KR100614107B1 - The method for manufacturing of Ceramics and It's use - Google Patents

Abstract

In the present invention, the mixture consisting of dolomite or biotite, sepiolite, smackite, tourmaline, and illite is added to a ball mill by a mixture consisting of 6: 1: 1: 1 by weight in a ball mill, and then the temperature is 500 to 700 ° C. After heating, 500 g of ethanol was added to form a bean size, and then molded using a conventional molding apparatus, and then impregnated with 0.1 N aqueous silver nitrate solution for 16 hours, and then reheated at 200 to 300 ° C. for disinfectant, water purifying agent, odor, and poisoning. The present invention relates to a method for producing a ceramic used for gas adsorption, deodorization, and a decomposition agent, and to a use of the ceramic.

Ceramics. Healthy drink. Fertilizer.

Description

The method for manufacturing of Ceramics and It's use}

In the present invention, the mixture consisting of dolomite or biotite, sepiolite, smackite, tourmaline, and illite is added to a ball mill by a mixture consisting of 6: 1: 1: 1 by weight in a ball mill, and then the temperature is 500 to 700 ° C. After heating, 500 g of ethanol was added to form a bean size, and then molded using a conventional molding apparatus, and then impregnated with 0.1 N aqueous silver nitrate solution for 16 hours, and then reheated at 200 to 300 ° C. for disinfectant, water purifying agent, odor The present invention relates to a method for producing a ceramic used for gas adsorption, deodorization, and a decomposition agent, and to a use of the ceramic.

Modern people are living with various symptoms of deterioration of physical strength due to mental and physical activities and excessive stress due to the rapid change of living culture and environment. In this context, the development of yangyangjiang beverages and the like is actively progressing, the sales of these products are rapidly increasing, and some of them are already generalized, and the manufacturing method of tea using natural foods has been widely known.

In addition, methods of ingesting healthy substances contained in extracts of minerals by using natural and synthetic minerals and tasting water extracted from minerals by impregnation with water have been widely known.

For example, Korean Patent Laid-Open Publication No. 2002-0009754 discloses a method and a composition of fruit juices based on non-ruptured fruits, and Publication No. 2002-0024127 discloses herbal ingredients and seaweeds. Drinks containing substances which are medicines for preparing drinks using animals, minerals, plants and health foods are described,

Publication No. 1995-0013394 discloses a method for preparing cholesterol-free healthy noodles using onion, which is mixed with onion powder, garlic powder, wheat flour and riboflavin, kneaded with natural salt or water and then prepared with noodles.

Korean Patent Publication No. 1996-0015255 discloses a method for preparing onion juice prepared by mixing water, onion, fructose, citric acid, vitamin C, pineapple juice and syrup,

In Korean Laid-Open Patent Publication No. 2000-2850, elite raw materials are added to a pulverizer and pulverized in a 320 to 2000 mesh, hydrosulfide is mixed at a volume ratio of 15: 1, water is added, and crushed by a friction crusher. Described is a technique for producing an ultrafine powder produced by adding a neutralizing agent to a sulfided material, followed by filtration and drying.

Korean Laid-Open Patent Publication Nos. 99-43936 and 93-413 include illite in mortar to neutralize the toxicity and odor of cement to prevent blood circulation, fatigue recovery, air purification, and various adult diseases. A method for producing light mortar is described,

Korean Laid-Open Patent Publication No. 10-1992-655 describes a method for producing a confused magnetic field composition based on elvan, sorghum and magnetic force.

Publication No. 2003-47957 discloses blissful beauty water that removes fine wrinkles, sunscreen, removes spots, removes mushrooms, and moisturizes skin when sediment of mica is used as beauty water.

Korean Patent Publication No. 1999-009259 discloses a method for preparing a mineral stock solution using biotitanium, which is prepared by heating and stirring the biotite, mixing with aqueous sulfuric acid solution, and mixing with mineral water again, and then removing the precipitate. No. 91-14148 discloses a coagulant for crushing an illite ore and mixing aluminum sulfate and calcium hydroxide to prepare a water purifying agent, and then adsorbing heavy metal ions, radioactive waste ions and organic ions dissolved in water by the water purifying agent. Although a method for preparing an adsorptive settling water purifier for purifying wastewater by coagulation of

The conventional techniques have been used to treat natural minerals by physical treatment, or simply by adding heavy metal solution to natural minerals and stirring to adsorb heavy metals. .

