KR100692969B1 - The manufacture method of the organic liquid fertilizer having functions - Google Patents
The manufacture method of the organic liquid fertilizer having functions Download PDFInfo
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- KR100692969B1 KR100692969B1 KR1020050043962A KR20050043962A KR100692969B1 KR 100692969 B1 KR100692969 B1 KR 100692969B1 KR 1020050043962 A KR1020050043962 A KR 1020050043962A KR 20050043962 A KR20050043962 A KR 20050043962A KR 100692969 B1 KR100692969 B1 KR 100692969B1
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F11/00—Other organic fertilisers
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
- C05D9/02—Other inorganic fertilisers containing trace elements
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
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- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
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Abstract
본 발명은 당류를 모재로 하여 키토산과 아미노산을 사용하여 만든 유기질 액체비료에 나노 규산염과 나노 셀레늄을 혼합시켜 기능성 유기질 액체비료를 제조하는 것으로써, 본 발명에 따라 제조되는 기능성 유기질 액체비료는 규산염이 인산(P)의 역할을 대신하여 뿌리의 발근, 세포조직분화를 촉진시켜 식물의 안정된 성장에 도움을 주고 셀레늄은 나노입자상태로 식물에 빠르고 쉽게 흡수되어 사람이 식물을 통해 섭취할 경우 인체에 항산화력, 면역기능향상, 생식기능향상, 암예방 및 질병예방에 효과가 있다.The present invention is to prepare a functional organic liquid fertilizer by mixing nano silicate and nano selenium in an organic liquid fertilizer made of chitosan and amino acids using a saccharide as a base material, the functional organic liquid fertilizer prepared according to the present invention is a silicate is Instead of phosphate (P), it promotes rooting and cell differentiation, which helps to stabilize plants. Selenium is nanoparticles that are quickly and easily absorbed by plants. It is effective in improving history, immune function, reproductive function, cancer prevention and disease prevention.
당류, 키토산, 아미노산, 유기질 액체, 나노규산염, 나노셀레늄, 인산 Sugars, chitosan, amino acids, organic liquids, nanosilicates, nanoselenium, phosphoric acid
Description
본 발명은 기능성 유기질 액체 비료 제조방법에 관한 것으로써, 보다 상세하게는 당류를 모재로 하여 키토산과 아미노산을 사용하여 만든 유기질 액체비료에 나노규산염과 나노셀레늄을 혼합시켜 기능성 유기질 액체비료를 제조하는 것이다.The present invention relates to a method for preparing a functional organic liquid fertilizer, and more particularly, to prepare a functional organic liquid fertilizer by mixing nanosilicate and nano selenium with an organic liquid fertilizer made of chitosan and amino acids based on sugars. .
종래의 액체비료 제조방법은 게르마늄, 셀레늄, 아연 등의 광물성 물질을 결합제로 하여 제조하는 것으로써 대한민국 특허번호 제259790호에 게재되어 있고 대한민국 특허공개번호 제2000-0001061호는 다공성의 게르마늄 광석분말을 고온에서 팽창처리한 후 미생물 배양액과 혼합제조한 다공성 광석 미생물 복합 분말 비료제조공정을 제시하고 있다.Conventional liquid fertilizer manufacturing method is to manufacture a mineral material such as germanium, selenium, zinc as a binder is disclosed in Korean Patent No. 259790 and Korean Patent Publication No. 2000-0001061 is a porous germanium ore powder A process for preparing a porous ore microbial complex powder fertilizer prepared by mixing with microbial culture medium after expansion at high temperature is proposed.
한편, 대한민국 특허공개번호 제2005-0015195에서는 게르마늄과 셀레늄을 물에 혼합한 수용액을 90℃이상 가열하여 필터링 한 후 제조된 게르마늄과 셀레늄 용액을 당액, 꿀, 엿, 포도당, 젤라틴, 무수유당 등으로 제조한 액체비료에 혼합하여 제조하는 방법을 제시하고 있다.Meanwhile, Korean Patent Publication No. 2005-0015195 discloses a solution of germanium and selenium prepared by heating an aqueous solution of germanium and selenium mixed with water at a temperature of 90 ° C. or higher to sugar, honey, malt, glucose, gelatin, anhydrous lactose, and the like. A method for mixing and preparing a liquid fertilizer is provided.
