JPWO2019158418A5 - - Google Patents
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- Publication number
- JPWO2019158418A5 JPWO2019158418A5 JP2020540314A JP2020540314A JPWO2019158418A5 JP WO2019158418 A5 JPWO2019158418 A5 JP WO2019158418A5 JP 2020540314 A JP2020540314 A JP 2020540314A JP 2020540314 A JP2020540314 A JP 2020540314A JP WO2019158418 A5 JPWO2019158418 A5 JP WO2019158418A5
- Authority
- JP
- Japan
- Prior art keywords
- hard material
- material particles
- cobalt
- powder
- coated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002245 particle Substances 0.000 claims description 118
- 239000000463 material Substances 0.000 claims description 83
- 239000000843 powder Substances 0.000 claims description 63
- 238000000034 method Methods 0.000 claims description 51
- 229910017052 cobalt Inorganic materials 0.000 claims description 49
- 239000010941 cobalt Substances 0.000 claims description 49
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical group [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 47
- -1 cobalt amine Chemical class 0.000 claims description 36
- 229910021503 Cobalt(II) hydroxide Inorganic materials 0.000 claims description 33
- 238000004519 manufacturing process Methods 0.000 claims description 21
- 238000000576 coating method Methods 0.000 claims description 20
- 239000011248 coating agent Substances 0.000 claims description 19
- 239000000203 mixture Substances 0.000 claims description 17
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 15
- 239000007864 aqueous solution Substances 0.000 claims description 13
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 12
- 150000003839 salts Chemical class 0.000 claims description 11
- 239000000725 suspension Substances 0.000 claims description 11
- 239000001257 hydrogen Substances 0.000 claims description 10
- 229910052739 hydrogen Inorganic materials 0.000 claims description 10
- UONOETXJSWQNOL-UHFFFAOYSA-N tungsten carbide Chemical compound [W+]#[C-] UONOETXJSWQNOL-UHFFFAOYSA-N 0.000 claims description 10
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 8
- 239000000654 additive Substances 0.000 claims description 7
- 230000000996 additive effect Effects 0.000 claims description 7
- 230000009467 reduction Effects 0.000 claims description 7
- 229910021529 ammonia Inorganic materials 0.000 claims description 6
- ASKVAEGIVYSGNY-UHFFFAOYSA-L cobalt(ii) hydroxide Chemical compound [OH-].[OH-].[Co+2] ASKVAEGIVYSGNY-UHFFFAOYSA-L 0.000 claims description 6
- 239000000126 substance Substances 0.000 claims description 6
- 235000010299 hexamethylene tetramine Nutrition 0.000 claims description 4
- 239000004312 hexamethylene tetramine Substances 0.000 claims description 4
- VKYKSIONXSXAKP-UHFFFAOYSA-N hexamethylenetetramine Chemical compound C1N(C2)CN3CN1CN2C3 VKYKSIONXSXAKP-UHFFFAOYSA-N 0.000 claims description 4
- 239000007800 oxidant agent Substances 0.000 claims description 4
- 150000001242 acetic acid derivatives Chemical class 0.000 claims description 3
- 150000003841 chloride salts Chemical class 0.000 claims description 3
- 150000002823 nitrates Chemical class 0.000 claims description 3
- 230000003647 oxidation Effects 0.000 claims description 3
- 238000007254 oxidation reaction Methods 0.000 claims description 3
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims description 3
- 229910052751 metal Inorganic materials 0.000 description 21
- 239000002184 metal Substances 0.000 description 21
- 230000008569 process Effects 0.000 description 21
- 238000009826 distribution Methods 0.000 description 8
- 239000011230 binding agent Substances 0.000 description 6
