KR100215991B1 - Far-infrared radiative ceramic composition and its method - Google Patents
Far-infrared radiative ceramic composition and its method Download PDFInfo
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- KR100215991B1 KR100215991B1 KR1019970003216A KR19970003216A KR100215991B1 KR 100215991 B1 KR100215991 B1 KR 100215991B1 KR 1019970003216 A KR1019970003216 A KR 1019970003216A KR 19970003216 A KR19970003216 A KR 19970003216A KR 100215991 B1 KR100215991 B1 KR 100215991B1
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Abstract
본 발명은 알루미나 76∼88중량%, 산화마그네슘 1.8∼2.2중량%, 산화칼슘 1.8∼2.0중량%, 산화나트륨 1.0~1.4중량%, 산화칼륨 0.1∼0.3중량%, 철분 0.1∼0.3중량% 및 실리카 6∼8중량%를 함유하는 천연광물 분말 7∼10중량%; 증류수 83∼86중량%; 항균조제 1∼2중량%; 우레탄실리콘수지 1∼2중량%; 및 이온화촉매제 2∼3중량%를 혼합하여, 그리고 선택적으로 쾌적향 원료와 대전방지제를 더 첨가하여 조성하는 것으로, 이들을 1,2차 교반에 의해 이온화시켜 방치함으로써 제조된다.이렇게 제조되는 원적외선 방사 조성물은 항균, 방취 기능 및 대전방지 기능이 있어 섬유에 적용시 독특한 천연향기가 발생되어 기분 좋은 향기와 상쾌함 등을 줄수 있을 뿐 아니라 신체 주위의 각종냄새를 제거하여 쾌적한 생활을 영위할 수 있도록 하고, 기존 원료에 비해 가격이 훨씬 싸서 대증화에 용이함은 물론 중성으로 제조 가능하여 섬유 전 분야에 부작용 없이 널리 이용될 수 있는 효과를 갖는다.The present invention comprises 76 to 88% by weight of alumina, 1.8 to 2.2% by weight of magnesium oxide, 1.8 to 2.0% by weight of calcium oxide, 1.0 to 1.4% by weight of sodium oxide, 0.1 to 0.3% by weight of potassium oxide, 0.1 to 0.3% by weight of iron and silica 7-10% by weight of natural mineral powder containing 6-8% by weight; 83 to 86% by weight of distilled water; 1 to 2% by weight of antibacterial aid; 1 to 2% by weight of urethane silicone resin; And by mixing 2-3 wt% of an ionization catalyst, and optionally further adding a pleasant flavor raw material and an antistatic agent, and preparing them by ionizing and leaving them by first and second stirring. The far-infrared radiation composition thus prepared is prepared. It has antibacterial, deodorizing function and antistatic function, so when applied to fiber, unique natural fragrance is generated, which can give pleasant fragrance and freshness, and remove various odors around the body so that it can lead a pleasant life. The price is much cheaper than the raw material, so it is easy to enlarge and can be manufactured in a neutral manner. Therefore, it can be widely used in all fields of the fiber without side effects.
Description
본 발명은 원적외선 방사 조성물에 관한 것으로서, 보다 상세하게는 의류 등의 각종 섬유류에 적용되어 쾌적향 발산, 항균, 방취 및 원적외선 방사 기능을 발휘, 인체의 신진대사를 원활하게 할 수 있음은 물론 그 외에도 식물성장촉진제나 기타 건강관련용품 등에 널리 이용될 수 있는 원적외선 방사 조성물과 그 제조방법에 관한 것이다.The present invention relates to a far-infrared radiation composition, and more particularly, it can be applied to various fibers such as clothing, exhibiting comfort emanation, antibacterial, deodorization and far-infrared radiation, and smoothing the metabolism of the human body as well as other things. The present invention relates to a far-infrared radiation composition which can be widely used for plant growth promoters or other health-related products, and a method of manufacturing the same.
원적외선은 물체 내부의 분자운동에 의한 전자력선의 진동파로서, 인체의 신진대사를 원활하게 해 주는 작용을 한다. 따라서 여러 산업분야에 이용되고 있는데, 특히 건강관련용품에 널리 이용되고 있다.Far-infrared rays are vibration waves of electromagnetic force lines caused by molecular motions inside the object, and function to smooth metabolism of the human body. Therefore, it is used in various industrial fields, in particular, it is widely used in health-related goods.
