JPS61232212A - 金属炭化物粉末の製造方法 - Google Patents
金属炭化物粉末の製造方法Info
- Publication number
- JPS61232212A JPS61232212A JP60073777A JP7377785A JPS61232212A JP S61232212 A JPS61232212 A JP S61232212A JP 60073777 A JP60073777 A JP 60073777A JP 7377785 A JP7377785 A JP 7377785A JP S61232212 A JPS61232212 A JP S61232212A
- Authority
- JP
- Japan
- Prior art keywords
- metal
- carbon
- powder
- group
- precipitate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 84
- 239000002184 metal Substances 0.000 title claims abstract description 82
- 239000000843 powder Substances 0.000 title claims abstract description 39
- 238000004519 manufacturing process Methods 0.000 title claims description 16
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 55
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 47
- 150000004703 alkoxides Chemical class 0.000 claims abstract description 30
- 239000002244 precipitate Substances 0.000 claims abstract description 26
- 230000000737 periodic effect Effects 0.000 claims abstract description 20
- 239000002245 particle Substances 0.000 claims abstract description 13
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 239000011261 inert gas Substances 0.000 claims abstract description 5
- 150000002739 metals Chemical class 0.000 claims description 16
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 abstract description 12
- 229910052719 titanium Inorganic materials 0.000 abstract description 6
- 125000003545 alkoxy group Chemical group 0.000 abstract description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 4
- 239000012153 distilled water Substances 0.000 abstract description 4
- 238000009826 distribution Methods 0.000 abstract description 4
- 230000003301 hydrolyzing effect Effects 0.000 abstract description 4
- 229910052804 chromium Inorganic materials 0.000 abstract description 3
- 238000002156 mixing Methods 0.000 abstract description 3
- 229910052758 niobium Inorganic materials 0.000 abstract description 3
- 229910052750 molybdenum Inorganic materials 0.000 abstract description 2
- 239000003960 organic solvent Substances 0.000 abstract description 2
- 238000004381 surface treatment Methods 0.000 abstract description 2
- 229910052726 zirconium Inorganic materials 0.000 abstract description 2
- 229910052720 vanadium Inorganic materials 0.000 abstract 1
- 238000000034 method Methods 0.000 description 24
- 239000010936 titanium Substances 0.000 description 15
- 238000003763 carbonization Methods 0.000 description 10
- 238000006460 hydrolysis reaction Methods 0.000 description 10
- 239000007789 gas Substances 0.000 description 9
- 150000001247 metal acetylides Chemical class 0.000 description 9
- 150000001722 carbon compounds Chemical class 0.000 description 8
- 230000007062 hydrolysis Effects 0.000 description 8
- 229910044991 metal oxide Inorganic materials 0.000 description 8
- 150000004706 metal oxides Chemical class 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 7
- 239000007791 liquid phase Substances 0.000 description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 5
- 229910045601 alloy Inorganic materials 0.000 description 5
- 239000000956 alloy Substances 0.000 description 5
- 239000012071 phase Substances 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 239000000443 aerosol Substances 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 3
- -1 iron group metals Chemical class 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 150000002736 metal compounds Chemical class 0.000 description 3
- 229910000000 metal hydroxide Inorganic materials 0.000 description 3
- 150000004692 metal hydroxides Chemical class 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000003746 solid phase reaction Methods 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 2
- 229910001111 Fine metal Inorganic materials 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 235000011114 ammonium hydroxide Nutrition 0.000 description 2
- 150000001720 carbohydrates Chemical class 0.000 description 2
- 235000014633 carbohydrates Nutrition 0.000 description 2
