter, exemplary embodiments of the present invention will be described in detail with reference to the accompanying drawings so that those skilled in the art may easily implement the present invention. However, in describing the preferred embodiment of the present invention in detail, if it is determined that the detailed description of the related known function or configuration may unnecessarily obscure the subject matter of the present invention, the detailed description thereof will be omitted. The same or similar reference numerals are used throughout the drawings for portions having similar functions and functions.

In addition, throughout the specification, when a part is 'connected' to another part, it is not only 'directly connected' but also 'indirectly connected' with another element in between. Include. In addition, the term 'comprising' of an element means that the element may further include other elements, not to exclude other elements unless specifically stated otherwise.

1 is a view showing the composition ratio of the sterilizing composition comprising a natural component according to an embodiment of the present invention. As shown in Figure 1, the sterilizing composition comprising a natural component according to an embodiment of the present invention, characterized in that it comprises 0.9 to 1.4% by weight of minerals, 7 to 13% by weight of sulfur, and water residual amount . In addition, the main component mineral in the sterilizing composition comprising a natural component according to an embodiment of the present invention, as shown in Figure 1, sulfate sulfate, water-soluble iron, nitrogen, water-soluble clay, water-soluble potassium, manganese, sodium , Cobalt, phosphorus, zinc, water soluble phosphoric acid.

Preferably, the composition ratio of the mineral which is the main component in the sterilizing composition comprising a natural component according to an embodiment of the present invention, 0.9 to 1.1% by weight sulfate, 0.09 to 0.17% by weight of water-soluble iron %, Nitrogen 0.09 ~ 0.17%, Water Soluble 0.005 ~ 0.015%, Potassium 0.0054 ~ 0.0076%, Manganese 0.005 ~ 0.007%, Sodium 0.003 ~ 0.005%, Cobalt 0.0005 ~ 0.0007, Phosphorus 0.0003 ~ 0.0005% , 0.0003 to 0.0005% by weight of zinc, 0.00005 to 0.0002% by weight of water-soluble phosphoric acid.

Sterilizing composition comprising a natural component according to an embodiment of the present invention, consisting of a substance and active ionized minerals extracted from a special soil and natural plants to maximize the expression of resistance to magnetic induction, to control pathogens. In addition, the main component of the composition for sterilization according to the embodiment proposed in the present invention is a substance of the combustion stream extracted from a natural plant, easily dissolved in water in the natural environment, and can be easily evaporated and decomposed by light. . It is therefore harmless to livestock and has no effect on bees, fish, algae, earthworms, soil microorganisms, and pest natural enemies. In addition, it has a high control effect comparable to chemical pesticides in the disinfection of harmful bacteria, reduces the residual components of chemical pesticides, and also serves as a plant nutrition source after use. In addition, useful components are coated on the leaf surface of the target plant can exhibit a continuous control effect. Preferably, the microparticle size of 1 to 4 nm can be rapidly absorbed into the interior of the plant to exhibit a fast pesticide effect.

In addition, the sterilizing composition comprising a natural component according to an embodiment of the present invention, the chelate iron hydrate, titanium, sulfur ions may be the main component. Sterilizing composition according to an embodiment proposed in the present invention, it is possible to increase the biological activity effect by the action of repeatedly producing ATP, to impair the energy metabolism and electron transfer system to destroy the habitat environment of germs. In particular, there is a control effect on anthrax, which is a disease that is difficult to cure even with chemical pesticides, by using the sterilizing composition according to an embodiment proposed in the present invention, it is possible to normal harvest by purifying the soil so that roots can grow normally You can switch to the state.

The main component of the sterilizing composition according to the embodiment proposed by the present invention does not contain an EPA (Environmental Protection Agency, US Environmental Protection Agency) regulatory substance, and because there is no chemical pesticide component, no residual pesticide is detected. With respect to the sterilizing composition comprising a natural component according to an embodiment of the present invention, it was examined whether the harmful components of the residual pesticides mainly detected in plants using chemical pesticides. As a result, 250 components such as Acetamiprid, Benalaxyl, Bitertanol, Diazinon, Fludioxonil, Parathion, Simazine, Thiamethoxam, and Zoxamide were not detected.

Toxicity test for the sterilizing composition comprising a natural component according to an embodiment of the present invention. Toxicity tests were performed in three ways: acute oral toxicity test, acute transdermal toxicity test, and acute fish toxicity test for carp. Hereinafter, the results of testing the toxicity of the sterilizing composition comprising a natural component according to an embodiment of the present invention.

Experimental Example 1

In the acute oral toxicity test method, mice (ICR system) were published and orally administered once, and then 14 days of mortality, general poisoning symptoms, weight change, and autopsy findings were examined. The number of published animals per dose level was 10 males and 5 males and 5 males, respectively, and forced administration was performed only once in the stomach by oral route of administration using an oral injection needle for mice.