일반적으로 원적외선 방사체는 분말 상태로 제조한 후 이를 그대로 또는 액상으로 만들어 어떠한 물건을 만들거나 또는 코팅, 침적 등의 방법으로 적용하게된다.In general, the far-infrared radiator is manufactured in a powder state and made as it is or in a liquid form to make any object or applied by a method such as coating or deposition.
특히 의류 등 섬유류에 원적외선 발생 물질을 적용하는 경우, 대부분은 원적외선 물질을 혼합, 가수 및 소성한 후 분말로 만들고 이것을 액상화하여 사용하였으나, 이미 소성 분말화된 원적외선 물질을 물 등에 액상 이온화시키기가 매우 어렵고, 또한 경제성이 떨어치는 단점이 있다.In particular, in the case of applying far-infrared ray generating materials to textiles such as clothing, most of them are mixed, hydrolyzed and calcined to make powder and then liquefied it, but it is very difficult to liquid ionize the already powdered far-infrared ray material in water and so on. In addition, it also has the disadvantage of low economic efficiency.
따라서 섬유류에 쉽게 적용할 수 있는 액상 또는 이온화된 상태의 원적외선방사 조성물 개발이 요구되고 있으며, 그 예로서 한국특허공고 96-15657호에 규산소다, 알루미늄소다, 산화나트륨, 치오황산나트륨, 이산화게 르마늄, 정제 포도당,상백당 등을 각각 30∼40℃에서 용해한 후 혼합하고 금을 염화금산으로 이온화한 것과 질산은을 치오황산은으로 이온화한 것을 상기 혼합액에 첨가한 후 상온에서 48∼72시간 방치하는 것을 특징으로 하는 액상(이온화) 바이오세라믹스의 제조방법이 개시된 바 있다.Therefore, there is a need for developing a far-infrared radiation composition in a liquid or ionized state that can be easily applied to fibers. For example, Korean Patent Publication No. 96-15657 discloses sodium silicate, aluminum soda, sodium oxide, sodium thiosulfate, and germanium dioxide. And purified glucose, white sugar and the like at 30 to 40 ° C., respectively, and then mixed, and ionized gold with gold chloride and silver nitrate with silver thiosulfate, added to the mixture, and left at room temperature for 48 to 72 hours. A method for producing a liquid (ionized) bioceramic has been disclosed.
그러나 상기한 액상(이온화) 바이오세라믹스의 제조방법은 유기화합물을 이온화하는 것으로, 여기에 사용되는 원료의 대부분이 강한 알칼리성으로서, 이 방법으로 만든 원적외선 발생 액상물질은 pH 11∼12로서 이를 섬유에 적용하면 재질에손상을 주고 가공하는 동안에 일정온도 이상에서 황변 현상이 발생하며, 그리고 촉감에 심한 변화를 주어 그 적용범위가 한정될 수밖에 없었다. 또한 이 방법에 의하면 금과 같은 비싼 원료를 사용하므로 경제성이 떨어질 수밖에 없었다.However, the above-mentioned method of preparing liquid (ionized) bioceramic is ionizing organic compounds, and most of the raw materials used are strong alkaline, and the far-infrared liquid liquid produced by this method is applied to fibers as pH 11-12. If the material is damaged and yellowing phenomenon occurs over a certain temperature during processing, and the touch is severely changed, the scope of application is inevitably limited. In addition, according to this method, the use of expensive raw materials, such as gold, was inevitably deteriorated.
이에 본 발명자는 상기의 문제를 해결하기 위하여 연구를 거듭한 바, 알루미나(산화알루미늄) 계열의 천연광물을 초미립자 상태로 분쇄한 후 액상으로 이온화하는 방법에 의해 저렴하고 간단하게 제조되는 액상(이온화) 원적외선 방사 조성물을 제공할 수 있음을 알게 되었다.Accordingly, the present inventors have repeatedly studied to solve the above problems, liquid (ionization) inexpensively and simply produced by a method of pulverizing alumina (aluminum oxide) -based natural minerals into ultrafine particles and ionizing them into a liquid phase It has been found that a far infrared emitting composition can be provided.
