KR100756310B1 - 입자형 다결정실리콘 제조용 고압 유동층반응기 - Google Patents

입자형 다결정실리콘 제조용 고압 유동층반응기 Download PDF

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Publication number
KR100756310B1
KR100756310B1 KR1020060011493A KR20060011493A KR100756310B1 KR 100756310 B1 KR100756310 B1 KR 100756310B1 KR 1020060011493 A KR1020060011493 A KR 1020060011493A KR 20060011493 A KR20060011493 A KR 20060011493A KR 100756310 B1 KR100756310 B1 KR 100756310B1
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KR
South Korea
Prior art keywords
pressure
fluidized bed
silicon
bed reactor
gas
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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KR1020060011493A
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English (en)
Korean (ko)
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KR20070080306A (ko
Inventor
김희영
윤경구
박용기
최원춘
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한국화학연구원
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Priority to KR1020060011493A priority Critical patent/KR100756310B1/ko
Application filed by 한국화학연구원 filed Critical 한국화학연구원
Priority to US12/093,513 priority patent/US7972562B2/en
Priority to EP07708807.8A priority patent/EP1984297B1/en
Priority to RU2008132506/15A priority patent/RU2397952C2/ru
Priority to PCT/KR2007/000657 priority patent/WO2007091834A1/en
Priority to ES07708807.8T priority patent/ES2436770T3/es
Priority to CN2007800044671A priority patent/CN101378989B/zh
Priority to JP2008554132A priority patent/JP4955706B2/ja
Publication of KR20070080306A publication Critical patent/KR20070080306A/ko
Application granted granted Critical
Publication of KR100756310B1 publication Critical patent/KR100756310B1/ko
Priority to US12/609,364 priority patent/US8114352B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A47FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
    • A47JKITCHEN EQUIPMENT; COFFEE MILLS; SPICE MILLS; APPARATUS FOR MAKING BEVERAGES
    • A47J37/00Baking; Roasting; Grilling; Frying
    • A47J37/06Roasters; Grills; Sandwich grills
    • A47J37/067Horizontally disposed broiling griddles
    • A47J37/0682Horizontally disposed broiling griddles gas-heated
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/02Silicon
    • C01B33/021Preparation
    • C01B33/027Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/04Pressure vessels, e.g. autoclaves
    • B01J3/046Pressure-balanced vessels
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1818Feeding of the fluidising gas
    • B01J8/1827Feeding of the fluidising gas the fluidising gas being a reactant
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1836Heating and cooling the reactor
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/02Silicon
    • C01B33/021Preparation
    • C01B33/027Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material
    • C01B33/029Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material by decomposition of monosilane
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/02Silicon
    • C01B33/021Preparation
    • C01B33/027Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material
    • C01B33/03Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material by decomposition of silicon halides or halosilanes or reduction thereof with hydrogen as the only reducing agent
    • AHUMAN NECESSITIES
    • A47FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
    • A47JKITCHEN EQUIPMENT; COFFEE MILLS; SPICE MILLS; APPARATUS FOR MAKING BEVERAGES
    • A47J37/00Baking; Roasting; Grilling; Frying
    • A47J37/06Roasters; Grills; Sandwich grills
    • A47J37/07Roasting devices for outdoor use; Barbecues
    • A47J37/0786Accessories
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00389Controlling the temperature using electric heating or cooling elements
    • B01J2208/00398Controlling the temperature using electric heating or cooling elements inside the reactor bed
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00389Controlling the temperature using electric heating or cooling elements
    • B01J2208/00407Controlling the temperature using electric heating or cooling elements outside the reactor bed

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Food Science & Technology (AREA)
  • Silicon Compounds (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
KR1020060011493A 2006-02-07 2006-02-07 입자형 다결정실리콘 제조용 고압 유동층반응기 Expired - Fee Related KR100756310B1 (ko)

Priority Applications (9)