그러나 이러한 방법으로 제조된 액체비료에 포함된 게르마늄 및 셀레늄 등은 성분이 함유된 수용액에 게르마늄 및 셀레늄 등이 포함된 함량이 정확하지 않고 파우더 상태로 액체비료에 섞어서 식물의 잎이나 관주에 엽면시비를 할 경우 식물의 잎이나 줄기에 있는 기공보다 입자가 커서 식물이 쉽게 흡수하지 못하는 단점이 있다.However, germanium and selenium contained in the liquid fertilizer prepared in this way is not accurate in the amount of germanium and selenium contained in the aqueous solution containing the components, and mixed with the liquid fertilizer in the form of powder to foliar fertilization If you do, the particles are larger than the pores on the leaves or stems of the plant has a disadvantage that the plant is not easily absorbed.
또한, 대부분의 복합 액체 비료는 그 모재를 단당류나 다당류를 사용하고 있는데 단당류나 다당류는 분해가 쉬워서 식물이 빨리 흡수하므로 빠른 성장을 하지만 뿌리가 약하여 식물의 수명이 짧고 병충해에 견디는 힘이 약해진다.In addition, most of the compound liquid fertilizer uses a monosaccharide or a polysaccharide of the base material, and monosaccharides or polysaccharides are easy to decompose, so the plant is quickly absorbed, so they grow quickly, but the roots are weak, and the plant life is short and the strength to withstand pests is weak.
따라서 식물의 뿌리 및 줄기가 강해지도록 규산염을 사용하고 있으나 일반 규산염은 물에 잘 녹지 않아 식물에 흡수가 어려운 단점이 있어 엽면이나 관주시비에는 규산염이 사용되지 않는다.Therefore, silicate is used to strengthen the roots and stems of plants, but general silicates are difficult to be absorbed by plants because they do not dissolve well in water.
본 발명은 종래의 문제점을 해결하기 위하여 안출된 것으로써. 다당류, 키토산, 비타민 등을 이용하여 식물성장에 좋은 액체비료를 제조시 규산염을 나노화 시킨 나노규산염과 유기나노셀레늄을 액체비료 제조과정에 첨가시켜 다당류, 키토산이 식물 성장제로 역할을 하면서 나노규산염이 직접 식물에 흡수되어 뿌리 및 줄기를 튼튼하게 함과 동시에 나노셀레늄이 식물에 흡수되어 인체에 좋은 셀레늄 식물이 성장하게 하는 기능성 유기질 액체비료 제조방법을 제공하고자 하는 것이다.The present invention has been made to solve the conventional problems. When producing liquid fertilizers that are good for plant growth using polysaccharides, chitosan, and vitamins, nanosilicates that have been nano-silicates and organo nano selenium are added to the liquid fertilizer manufacturing process. It is to provide a functional organic liquid fertilizer manufacturing method that is absorbed by plants to strengthen the roots and stems and at the same time nano selenium is absorbed by the plants to grow selenium plants good for the human body.
상기 목적을 달성하기 위한 본 발명은,The present invention for achieving the above object,
액체 비료의 원료인 당밀 등 다당류에 키토산, 아미노산 등을 첨가하여 모재 를 만들고 여기에 셀룰로오스, 인산, 수소칼슘 등을 첨가하여 용도에 따라 여러종류의 액체비료를 생산함에 있어서 기능성 나노물질을 첨가하여 기능성 액체비료를 만드는 것이다.Chitosan, amino acids, etc. are added to polysaccharides such as molasses, a raw material of liquid fertilizer, to make a base material, and cellulose, phosphoric acid, and calcium hydrogen are added to produce various types of liquid fertilizers depending on the purpose. It is to make liquid fertilizer.
기능성 나노물질은 규산염을 나노입자화시킨 후 실리카계 분산제를 사용하여 초순수에 분산시켜 5,000 내지 20,000ppm의 나노 규산염 수용액을 제조하고, 셀레늄을 나노입자화 시킨 후 초순수에 분산시켜 5,000 내지 10,000ppm의 고농도 셀레늄 수용액으로 제조한 뒤 수용액 중량비로 1 내지 3％의 단백질을 혼합하여 혼합수용액으로 제조한 후 이 혼합 수용액을 이리듐 전극판을 가진 10,000V의 직류 전압이 공급되는 고압 전극통에 넣어서 3시간 이상 가압하여 셀레늄의 (+) 전자기와 단백질내의 질소성분의 (-) 전자기가 결합하여 셀레늄에 단백질이 붙은 셀레늄-프로테인으로 제조하여 셀레늄이 식물의 세포조직에 흡수되어 식물이 프로테인을 분해하여 성장원료로 사용함과 동시에 셀레늄이 식물내에 많이 농축되도록 구성시켰다.The functional nanomaterial is nanoparticles of silicate and then dispersed in ultrapure water using a silica-based dispersant to prepare an aqueous nanosilicate solution of 5,000 to 20,000 ppm, and nanoparticles of selenium are dispersed in ultrapure water to be dispersed at high purity of 5,000 to 10,000 ppm. Prepared by the aqueous solution of selenium and then mixed with 1 to 3% protein by weight of the aqueous solution to prepare a mixed aqueous solution, the mixed aqueous solution was put into a high-pressure electrode cylinder supplied with a direct current of 10,000V with an iridium electrode plate and pressurized for more than 3 hours By combining the (+) electromagnetic of selenium and the (-) electromagnetic of nitrogen in protein, it is made of selenium-protein with protein attached to selenium. Selenium is absorbed by plant cell tissues and plants decompose protein and use it as growth material. At the same time, the selenium was configured to concentrate a lot in the plant.