즉, 본 발명의 목적은 원적외선의 방사율이 높고 쾌적향 발산, 항균, 방취기능 등을 가지고 있어 인체 건강을 보다 이롭게 할 수 있고, 값싼 원료를 사용하여 저렴하므로 대중화에 용이하며, 중성으로 이온화되어 모든 섬유 재질에 대해서가공시 부작용이 거의 없는 원적외선 방사 조성물 및 그 제조방법을 제공하는 데에 있다.That is, the object of the present invention is high far-infrared emissivity and has a comfortable smell divergence, antibacterial, deodorizing function, etc., which can be beneficial to human health, and is easy to popularize because it is cheap using cheap raw materials, and is ionized to neutral It is to provide a far-infrared radiation composition and a method for producing the same that have little side effects in processing for the fiber material.
도 1은 본 발명에 따른 원적외선 방사 조성물의 제조 공정도.1 is a manufacturing process diagram of the far-infrared radiation composition according to the present invention.
본 발명의 목적을 달성하기 위한 원적외선 방사 조성물은, 알루미나 계열의 천연광물 분말 7∼10중량%, 증류수 83∼86중량%, 항균조제 1∼2중량%, 우레탄실리콘 수지 1∼2중량% 및 이온화촉매제 2∼3중량%로 조성되는 데에 특징이 있으며, 여기에 선택적으로 쾌적향 원료를 전체의 2∼3중량%와 소량의 대전방지제를 더 첨가하여 조성될 수 있는 것이다.Far-infrared radiation composition for achieving the object of the present invention, alumina-based natural mineral powder 7-10% by weight, distilled water 83-86% by weight, antibacterial aid 1-2%, urethane silicon resin 1-2% and ionization It is characterized in that it is composed of 2 to 3% by weight of the catalyst, and may optionally be added by adding 2 to 3% by weight of the total amount of the comfort material and a small amount of antistatic agent.
본 발명에서 사용하는 알루미나 계열의 천연광물 분말은 알루미나, 산화마그네슘, 산화칼슘, 산화나트륨, 산화칼륨, 철분 및 실리카(이산화규소) 등을 함유한 것인데, 구체적으로는 알루미나 76∼88중량%, 산화마그네슘 1.8∼2.2중량% , 산화칼슘 1.8∼2.0중량%, 산화나트륨 1.0~1.4중량%, 산화칼륨 0.1∼0.3중량%, 철분0.1∼0.3중량% 및 실리카 6∼8중량%을 함유한 광물 분말을 사용한다.The alumina-based natural mineral powder used in the present invention contains alumina, magnesium oxide, calcium oxide, sodium oxide, potassium oxide, iron, silica (silicon dioxide), and the like, specifically, alumina 76 to 88% by weight, oxidation Mineral powder containing 1.8 to 2.2% of magnesium, 1.8 to 2.0% of calcium oxide, 1.0 to 1.4% of sodium oxide, 0.1 to 0.3% of potassium oxide, 0.1 to 0.3% of iron, and 6 to 8% of silica use.
상기 항균조제와 이온화촉매는 특별히 한정되는 바 없으며, 쾌적향 원료는 천연물질에서 추출된 것으로 인체에 유해하지 않은 꽃 향료, 나무 향료 등을 마이크로캡슐화 하여 사용한다:The antimicrobial preparations and ionization catalysts are not particularly limited, and the pleasant fragrance raw materials are extracted from natural materials and used by microcapsulating flowers, wood fragrances, etc., which are not harmful to the human body:
또한 원적외선 방사 조성물의 제조방법은, 천연광물 분말, 증류수, 항균조제, 우레탄실리콘수지 및 이온화촉매제를 혼합하는 제 1 공정; 제 1 공정의 혼합물과 지르콘소재세라믹볼을 함께 분쇄기에 넣고 교반하여 원재료를 미립자로 분쇄하는 제 2 공정; 상기 제 2 공정의 처리물에 선택적으로 향료와 대전방지제를 첨가한 후 교반하여 이온화시키는 제 3 공정; 및, 제 3 공정의 처리물을 여과하여 방치하는 제 4 공정을 포함한다.In addition, the method for producing a far-infrared radiation composition includes a first step of mixing a natural mineral powder, distilled water, an antimicrobial aid, a urethane silicone resin and an ionization catalyst; A second step of putting the mixture of the first step and the zircon material ceramic ball together into a grinder and stirring to grind the raw material into fine particles; A third step of selectively adding fragrance and an antistatic agent to the treated material of the second step, followed by stirring to ionize; And a fourth step of filtering and leaving the processed material of the third step.