Application Number Priority Date Filing Date Title
KR1020060011493A KR100756310B1 (ko) 2006-02-07 2006-02-07 입자형 다결정실리콘 제조용 고압 유동층반응기
EP07708807.8A EP1984297B1 (en) 2006-02-07 2007-02-07 High-pressure fluidized bed reactor for preparing granular polycrystalline silicon
RU2008132506/15A RU2397952C2 (ru) 2006-02-07 2007-02-07 Реактор высокого давления с псевдоожиженным слоем для получения гранулированного поликристаллического кремния
PCT/KR2007/000657 WO2007091834A1 (en) 2006-02-07 2007-02-07 High-pressure fluidized bed reactor for preparing granular polycrystalline silicon
US12/093,513 US7972562B2 (en) 2006-02-07 2007-02-07 High-pressure fluidized bed reactor for preparing granular polycrystalline silicon
ES07708807.8T ES2436770T3 (es) 2006-02-07 2007-02-07 Reactor de lecho fluidizado de alta presión para preparar silicio policristalino granular
CN2007800044671A CN101378989B (zh) 2006-02-07 2007-02-07 用于制备粒状多晶硅的高压流化床反应器
JP2008554132A JP4955706B2 (ja) 2006-02-07 2007-02-07 粒状多結晶シリコン製造用流動層反応器
US12/609,364 US8114352B2 (en) 2006-02-07 2009-10-30 High-pressure fluidized bed reactor for preparing granular polycrystalline silicon

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR1020060011493A KR100756310B1 (ko) 2006-02-07 2006-02-07 입자형 다결정실리콘 제조용 고압 유동층반응기

Publications (2)

Publication Number Publication Date
KR20070080306A KR20070080306A (ko) 2007-08-10
KR100756310B1 true KR100756310B1 (ko) 2007-09-07

Family

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Family Applications (1)

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KR1020060011493A Expired - Fee Related KR100756310B1 (ko) 2006-02-07 2006-02-07 입자형 다결정실리콘 제조용 고압 유동층반응기

Country Status (8)

Country Link
US (2) US7972562B2 (https=)
EP (1) EP1984297B1 (https=)
JP (1) JP4955706B2 (https=)
KR (1) KR100756310B1 (https=)
CN (1) CN101378989B (https=)
ES (1) ES2436770T3 (https=)
RU (1) RU2397952C2 (https=)
WO (1) WO2007091834A1 (https=)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20130053693A (ko) * 2011-11-16 2013-05-24 주식회사 실리콘밸류 유동층 반응기
US8580203B2 (en) 2010-10-01 2013-11-12 Siliconvalue Llc Fluidized bed reactor
US8580204B2 (en) 2011-04-20 2013-11-12 Siliconvalue Llc Fluidized bed reactor
KR101329032B1 (ko) * 2011-04-20 2013-11-14 주식회사 실리콘밸류 다결정 실리콘 제조장치 및 이를 이용한 다결정 실리콘의 제조방법
KR101329033B1 (ko) * 2011-04-20 2013-11-14 주식회사 실리콘밸류 유동층 반응기
KR101356391B1 (ko) * 2011-04-20 2014-02-03 주식회사 실리콘밸류 다결정 실리콘 제조장치
US10569247B1 (en) 2019-03-11 2020-02-25 Korea Institute Of Energy Research Installation and operation method of dual control valves in a high pressure fluidized bed system
KR20220047967A (ko) * 2019-06-26 2022-04-19 엑스-에너지 엘엘씨 진행 반응 중에 입자 샘플링을 허용하는 유동화 베드 반응기 시스템