In order to solve the above problems, the present invention has been studied to improve the physical properties as a result of using a mixture of dolomite or mica, sepiorite, smackite, tourmaline, illite excellent antibacterial and adsorption effect After pulverizing and heating, molding using ethanol and impregnating with silver nitrate solution for a while, the present invention relates to a method for producing ceramics used as a disinfectant, water purifying agent, odor and toxic gas adsorption, deodorization, and decomposing agent and uses of ceramic .

In order to achieve the above object, the present invention is a mixture of dolomite or mica, sepiolite, smackite, tourmaline, illite 6: 1: 1: 1 by weight into a ball mill and crushed to a size of 300 mesh Then, after heating to a temperature of 500 ~ 700 ℃, 500g of ethanol was added to the size of the bean grains using a conventional molding apparatus, and then impregnated in 0.1N silver nitrate aqueous solution for 16 hours, then reheated at 200 ~ 300 ℃ The present invention relates to a method for producing a ceramic used as a disinfectant, a water purifying agent, a malodorous and toxic gas adsorption, a deodorizing agent, and a use of the ceramic.

According to the present invention, the mica and the mica are a kind of mica, and according to the record of the new cultivated herbaceous plant, the medicinal herb, and the Dongbogam record, the taste is spicy, the property is flat, and there is no poison.

It is used to treat the body's skin with fleshy skin, stroke, cold and fever, and surrey and stomach motion sickness. It brightens the eyes and eats for a long time. In addition, the will is strong without getting cold or hot.

Biotite is also suitable for eliminating far-infrared radiation, mineral elution, detoxification, weight loss (improved obesity), various neuralgia, and arthritis pain when used as flooring in a room.

Citizens used granite paddle ball instead of mica paddle ball, but when firewood was burned, the stone became hot and splashed, and the medicinal ingredients were weak.

According to the New Nongbyeon Herbal Medicine, the Herbal Medicine Collection Room, and Dongbogam Record, the biotite is sweet and warm, and the name of the Mistletoe is poisonous.

It was used to listen to hemostasis, dizziness, game, diarrhea, and to eliminate seasickness and especially fat. Because of the strength of the muscles and muscles down, it became a standing medicine of the anti-horse army in Kang Byeong-Shin (强 兵 術).

The strongest detoxification and when the mica is mixed with a lot of loess, the loess is said to be excellent detoxification.

According to Yasa, high-quality mica was produced at Gyeryongsan, and if it was designated as the royal road (Seoul), the soldiers insisted that Ganggun (强 軍) would be in good health and that the royal citizens would be healthy.

Sepiolite is a fibrous tissue, which is like a parallel row centered on fibrin, which consists of two layers aligned with a silicic tetrahedron, a magnesium octahedron produced by a layer of silicon tetrahedra and the remaining oxygen atoms. Is the other floor.

When the arrangement is changed, the fibrous tube appears according to the direction of the fibrin, and the sepiolite as the tissue constituent has suction moisture crystal water and chemical hydroxyl water.

Thus, the sepiolite is a lot of water exchange, and as the fiber tube absorbs only the other small molecule, it is to help the production of potassium permanganate and antimicrobial ceramics through the sepiolite, and to start the active absorption.

In addition, the far-infrared emissivity and radiation energy in

Emissivity: 0.99㎛

Radiated energy: 3.81 × 10 ² (W / m ² ㎛ 40 ℃)

The molecular structure of the tourmaline used in the present invention is as follows, specific gravity is about 3.1, Mohs hardness is about 7.3.

3 [NaX ₃ Al ₆ (BO ₃ ) Si ₆ O ₁₆ (OH ₉ F) ₄ ]

Where (X is Mg, Fe, Li, etc.),

Therefore, the addition of the smacktite and tourmaline (tourmaline) has no wide range of antibacterial activity and toxicity to the human body, is an environmentally friendly material, no discoloration by ultraviolet light, maintains the freshness of food for a long time, There is an advantage that can suppress the occurrence of odor, adsorptive decomposition of odor molecules, and increase the growth of animals and plants.

The distribution of illite is rare in the world, and is distributed in Illinois, Mississippi, Canada, Quik province, Europe, Hungary, and Yeongdong, Korea, but most of them are sedimentary minerals. It is a high-quality product with few impurities. It has a three-layered mineral structure. Its main components are SiO ₂ , Al ₂ O ₃ , and K ₂ O. It is a yellowish white (white, red) synthetic mineral. It emits 89 ~ 92% of far-infrared rays of micron wavelength, it has strong deodorizing power (98%), emits strong groups, activates water molecules in water, secures more than three times of dissolved oxygen, and has strong oxygen coagulation power. , (-) 2 has charge in water, adsorbs cationic organic ions in water, its own function makes moisturizing effect large, prevents direct ultraviolet rays, high vitality, Improves (by oxygen, far infrared rays, anions, groups, etc.), and emits strong anions (dry powder state: 141ion / cc).