기능성 유기질 액체비료제조에는 기존의 복합액체 비료제조과정과 같이 다당류나 아미노산, 키토산 등을 첨가하여 모재를 만들고 여기에 셀룰로오스, 인산, 수산칼슘 등을 첨가한 액체비료 용액에 나노규산염 수용액과 나노셀레늄-프로테인 수용액을 혼합하여 완성하는 것이다.Functional organic liquid fertilizers are prepared by adding polysaccharides, amino acids, chitosan, etc. as in the conventional composite liquid fertilizer manufacturing process, and then adding nanosilicate solution and nano selenium- to liquid fertilizer solution containing cellulose, phosphoric acid and calcium hydroxide. It is completed by mixing a protein aqueous solution.
본 발명에 따른 기능성 유기질 액체비료는 나노규산염 농도가 50 내지 2,000ppm, 나노 셀레늄-프로테인 농도가 2 내지 50ppm 포함되도록 만들어진 것이다.Functional organic liquid fertilizer according to the present invention is made to include a nano silicate concentration of 50 to 2,000ppm, nano selenium-protein concentration of 2 to 50ppm.
본 발명은 일반적인 유기질 액체비료에 나노규산염 및 나노 셀레늄-프로테인을 첨가한 기능성 유기질 액체비료의 제조방법을 제공함으로써 나노규산염이 식물의 뿌리 및 줄기 성장을 촉진하고 셀레늄이 식물내에 흡착저장되게 함으로써 항암, 항산화 효과가 있는 유익한 셀레늄을 인체가 직접 섭취할 수 있도록 하여 인간의 건강 증진에 크게 기여할 수 있을 것이다.The present invention provides a method for preparing a functional organic liquid fertilizer, in which nanosilicate and nano selenium-protein are added to a general organic liquid fertilizer, thereby promoting the growth of roots and stems of plants and allowing selenium to be adsorbed and stored in plants. It will be able to contribute to the improvement of human health by allowing the human body to directly consume the beneficial selenium with antioxidant effect.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100964749B1 (en) | 2009-12-03 | 2010-06-21 | 동양정밀화학(주) | Compound nano fertilizer of amino acid material using nano-sheet of layered clay minerals and manufacturing method thereof |
| KR101246342B1 (en) | 2011-03-09 | 2013-03-21 | 함지박(주) | Method for preparing a fertilizer containing amino acids with water-soluble silicic acid |
| KR20160047928A (en) * | 2014-10-23 | 2016-05-03 | 주식회사 마이크로젠 | Manufacturing method of chitosan-amino acid nano composite |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101301003B (en) * | 2008-06-23 | 2010-12-22 | 四川师范大学 | Selenium-rich antistaling agent for fruits and vegetables and antistaling solution prepared therefrom |
| CN104829382B (en) * | 2015-05-20 | 2017-12-26 | 内蒙古朵日纳硒科生物技术有限公司 | A kind of high-efficient selenium-rich wheat or rice leaf spray fertilizer |
| CN107162777A (en) * | 2017-06-23 | 2017-09-15 | 华南农业大学 | One kind spraying film forming controllable sustained-release type blade face selenium fertilizer and preparation method and application |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100964749B1 (en) | 2009-12-03 | 2010-06-21 | 동양정밀화학(주) | Compound nano fertilizer of amino acid material using nano-sheet of layered clay minerals and manufacturing method thereof |
| KR101246342B1 (en) | 2011-03-09 | 2013-03-21 | 함지박(주) | Method for preparing a fertilizer containing amino acids with water-soluble silicic acid |
| KR20160047928A (en) * | 2014-10-23 | 2016-05-03 | 주식회사 마이크로젠 | Manufacturing method of chitosan-amino acid nano composite |
| KR101662146B1 (en) | 2014-10-23 | 2016-10-05 | 주식회사 마이크로젠 | Manufacturing method of chitosan-amino acid nano composite |
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