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KR100756310B1 (ko) * 2006-02-07 2007-09-07 한국화학연구원 입자형 다결정실리콘 제조용 고압 유동층반응기
KR100783667B1 (ko) * 2006-08-10 2007-12-07 한국화학연구원 입자형 다결정 실리콘의 제조방법 및 제조장치
DE102007021003A1 (de) 2007-05-04 2008-11-06 Wacker Chemie Ag Verfahren zur kontinuierlichen Herstellung von polykristallinem hochreinen Siliciumgranulat
US8790782B2 (en) * 2008-07-02 2014-07-29 E I Du Pont De Nemours And Company Method for making glass frit powders using aerosol decomposition
CN101318654B (zh) * 2008-07-04 2010-06-02 清华大学 一种流化床制备高纯度多晶硅颗粒的方法及流化床反应器
CN103058194B (zh) 2008-09-16 2015-02-25 储晞 生产高纯颗粒硅的反应器
DE102009043947B4 (de) 2009-09-04 2011-07-07 G+R Technology Group AG, 93128 Anlage zur Herstellung von polykristallinem Silizium mit Vorrichtung zum Ausleiten gasförmiger Messproben
US9023425B2 (en) 2009-11-18 2015-05-05 Rec Silicon Inc Fluid bed reactor
JP5637013B2 (ja) * 2010-03-04 2014-12-10 三菱マテリアル株式会社 トリクロロシラン製造装置及び製造方法
US8404199B2 (en) 2010-08-06 2013-03-26 Empire Technology Development Llc Fluorine based vanadium boride nanoparticle synthesis
KR101057101B1 (ko) * 2010-10-12 2011-08-17 (주)기술과가치 입자형 다결정실리콘 제조용 유동층 반응기 및 이를 이용한 다결정 실리콘 제조방법
US20120100061A1 (en) 2010-10-22 2012-04-26 Memc Electronic Materials, Inc. Production of Polycrystalline Silicon in Substantially Closed-loop Processes
US8449848B2 (en) 2010-10-22 2013-05-28 Memc Electronic Materials, Inc. Production of polycrystalline silicon in substantially closed-loop systems
US9156705B2 (en) 2010-12-23 2015-10-13 Sunedison, Inc. Production of polycrystalline silicon by the thermal decomposition of dichlorosilane in a fluidized bed reactor
US8849584B2 (en) * 2010-12-29 2014-09-30 Sunedison, Inc. Systems and methods for particle size determination and control in a fluidized bed reactor for use with thermally decomposable silicon-containing gas
US8452547B2 (en) 2010-12-29 2013-05-28 Memc Electronic Materials, Inc. Systems and methods for particle size determination and control in a fluidized bed reactor
US20120183686A1 (en) * 2011-01-19 2012-07-19 Rec Silicon Inc. Reactor system and method of polycrystalline silicon production therewith
US20130129570A1 (en) * 2011-04-20 2013-05-23 Siliconvalue Llc. Polycrystal silicon manufacturing apparatus
TW201304864A (zh) * 2011-06-10 2013-02-01 Rec Silicon Inc 高純度矽塗佈顆粒之製造
JP5897851B2 (ja) * 2011-09-12 2016-04-06 東洋炭素株式会社 粉体処理装置および粉体処理方法
WO2013049325A1 (en) 2011-09-30 2013-04-04 Memc Electronic Materials, Inc. Production of polycrystalline silicon by the thermal decomposition of silane in a fluidized bed reactor
WO2013049314A2 (en) 2011-09-30 2013-04-04 Memc Electronic Materials, Inc. Production of polycrystalline silicon by the thermal decomposition of silane in a fluidized bed reactor
KR101432896B1 (ko) * 2012-10-29 2014-08-21 웅진에너지 주식회사 폴리실리콘 제조용 유동층 반응기
US9212421B2 (en) 2013-07-10 2015-12-15 Rec Silicon Inc Method and apparatus to reduce contamination of particles in a fluidized bed reactor
US9587993B2 (en) 2012-11-06 2017-03-07 Rec Silicon Inc Probe assembly for a fluid bed reactor
KR20150082349A (ko) * 2012-11-06 2015-07-15 알이씨 실리콘 인코포레이티드 유동상 반응기 내의 입자들의 오염을 감소시키는 방법 및 장치
WO2014099502A1 (en) * 2012-12-21 2014-06-26 Rec Silicon Inc High-temperature grade steel for fluidized bed reactor equipment
CN107364869A (zh) * 2013-04-16 2017-11-21 江苏中能硅业科技发展有限公司 流化床反应器及其用于制备高纯粒状多晶硅的方法
CN103449442B (zh) * 2013-09-03 2015-03-18 浙江精功新材料技术有限公司 一种流化床多晶硅颗粒的制备系统及利用该系统制备多晶硅的工艺
US20150104369A1 (en) * 2013-10-11 2015-04-16 Rec Silicon Inc Polysilicon transportation device and a reactor system and method of polycrystalline silicon production therewith
DE102014212049A1 (de) 2014-06-24 2015-12-24 Wacker Chemie Ag Wirbelschichtreaktor und Verfahren zur Herstellung von polykristallinem Siliciumgranulat
US9446367B2 (en) * 2014-08-15 2016-09-20 Rec Silicon Inc Joint design for segmented silicon carbide liner in a fluidized bed reactor
US9238211B1 (en) * 2014-08-15 2016-01-19 Rec Silicon Inc Segmented silicon carbide liner
US9662628B2 (en) 2014-08-15 2017-05-30 Rec Silicon Inc Non-contaminating bonding material for segmented silicon carbide liner in a fluidized bed reactor
DE102014221928A1 (de) * 2014-10-28 2016-04-28 Wacker Chemie Ag Wirbelschichtreaktor und Verfahren zur Herstellung von polykristallinem Siliciumgranulat
KR20170101985A (ko) * 2014-12-31 2017-09-06 알이씨 실리콘 인코포레이티드 하부 밀봉 장치를 갖는 실리콘 증착 반응기
US10837106B2 (en) 2015-05-12 2020-11-17 Corner Star Limited Clamping assembly for a reactor system
DE102015224120A1 (de) * 2015-12-02 2017-06-08 Wacker Chemie Ag Wirbelschichtreaktor und Verfahren zur Herstellung von polykristallinem Siliciumgranulat
RU2691344C1 (ru) * 2018-09-10 2019-06-11 Вадим Георгиевич Кузьмин Способ очистки зерен кварца и зерно кварца, полученное согласно способу
FR3112148B1 (fr) 2020-07-01 2022-07-15 Safran Ceram Dispositif pour le dépôt chimique en phase vapeur en lit fluidisé
CN115078450A (zh) * 2021-03-11 2022-09-20 中国科学院过程工程研究所 一种热转化反应的分析装置及其分析方法
CN113501794A (zh) * 2021-07-28 2021-10-15 南京硕达生物科技有限公司 一种2-氨基-5-巯基-1,3,4-噻二唑的制备方法
CN115007066A (zh) * 2022-08-05 2022-09-06 山西阳煤化工机械(集团)有限公司 一种冷氢化反应器
KR102712596B1 (ko) * 2022-08-29 2024-09-30 오씨아이 주식회사 실리콘 마이크로 입자의 제조방법 및 이에 의해 제조된 실리콘 마이크로 입자