- 238000005245 sintering Methods 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 230000002776 aggregation Effects 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 5
- 150000001875 compounds Chemical class 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 239000000758 substrate Substances 0.000 description 5
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 4
- 238000005054 agglomeration Methods 0.000 description 4
- 238000002844 melting Methods 0.000 description 4
- 230000008018 melting Effects 0.000 description 4
- 238000001556 precipitation Methods 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 229910052723 transition metal Inorganic materials 0.000 description 4
- 150000003624 transition metals Chemical class 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 3
- JAWGVVJVYSANRY-UHFFFAOYSA-N cobalt(3+) Chemical compound [Co+3] JAWGVVJVYSANRY-UHFFFAOYSA-N 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 150000001247 metal acetylides Chemical class 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 3
- 150000004767 nitrides Chemical class 0.000 description 3
- 230000001590 oxidative effect Effects 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 3
- 229910052721 tungsten Inorganic materials 0.000 description 3
- 239000010937 tungsten Substances 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 2
- 239000011324 bead Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 230000000711 cancerogenic effect Effects 0.000 description 2
- 231100000315 carcinogenic Toxicity 0.000 description 2
- 239000003638 chemical reducing agent Substances 0.000 description 2
- 229910052804 chromium Inorganic materials 0.000 description 2
- 239000011651 chromium Substances 0.000 description 2
- KTVIXTQDYHMGHF-UHFFFAOYSA-L cobalt(2+) sulfate Chemical group [Co+2].[O-]S([O-])(=O)=O KTVIXTQDYHMGHF-UHFFFAOYSA-L 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 238000000635 electron micrograph Methods 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 230000000640 hydroxylating effect Effects 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 238000003801 milling Methods 0.000 description 2
- 229910052750 molybdenum Inorganic materials 0.000 description 2
- 239000011733 molybdenum Substances 0.000 description 2
- 229910052759 nickel Inorganic materials 0.000 description 2
- 229910052758 niobium Inorganic materials 0.000 description 2
- 239000010955 niobium Substances 0.000 description 2
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 2
- 229910052763 palladium Inorganic materials 0.000 description 2
- 238000004663 powder metallurgy Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 229910052715 tantalum Inorganic materials 0.000 description 2
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 description 2
- 239000010936 titanium Substances 0.000 description 2
- 229910052719 titanium Inorganic materials 0.000 description 2
- 238000002604 ultrasonography Methods 0.000 description 2
- 229910052720 vanadium Inorganic materials 0.000 description 2
- GPPXJZIENCGNKB-UHFFFAOYSA-N vanadium Chemical compound [V]#[V] GPPXJZIENCGNKB-UHFFFAOYSA-N 0.000 description 2
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 229910018916 CoOOH Inorganic materials 0.000 description 1
- 239000008186 active pharmaceutical agent Substances 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 239000003570 air Substances 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 239000012736 aqueous medium Substances 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 239000012300 argon atmosphere Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 229910021446 cobalt carbonate Inorganic materials 0.000 description 1