도 1를 참조하면, 상기 제 1 공정은 단순한 재료의 혼합 공정(S1)이고, 제 2 공정은 순환식 분쇄기를 사용하여 통상 500rpm의 속도로 4시간 정도 진행하는 원재료 미세화, 분쇄 공정(S2)이다. 여기서 지르콘소재세라믹볼은 3Φ정도의 분쇄볼로서 원료의 미세화를 촉진하기 위해 함께 넣어 교반한다. 제 3 공정은 2차 분쇄 이온화 공정(S3)으로 보다 용량이 큰 혼합분쇄기에 제 2 공정의 처리물을 넣어 약500rpm의 속도로 약 2시간 정도 교반하는 과정이고, 제 4 공정은 제 3 공정의 처리물을 여과시스템을 천천히 통과시켜(S4; 여과공정) 그 여과액을 약 1일 정도 상온에서 방치하는 공정(S5)이다.Referring to FIG. 1, the first step is a simple material mixing step (S1), and the second step is a raw material refinement and grinding step (S2) that proceeds for about 4 hours at a speed of 500 rpm using a circulating grinder. . Here, the zircon material ceramic ball is a grinding ball of about 3Φ and put together to promote the miniaturization of the raw material and stirred. The third step is a secondary pulverization ionization step (S3), in which the processed material of the second step is added to a larger mixing grinder and stirred at a speed of about 500 rpm for about two hours. The processed material is passed slowly through the filtration system (S4; filtration step), and the filtrate is left at room temperature for about 1 day (S5).
이러한 제조공정에 있어서, 원료로 사용되는 쾌적향 원료와 대전방지제는 상기 제 1 공정에서 다른 원료와 함께 혼합할 수도 있고, 제 3 공정을 진행시에 혼합물에 첨가할 수도 있다.In such a manufacturing process, the comfort-oriented raw material and the antistatic agent used as the raw material may be mixed with other raw materials in the first step, or may be added to the mixture during the third step.
본 발명에 따른 이온화된 원적외선 방사 조성물과 타사(특허공고 제96-15657호의 발명)의 액상 바이오세라믹스 제조방법에 의해 제조된 원적외선 방사 조성물의 특성을 상온(35℃)에서 측정하여 비교하면 다음 표 1과 같다.When comparing the characteristics of the ionized far-infrared radiation composition according to the present invention and the far-infrared radiation composition prepared by the liquid bioceramic manufacturing method of another company (Invention No. 96-15657) measured at room temperature (35 ℃) Table 1 Same as
[표 1] 특성비교표[Table 1] Characteristics comparison table
-스캔--scan-
상기 표 1을 참조하면, 본 발명에 따른 원적외선 방사 조성물은 원적외선 방사율 및 방사강도에 있어서 타사원료 보다 조금 더 우수하고, pH에 있어서 타사원료는 11∼12로서 알칼리성인데 반해 본 발명의 조성물은 3∼11로서 중성 조제가 가능하다.따라서 중성의 원적외선 방사 조성물을 섬유 가공에 사용하면 부작용이 없는 바, 섬유 전 분야에 널리 적용될 수 있다. 또한 본 발명의 조성물은 쾌적향 기능, 항균, 방취 기능 등의 다기능성을 보유하고 있음은 물론 가격면에 있어서도 타사원료의 1/30에 불과할 정도로 경제적이다.Referring to Table 1, the far-infrared radiation composition according to the present invention is slightly better than the other company's raw material in far infrared emissivity and radiation intensity, while the other company's raw material is alkaline in pH 11 to 12, while the composition of the present invention is 3 ~ Neutral preparation is possible. Therefore, when the neutral far-infrared radiation composition is used for fiber processing, there is no side effect, and thus it can be widely applied to all fields of fiber. In addition, the composition of the present invention is not only economical enough to retain the versatility of the comfort function, antibacterial, deodorizing function, etc., but also in the price of 1/30 of the raw materials of other companies.