Silver is a metal as old as copper was discovered about 5000 to 6000 years ago, and has been known as a precious metal since ancient times, along with gold, iridium, palladium, and platinum.

However, the reason why it is inferior in terms of use compared to gold is that it can be obtained by using less refined refining than that produced by nature. For this reason, there were several records of trade in silver in the Bible because of their former value as gold. With the discovery of the new continent in the 16th century, a massive amount of silver was introduced, the price revolution and refinement methods developed, and the supply of silver increased, which is now widely used in currency, ornaments, stoneware, photography, advanced science, etc. In the East our country has been known as a country of high quality silver. There are a number of silver rings in the tombs of Taeseong-ri, Gangseo-gun, Pyeongan-do, Pyeongan-do. Silla's silver is well-known in the east for its high quality, and many people have produced a lot of gold and silver to decorate their heads and clothes. Has been exported. In Korea, the production of silver increased, and in 1101 silver coins began to be used. Since then, mining of silver continued to increase, and in 1678 there were 68 silver-producing areas in our country. The most famous. Babylonia in Europe had already made and used alloys of gold and silver before 3000-4000 B.C., at that time gold and silver were more expensive than alloyed gold, probably because it was very difficult to smelt silver. There is also a record of mining silver in mines around Greece in the 9th century B.C., since silver is usually obtained from mixed minerals, it first obtains an alloy of lead, zinc, silver, etc. and then heats it strongly in the air to produce lead and zinc. Removed and pure silver was obtained. In Germany, silver began to be harvested around the 10th century. Mexico and Pepu are the world's largest deposits of silver, and the world accounts for almost all of its production. Silver is still smelted from mixed minerals as it used to be. These mixed minerals usually contain 15-20% zinc, 10-15% lead and 0.15-0.25% silver. However, silver is more soluble in zinc than lead in heated conditions, so melting the primary alloy from the ore will cause the silver to float up with the zinc. When it is split and heated again, zinc evaporates and a small amount of lead oxidizes to separate it from silver.

Silver is an atomic symbol: Ag, atomic number: 47, atomic weight: 107.88, specific gravity: 10.5 (20 ℃), melting point: 960.8 ℃, boiling point: 2.212 ℃. They found that they could be stored for a long time, and that water did not deteriorate at all for a long time in the silver vessel they had kept.In the herbaceous wood, the five organs were comfortable, the mind and body were stabilized, and the body was lightened. It is said to lengthen,

As a result of the experiments to date, silver has been confirmed to sterilize almost all single cell pathogens on the earth. The most promising theory is that silver disinfects pathogens by special catalysis that is involved in metabolism (digestion, respiration) of single cell pathogens. . In addition to preventing and sterilizing the metabolism of pathogens, it has been known that the electrical load of silver ions released by metals inhibits the reproductive function of pathogens.

In the present invention, the addition of silver nitrate is a process for removing the toxicity by treating the solution by impregnation for 16 hours and reheating at 200-300 ° C. to remove the toxicity by coating the silver component.

Hereinafter, described in detail through the preferred embodiment of the present invention.

Example 1

Dolomite 600g, Sepiolite 100g, Smactite 100g, Tourmaline 100g, Illite 100g are put into a ball mill and pulverized to 300 mesh size, heated to a temperature of 500 ~ 700 ℃, and 500g of ethanol is added to the size of bean beans. After molding using a molding apparatus, and then impregnated with 0.1 N silver nitrate aqueous solution for 16 hours, and reheated at 200 ~ 300 ℃ to prepare a ceramics.

Example 2

Cicadas 600g, Sepiolite 100g, Smactite 100g, Tourmaline 100g, Illite 100g are put into a ball mill and pulverized to a size of 300 mesh, heated to a temperature of 500 ~ 700 ℃, 500g of water in the size of the bean After molding using a molding apparatus, and then impregnated with 0.1 N silver nitrate aqueous solution for 16 hours, and reheated at 200 ~ 300 ℃ to prepare a ceramics.

Example 3

The ceramics prepared in Examples 1 and 2 were immersed in water for about 6 hours to purify the water, and then purified water was removed to prepare a supernatant and used as drinking water (health drink).