- UFMZWBIQTDUYBN-UHFFFAOYSA-N cobalt dinitrate Chemical group [Co+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O UFMZWBIQTDUYBN-UHFFFAOYSA-N 0.000 description 1
- 229910001981 cobalt nitrate Inorganic materials 0.000 description 1
- 229940044175 cobalt sulfate Drugs 0.000 description 1
- 229910000361 cobalt sulfate Inorganic materials 0.000 description 1
- XLJKHNWPARRRJB-UHFFFAOYSA-N cobalt(2+) Chemical class [Co+2] XLJKHNWPARRRJB-UHFFFAOYSA-N 0.000 description 1
- MEYVLGVRTYSQHI-UHFFFAOYSA-L cobalt(2+) sulfate heptahydrate Chemical compound O.O.O.O.O.O.O.[Co+2].[O-]S([O-])(=O)=O MEYVLGVRTYSQHI-UHFFFAOYSA-L 0.000 description 1
- ZOTKGJBKKKVBJZ-UHFFFAOYSA-L cobalt(2+);carbonate Chemical compound [Co+2].[O-]C([O-])=O ZOTKGJBKKKVBJZ-UHFFFAOYSA-L 0.000 description 1
- OBWXQDHWLMJOOD-UHFFFAOYSA-H cobalt(2+);dicarbonate;dihydroxide;hydrate Chemical compound O.[OH-].[OH-].[Co+2].[Co+2].[Co+2].[O-]C([O-])=O.[O-]C([O-])=O OBWXQDHWLMJOOD-UHFFFAOYSA-H 0.000 description 1
- FXVNMSSSMOVRTC-UHFFFAOYSA-K cobalt(3+);trihydroxide Chemical class [OH-].[OH-].[OH-].[Co+3] FXVNMSSSMOVRTC-UHFFFAOYSA-K 0.000 description 1
- 229910000001 cobalt(II) carbonate Inorganic materials 0.000 description 1
- PKSIZOUDEUREFF-UHFFFAOYSA-N cobalt;dihydrate Chemical compound O.O.[Co] PKSIZOUDEUREFF-UHFFFAOYSA-N 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 238000010017 direct printing Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000007772 electroless plating Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 238000007499 fusion processing Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 150000002429 hydrazines Chemical class 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- TVZISJTYELEYPI-UHFFFAOYSA-N hypodiphosphoric acid Chemical class OP(O)(=O)P(O)(O)=O TVZISJTYELEYPI-UHFFFAOYSA-N 0.000 description 1
- 238000001746 injection moulding Methods 0.000 description 1
- 239000000976 ink Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000007561 laser diffraction method Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 238000001000 micrograph Methods 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 239000003870 refractory metal Substances 0.000 description 1
- 238000000110 selective laser sintering Methods 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 229910021332 silicide Inorganic materials 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP18156802.3A EP3527306A1 (de) | 2018-02-14 | 2018-02-14 | Pulver umfassend beschichtete hartstoffpartikel |
| EP18156802.3 | 2018-02-14 | ||
| PCT/EP2019/052917 WO2019158418A1 (de) | 2018-02-14 | 2019-02-06 | Pulver umfassend beschichtete hartstoffpartikel |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2021513601A JP2021513601A (ja) | 2021-05-27 |
| JPWO2019158418A5 true JPWO2019158418A5 (es) | 2022-02-16 |
| JP7394769B2 JP7394769B2 (ja) | 2023-12-08 |
Family
ID=61258129
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2020540314A Active JP7394769B2 (ja) | 2018-02-14 | 2019-02-06 | 硬質材料粒子、硬質材料粒子の製造方法、硬質材料粒子の使用方法、硬質材料粒子を含む粉末、及び硬質材料粒子を含む粉末の使用方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US11478848B2 (es) |
| EP (2) | EP3527306A1 (es) |
| JP (1) | JP7394769B2 (es) |
| CN (1) | CN111699062B (es) |
| CA (1) | CA3089525C (es) |
| IL (1) | IL275904B2 (es) |
| MX (1) | MX2020007800A (es) |
| RU (1) | RU2763369C1 (es) |
| WO (1) | WO2019158418A1 (es) |
Family Cites Families (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4214895A (en) * | 1979-05-14 | 1980-07-29 | Gte Sylvania Incorporated | Method for producing cobalt metal powder |