또한 타사원료는 섬유에 가공시 130℃에서 황변 현상이 발생하였는데 반해, 본 발명의 조성물을 섬유에 적용한 경우에는 황변 현상을 발견할 수 없었다. 이와같이 본 발명의 조성물이 우레탄계 실리콘 수지를 사용함에도 불구하고 황변 현상이 발생하지 않은 것은 우레탄계 수지의 사용량이 매우 적고 또한 이온화 과정에서 다른 성분이 우레탄계 수지에 작용하여 특성을 변화시켰기 때문이라고 생각된다.In addition, the raw material is yellowing phenomenon occurs at 130 ℃ when processing the fiber, the yellowing phenomenon was not found when the composition of the present invention is applied to the fiber. Thus, even though the composition of the present invention uses a urethane-based silicone resin, yellowing does not occur because the amount of the urethane-based resin is very small and other components act on the urethane-based resin in the ionization process to change characteristics.
이상에서 상세히 설명한 바와 같이, 본 발명에 따른 원적외선 방사 조성물은 항균, 방취 기능 및 대전방지 기능이 있어 각종 섬유에 적용시 독특한 천연향기가 발생되어 기분 좋은 향기와 상쾌함 등을 줄 수 있을 뿐 아니라 신체 주위의 각종냄새를 제거하여 쾌적한 생활을 영위할 수 있도록 하고, 기존 원료에 비해 가격이 훨씬 싸서 대중화에 용이함은 물론 중성으로 제조 가능하여 섬유 전 분야에 부작용없이 널리 이용될 수 있는 효과를 갖는다.As described in detail above, the far-infrared radiation composition according to the present invention has antibacterial, deodorizing function, and antistatic function, so that a unique natural fragrance is generated when applied to various fibers to give a pleasant fragrance and freshness as well as surrounding the body. It removes various odors and allows you to live a pleasant life. The price is much cheaper than existing raw materials, so it is easy to popularize and can be manufactured with neutrality.
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| KR20030080352A (en) * | 2002-04-08 | 2003-10-17 | 장시원 | Manufacturing method of far infrared ray radiation ceramic ball |
| KR100403033B1 (en) * | 2001-01-30 | 2003-10-23 | 인따르시아주식회사 | Method for manufacturing multi-functional bra and bra pad |
| KR100717509B1 (en) | 2005-10-05 | 2007-05-16 | 박영웅 | The Antibiotic Plastics and The Products |
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| KR20020072690A (en) * | 2001-03-12 | 2002-09-18 | 주식회사 지엘미디어 | Far infrared radiating paint and method for manufacturing the same |
| KR20030037967A (en) * | 2001-11-07 | 2003-05-16 | 윤선규 | Aquactivated light of laws governing manufacture |
| KR20020074104A (en) * | 2002-08-17 | 2002-09-28 | 주식회사 준일 제네시스 | manufacture method of liquid state composite radiating infrared and heat |
| DE10312549B3 (en) | 2003-03-21 | 2004-08-26 | Hüttinger Elektronik Gmbh + Co. Kg | Power supply for direct current gas discharge equipment has three-phase supply with full-wave rectifier followed by inverter, transformer, second rectifier and second voltage reduction stage |
| KR101310776B1 (en) * | 2013-03-14 | 2013-09-25 | 주식회사 솔라텍코리아 | Far infrared ceramic coatings |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR100403033B1 (en) * | 2001-01-30 | 2003-10-23 | 인따르시아주식회사 | Method for manufacturing multi-functional bra and bra pad |
| KR20030080352A (en) * | 2002-04-08 | 2003-10-17 | 장시원 | Manufacturing method of far infrared ray radiation ceramic ball |
| KR100717509B1 (en) | 2005-10-05 | 2007-05-16 | 박영웅 | The Antibiotic Plastics and The Products |
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