Table 1 to Table 4, as a result of acute oral toxicity test of the sterilizing composition comprising a natural component according to an embodiment of the present invention, Table 1 is the lethal number, Table 2 is a general poisoning symptoms, Table 3 is the weight change, Table 4 shows the results of autopsy findings. As can be seen from Tables 1 to 4, at the dosages of 525, 683, 887, 1153, 1499, 1949 mg / kg, males are 0, 1, 2, 2, 3, 5, females are 0, 2 , 3, 4, 4 and 5 were killed, and the acute oral toxicity LD50 value was 985.7 mg / kg (95% confidence limit: 818.5-1181.3 mg / kg) in both males and females. Convulsions and postural abnormalities were observed as symptoms of general intoxication, and body weight changes decreased from day 1 to day 1 in both males and females according to the days after drug administration. The animals were autopsied 14 days after treatment and visually inspected for internal organ abnormalities, but no abnormalities were observed in all organs. The sterilizing composition according to an embodiment of the present invention had no effect on each organ, and was classified as Class IV (low toxicity) based on the pesticide management method.

Experimental Example 2

In the acute transdermal toxicity test method, rats (SD system) were disclosed and observed for 14 days after one drug treatment, and the number of deaths, general poisoning symptoms, weight change, and autopsy findings were examined. The number of test animals per drug dose was set to 10 groups of 5 males and 5 females, and the amount of treatment fluid was set to 5.0 ml / kg (weight) for each dose level. Was applied.

Table 5 to Table 8, as a result of the acute transdermal toxicity test of the sterilizing composition comprising a natural component according to an embodiment of the present invention, Table 5 is a lethal number, Table 6 is a general poisoning symptoms, Table 7 is a weight change, Table 8 shows the results of autopsy findings. As can be seen from Tables 5 to 8, there were no lethal animals at 4000 mg / kg, the dose level of the baseline test. Erythema was observed as a general poisoning symptom, and body weight after the administration of drugs decreased until day 1 in both sexes, but recovered from day 3 and increased. Autopsy findings showed no specific symptoms at the dose of 4000 mg / kg. The bactericidal composition according to one embodiment of the present invention has no effect on each organ, and is classified as Class IV (low toxicity) when the toxicity is classified according to the pesticide control method.

[Experimental Example 3]

In the acute percutaneous toxicity test method, the carp (Cyprinus Carpio) was disclosed and exposed to the sterilizing composition containing a natural component according to an embodiment of the present invention for 96 hours to investigate the cumulative mortality. The number of test fish was put into two groups of 10 l water tanks, 5 in total and 10 in total. Group 1 was treated with untreated groundwater as a negative control.

Table 9 shows the results of the acute transdermal toxicity test of the bactericidal composition containing natural ingredients according to an embodiment of the present invention. As can be seen from Table 9, the 96 hour half lethal concentration (LD50) is 10 mg. / l or more. Sterilizing composition according to an embodiment of the present invention was classified into class III by classifying fish toxicity according to the degree of toxicity according to the pesticide control method.

In addition, the sterilization composition comprising a natural component according to an embodiment of the present invention, the problem due to weakness does not occur. Hereinafter, through the Experimental Example 4, it will be described whether the weakening of the composition for sterilization comprising a natural component according to an embodiment of the present invention.

[Experimental Example 4]

After sterilizing the composition for sterilizing the composition containing natural ingredients according to an embodiment of the present invention to melon and strawberry (sulfur) in a standard amount and a pear, after 24 hours to investigate the growth disorder and the occurrence of damage symptoms.

Table 10 is a result of comparing and inspecting the presence or absence of the harmful treatment of the treatment treatment treated with a sterilizing composition comprising a natural component according to an embodiment of the present invention and the water treated untreated. As can be seen from Table 10, no damage occurred even in the batch treatment.

Trial crop Weakness Remarks Non-treatment Reference Treatment Displacement Treatment melon 0 0 0 No weakness Strawberry (Snow) 0 0 0 No weakness

On the other hand, the sterilizing composition comprising a natural component according to an embodiment of the present invention, is particularly effective in controlling diseases such as powdery mildew, mold, anthrax, late blight, mango disease, blasting, aptitude, blackness, stomach disease. Hereinafter, the results of experimenting with the effect of the sterilizing composition comprising natural ingredients according to an embodiment of the present invention will be examined.

[Experimental Example 5]

The effect of powdery mildew on the melon of the sterilizing composition comprising a natural component according to an embodiment of the present invention was tested. The experimental method was divided into a total of three treatment groups of the recommendation sphere treated with the standard amount, the drainage treated drainage ball, and the untreated water treated water treatment composition including the sterilizing composition including natural ingredients according to an embodiment of the present invention. The experiment was repeated three times in total.

Table 11 and Table 12 are the results of experiments on powdery mildew control effect on the melon of the composition for sterilization according to an embodiment of the present invention. Table 11 shows the results of investigation of the control value after the two treatments of the composition for sterilization according to one embodiment of the present invention in June (primary packaging), and Table 12 is according to one embodiment of the present invention in July. It is the result of investigating the control value after two treatments of the composition for sterilization (secondary packaging). As can be seen in Table 11 and Table 12, the sterilizing composition according to an embodiment of the present invention, on average, showed an excellent control value of more than 80%.