| US4218240A (en) * | 1979-05-14 | 1980-08-19 | Gte Products Corporation | Method for producing cobaltic hexammine compounds and cobalt metal powder |
| SU1588503A1 (ru) * | 1988-03-14 | 1990-08-30 | Научно-Исследовательский Институт Композиционных Систем И Покрытий | Способ получени плакированного композиционного порошкового материала |
| SE502754C2 (sv) * | 1994-03-31 | 1995-12-18 | Sandvik Ab | Sätt att framställa belagt hårdämnespulver |
| SE507212C2 (sv) * | 1995-09-29 | 1998-04-27 | Sandvik Ab | Sätt att belägga hårdämnespulver med Co eller Ni genom reduktion med polyol |
| CN1212191A (zh) * | 1997-09-23 | 1999-03-31 | 上海华明高技术（集团）有限公司 | 制造WC/Co复合纳米粉末的方法 |
| SE510749C2 (sv) * | 1997-12-22 | 1999-06-21 | Sandvik Ab | Sätt att framställa ett metallkompositmaterial innehållande hårda partiklar och bindemetall |
| RU2149217C1 (ru) * | 1998-07-17 | 2000-05-20 | Фокина Елена Леонидовна | Способ нанесения металлического покрытия на поверхность порошков и подложек |
| JP2000149941A (ja) | 1998-11-16 | 2000-05-30 | Sumitomo Metal Mining Co Ltd | アルカリ二次電池用水酸化ニッケル粉末の製造方法 |
| DE19962015A1 (de) | 1999-12-22 | 2001-06-28 | Starck H C Gmbh Co Kg | Pulvermischungen bzw. Verbundpulver, Verfahren zu ihrer Herstellung und ihre Verwendung in Verbundwerkstoffen |
| US20030097907A1 (en) * | 2001-11-28 | 2003-05-29 | Carroll Daniel F. | Methods of producing composite powders |
| GB2399824A (en) | 2002-09-21 | 2004-09-29 | Univ Birmingham | Metal coated metallurgical particles |
| KR100528330B1 (ko) * | 2003-02-19 | 2005-11-16 | 삼성전자주식회사 | 무기 분말의 코팅방법 및 이에 의하여 제조된 코팅된무기입자 |
| RU2260500C1 (ru) * | 2004-03-22 | 2005-09-20 | Иркутский институт химии им. А.Е. Фаворского Сибирского отделения Российской академии наук (ИрИХ СО РАН) | Способ получения наноразмерных металлических и металлоксидных частиц |
| CN101090786A (zh) | 2004-12-27 | 2007-12-19 | 优米科尔公司 | 硬质金属用复合粉末 |
| US9403137B2 (en) * | 2005-09-15 | 2016-08-02 | Diamond Innovations, Inc. | Polycrystalline diamond material with extremely fine microstructures |
| AT504319B1 (de) | 2006-09-15 | 2010-03-15 | Wolfram Bergbau Huetten Gmbh | Verfahren zur herstellung von kompositpulvern sowie kompositpulver |
| CN100548539C (zh) * | 2007-09-29 | 2009-10-14 | 中南大学 | 一种超细硬质合金复合粉末的制造方法 |
| CN101186990A (zh) * | 2007-10-19 | 2008-05-28 | 中南大学 | 超细硬质合金包覆粉末及其制造方法 |
| US9187809B2 (en) | 2009-08-04 | 2015-11-17 | Allomet Corporation | Tough coated hard particles consolidated in a tough matrix material |
| WO2011031549A2 (en) | 2009-08-27 | 2011-03-17 | Smith International, Inc. | Method of forming metal deposits on ultrahard materials |
| CN102294473B (zh) | 2011-08-31 | 2013-04-10 | 株洲钻石切削刀具股份有限公司 | TiC/Ti(C,N)-Mo-Ni/Co复合粉末及其制备方法和应用 |
| CN104338935B (zh) * | 2014-10-30 | 2017-01-18 | 赣州有色冶金研究所 | 一种简单快速制备纳米WC-Co复合粉的方法 |
| JP6489315B2 (ja) | 2015-07-03 | 2019-03-27 | 住友金属鉱山株式会社 | コバルト粉の製造方法 |
-
2018
- 2018-02-14 EP EP18156802.3A patent/EP3527306A1/de active Pending
-
2019
- 2019-02-06 WO PCT/EP2019/052917 patent/WO2019158418A1/de unknown
- 2019-02-06 EP EP19702304.7A patent/EP3752305A1/de active Pending
- 2019-02-06 JP JP2020540314A patent/JP7394769B2/ja active Active
- 2019-02-06 CN CN201980012679.7A patent/CN111699062B/zh active Active
- 2019-02-06 US US16/960,419 patent/US11478848B2/en active Active
- 2019-02-06 MX MX2020007800A patent/MX2020007800A/es unknown
- 2019-02-06 IL IL275904A patent/IL275904B2/en unknown
- 2019-02-06 CA CA3089525A patent/CA3089525C/en active Active
- 2019-02-06 RU RU2020127094A patent/RU2763369C1/ru active
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