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JP2001214271A (ja) 2000-01-31 2001-08-07 Seiko Epson Corp 成膜装置
KR20020059172A (ko) * 2001-01-03 2002-07-12 김충섭 다결정실리콘의 제조방법과 그 장치

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8580203B2 (en) 2010-10-01 2013-11-12 Siliconvalue Llc Fluidized bed reactor
KR101329030B1 (ko) * 2010-10-01 2013-11-13 주식회사 실리콘밸류 유동층 반응기
US8580204B2 (en) 2011-04-20 2013-11-12 Siliconvalue Llc Fluidized bed reactor
KR101329035B1 (ko) 2011-04-20 2013-11-13 주식회사 실리콘밸류 유동층 반응기
KR101329032B1 (ko) * 2011-04-20 2013-11-14 주식회사 실리콘밸류 다결정 실리콘 제조장치 및 이를 이용한 다결정 실리콘의 제조방법
KR101329033B1 (ko) * 2011-04-20 2013-11-14 주식회사 실리콘밸류 유동층 반응기
KR101356391B1 (ko) * 2011-04-20 2014-02-03 주식회사 실리콘밸류 다결정 실리콘 제조장치
KR20130053693A (ko) * 2011-11-16 2013-05-24 주식회사 실리콘밸류 유동층 반응기
US10569247B1 (en) 2019-03-11 2020-02-25 Korea Institute Of Energy Research Installation and operation method of dual control valves in a high pressure fluidized bed system
KR20220047967A (ko) * 2019-06-26 2022-04-19 엑스-에너지 엘엘씨 진행 반응 중에 입자 샘플링을 허용하는 유동화 베드 반응기 시스템
KR102419304B1 (ko) 2019-06-26 2022-07-11 엑스 에너지, 엘엘씨 진행 반응 중에 입자 샘플링을 허용하는 유동화 베드 반응기 시스템

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RU2397952C2 (ru) 2010-08-27
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JP4955706B2 (ja) 2012-06-20
CN101378989B (zh) 2012-09-05
US20080267834A1 (en) 2008-10-30
WO2007091834A1 (en) 2007-08-16
US20100047136A1 (en) 2010-02-25
EP1984297A1 (en) 2008-10-29
EP1984297A4 (en) 2012-10-10
RU2008132506A (ru) 2010-02-20
US7972562B2 (en) 2011-07-05
US8114352B2 (en) 2012-02-14
JP2009525937A (ja) 2009-07-16
KR20070080306A (ko) 2007-08-10
EP1984297B1 (en) 2013-10-30

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