Experimental Example

Table 1 Lead Content Test

Lead Detection method of inspection Remarks Example 1 Not detected Atomic absorption analysis Example 2 Not detected Atomic absorption analysis Example 3 Not detected Atomic absorption analysis

Table 2 Detection of Hazardous Heavy Metals

Heavy metals method of inspection Remarks Example 1 Not detected Atomic Absorption Analysis and USP 23 Example 2 Not detected Atomic Absorption Analysis and USP 23 Example 3 Not detected Atomic Absorption Analysis and USP 23

The results of the sensory test on the taste (A), color (B), overall aroma (C) of the health drink were randomly extracted by panelists from 10 men and women in their 30s and 40s. same.

Table 3 Sensory Test Results

division A B C Example 1 95 96 95 Example 2 94 95 94 Example 3 95 95 93

Very good 10 points, good 8-9 points, usually 6-7 points, bad 4-5,

Very bad below 3 points.

As can be seen through various embodiments of the present invention, the health beverage prepared by Example 3 of the present invention has a unique taste unlike the general health beverage, and after the harmful substances contained in natural ores are extracted Fermented and matured, the health drink was distributed to the general public and developed according to consumer's taste, and its taste, color and aroma were significantly improved than the general health drink.

In addition, applying the health beverage prepared in Example 3 to the skin showed a skin moisturizing effect such as applying a pack using a tidal flat.

Example 1

5 L to 20 L of the health beverage prepared in Example 3, the wheat flour rate 1000 kg and molasses 20 kg, charcoal powder 1 kg, water and 100 L evenly mixed and fermented and dried to prepare the composition prepared in the existing feed 1 ~ When mixed with 5% by weight, cows, pigs, and chickens have less smell on stools. Especially, pigs are effective for diarrheal diseases, and chickens are better for respiratory diseases. In addition, as a result of drinking the manufactured healthy beverage for drinking of the livestock, the feed efficiency of the livestock and the disease resistance or the stools of the livestock come out clean.

Example 2

The fermentation of the health beverage prepared in Example 3 together with the livestock waste and breeding and fermentation of the organic microorganism prepared by fertilizing the fertilizer 1 ~ 5% by weight to the existing fertilizer when used in the cultivation rate of plants, viruses Resistant to the disease caused, fruit water appears to have a great effect such as cultivating high sugar.

Example 3

As a result of applying the health beverage prepared in Example 3 to the skin, it was confirmed that the moisturizing effect of the skin is high, especially in the case of dry skin, the dryness of the skin is reduced.

Example 4

The synthetic yarns were prepared by drying the fine minerals such as treated serpentine, mica, and gold mica, which are by-products produced by Example 3, by drying them, and then applying microparticles to the surface of the yarn as a raw material of the fiber. , As a result of wearing the garments woven with the synthetic yarn prepared above, after a few days it was found that the smell does not smell without washing.

Example 5

Natural ores such as by-products produced after the manufacture according to Example 3, such as serpentine, mica, and gold mica are dried and finely powdered, and then used as a building material. Worked

The present invention as described above has the effect that can be widely used in health supplements, building materials, exteriors, skin protectors, clothing and yarn use, animal feeds and plant fertilizers.

Claims (5)

In the manufacturing method of the ceramic, After a mixture of dolomite or camellia, sepiolite, smoctite, tourmaline, and illite was added to a ball mill, a mixture of 6: 1: 1: 1 was added to a ball mill and crushed to a size of 300 mesh, and then heated to a temperature of 500 to 700 ° C. , 500g of ethanol was molded into a bean sized size using a conventional molding apparatus, and then impregnated with 0.1 N aqueous silver nitrate solution for 16 hours, followed by reheating at 200-300 ° C. to manufacture a ceramic. In the manufacturing method of a health beverage using ceramic, After a mixture of dolomite or camellia, sepiolite, smoctite, tourmaline, and illite was added to a ball mill, a mixture of 6: 1: 1: 1 was added to a ball mill and crushed to a size of 300 mesh, and then heated to a temperature of 500 to 700 ° C. , 500g of ethanol was formed into a bean sized size using a conventional molding apparatus, and then impregnated with 0.1N silver nitrate solution for 16 hours, and then reheated at 200-300 ° C. After immersing the prepared ceramics in water for about 6 hours to purify the water, and then remove the precipitate of the purified water to prepare a supernatant liquid, characterized in that for producing a supernatant. In the method of using a healthy beverage prepared using ceramic, Method for using the health beverage prepared in claim 2 as a feed. In the method of using a healthy beverage prepared using ceramic, A method of using the health beverage prepared in claim 2 as a fertilizer. delete