Treatment Disease Incidence (%) Control price (%) 1 repetition 2 repetitions 3 repetitions Average Non-treatment 78.4 75.1 89.4 80.97 - Recommended phrase 15.4 10.7 15.7 13.94 86.06 Drain 17.4 13.5 12.4 14.43 85.57

Treatment Disease Incidence (%) Control price (%) 1 repetition 2 repetitions 3 repetitions Average Non-treatment 82.9 91.5 71.8 82.07 - Recommended phrase 22.7 19.7 25.1 22.5 77.5 Drain 20.8 18.7 23.4 20.97 79.03

Experimental Example 6

The control effect of ash fungus disease on the strawberry (Shanghyang) of the bactericidal composition comprising natural ingredients according to an embodiment of the present invention was tested. Experimental method was repeated three times by the egg mass method, the total amount of the recommendation treatment, the amount of the treated amount, and the water-treated untreated sphere treated with a standard amount of the sterilizing composition comprising a natural component according to an embodiment of the present invention The treatment was divided into three treatment groups, and the leaves were treated four times at two week intervals.

Table 13 and Table 14, the results of the experiment to control the ash fungus disease control effect on the strawberry of the composition for sterilization according to an embodiment of the present invention. Table 13 is a result of examining the first control value after treating the sterilizing composition according to an embodiment of the present invention two times at intervals of two weeks, Table 14 is after the first control value was investigated again one embodiment of the present invention After treating the sterilizing composition according to the example twice at intervals of two weeks, the secondary control value was investigated. As can be seen in Table 13 and Table 14, the sterilizing composition according to an embodiment of the present invention, on average, showed an excellent control value of 80%.

Treatment Disease Incidence (%) Control price (%) 1 repetition 2 repetitions 3 repetitions Average Non-treatment 53.5 67.1 50.9 57.17 - Recommended phrase 16.13 13.02 15.66 14.94 85.06 Drain 15.12 14.56 17.21 15.63 84.37

Treatment Disease Incidence (%) Control price (%) 1 repetition 2 repetitions 3 repetitions Average Non-treatment 68.4 80.25 70.58 73.08 - Recommended phrase 20.78 28.97 22.85 24.2 75.8 Drain 26.13 23.3 19.7 23.04 76.96

Figure 2 is a view showing a comparison of the results of using a sterilizing composition containing a natural component for controlling fungal diseases according to an embodiment of the present invention. We compared the strawberry (salt) treated with a standard amount of the sterilizing composition containing natural ingredients according to an embodiment of the present invention, and whether the gray mold fungal disease of the strawberry treated with water. As a result, as can be seen in Figure 2, the occurrence of gray mold in the strawberry treated with the sterilizing composition according to an embodiment of the present invention significantly reduced.

Figure 3 is a view showing a comparison of the results of using a sterilizing composition containing natural ingredients according to an embodiment of the present invention for powdery mildew disease control. In the case of spraying foliar with a sterilizing composition comprising natural ingredients according to an embodiment of the present invention and when not otherwise compared to the control effect of powdery mildew, mildew disease. As a result, as can be seen in Figure 3, after treating the sterilizing composition comprising a natural component according to an embodiment of the present invention, powder powder and mildew disease significantly reduced.

Sterilizing composition comprising a natural component according to an embodiment of the present invention, a dark brown liquid and has a unique smell, specific gravity of 1.05 ~ 1.20, pH may be 9.5 ~ 11. Examining an example of the use of the sterilizing composition comprising a natural component according to an embodiment of the present invention, before or after the occurrence of the disease, 400-500-fold dilution can be evenly sprayed on the target plant leaf surface.

The present invention described above may be variously modified or applied by those skilled in the art, and the scope of the technical idea according to the present invention should be defined by the following claims.

Claims (5)

Mineral 0.9-1.4 wt%;
Sulfur 7-13 weight percent; And
Includes the remaining water,
The mineral is,
Contains sulfate, water soluble iron, nitrogen, water soluble earth, water soluble potassium, manganese, sodium, cobalt, phosphorus, zinc, water soluble phosphoric acid,
A sterilizing composition comprising a natural component, characterized by having a particle size of 1 to 4 nm.
delete The method of claim 1, wherein the mineral,
0.9 ~ 1.1 wt% sulfate sulfate, 0.09 ~ 0.17 wt% water soluble, 0.09 ~ 0.17 wt% nitrogen, 0.005 ~ 0.015 wt% water soluble earth, 0.0054 ~ 0.0076 wt% water soluble potassium, manganese 0.005 ~ 0.007 Sterilizing composition comprising natural ingredients, characterized in that the weight percent, sodium 0.003-0.005 weight percent, cobalt 0.0005-0.0007, phosphorus 0.0003-0.0005 weight percent, zinc 0.0003-0.0005 weight percent, water-soluble phosphoric acid 0.00005-0.0002 weight percent .
delete The method of claim 1,
A sterilizing composition comprising natural ingredients, characterized in that it is used to control at least one disease among powdery mildew and mildew.

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