- 238000010000 carbonizing Methods 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 238000010304 firing Methods 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000001404 mediated effect Effects 0.000 description 2
- 229910001507 metal halide Inorganic materials 0.000 description 2
- 239000011812 mixed powder Substances 0.000 description 2
- 238000004663 powder metallurgy Methods 0.000 description 2
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 2
- 229910010271 silicon carbide Inorganic materials 0.000 description 2
- 239000007790 solid phase Substances 0.000 description 2
- 229910052717 sulfur Inorganic materials 0.000 description 2
- 229910052582 BN Inorganic materials 0.000 description 1
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 229910000997 High-speed steel Inorganic materials 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 229910052581 Si3N4 Inorganic materials 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 238000010306 acid treatment Methods 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- YHWCPXVTRSHPNY-UHFFFAOYSA-N butan-1-olate;titanium(4+) Chemical compound [Ti+4].CCCC[O-].CCCC[O-].CCCC[O-].CCCC[O-] YHWCPXVTRSHPNY-UHFFFAOYSA-N 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 239000011195 cermet Substances 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000005261 decarburization Methods 0.000 description 1
- 229910003460 diamond Inorganic materials 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 229910052735 hafnium Inorganic materials 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 125000000468 ketone group Chemical group 0.000 description 1
- 229910001510 metal chloride Inorganic materials 0.000 description 1
- 150000005309 metal halides Chemical class 0.000 description 1
- 125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- HQVNEWCFYHHQES-UHFFFAOYSA-N silicon nitride Chemical compound N12[Si]34N5[Si]62N3[Si]51N64 HQVNEWCFYHHQES-UHFFFAOYSA-N 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000006104 solid solution Substances 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052715 tantalum Inorganic materials 0.000 description 1
- MTPVUVINMAGMJL-UHFFFAOYSA-N trimethyl(1,1,2,2,2-pentafluoroethyl)silane Chemical compound C[Si](C)(C)C(F)(F)C(F)(F)F MTPVUVINMAGMJL-UHFFFAOYSA-N 0.000 description 1
- 239000012808 vapor phase Substances 0.000 description 1
Landscapes
- Carbon And Carbon Compounds (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP60073777A JPS61232212A (ja) | 1985-04-08 | 1985-04-08 | 金属炭化物粉末の製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP60073777A JPS61232212A (ja) | 1985-04-08 | 1985-04-08 | 金属炭化物粉末の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61232212A true JPS61232212A (ja) | 1986-10-16 |
| JPH0114167B2 JPH0114167B2 (enrdf_load_stackoverflow) | 1989-03-09 |
Family
ID=13527970
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP60073777A Granted JPS61232212A (ja) | 1985-04-08 | 1985-04-08 | 金属炭化物粉末の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61232212A (enrdf_load_stackoverflow) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH02204319A (ja) * | 1989-02-03 | 1990-08-14 | Japan Atom Energy Res Inst | 高融点炭化物超微粉の製造方法 |
| WO1995004703A1 (en) * | 1993-08-09 | 1995-02-16 | The Dow Chemical Company | Method for making submicrometer carbides, submicrometer solid sollution carbides, and the material resulting therefrom |
| WO2006106873A1 (ja) * | 2005-03-30 | 2006-10-12 | Fukuoka Prefecture | 炭化チタン粉末および炭化チタン－セラミックス複合粉末とその製造方法ならびにその炭化チタン粉末の焼結体および炭化チタン－セラミックス複合粉末の焼結体とその製造方法 |
-
1985
- 1985-04-08 JP JP60073777A patent/JPS61232212A/ja active Granted
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH02204319A (ja) * | 1989-02-03 | 1990-08-14 | Japan Atom Energy Res Inst | 高融点炭化物超微粉の製造方法 |
| WO1995004703A1 (en) * | 1993-08-09 | 1995-02-16 | The Dow Chemical Company | Method for making submicrometer carbides, submicrometer solid sollution carbides, and the material resulting therefrom |
| CN1045190C (zh) * | 1993-08-09 | 1999-09-22 | Omg美国公司 | 亚微米碳化物、亚微米碳化物固溶体的制备方法 |
| WO2006106873A1 (ja) * | 2005-03-30 | 2006-10-12 | Fukuoka Prefecture | 炭化チタン粉末および炭化チタン－セラミックス複合粉末とその製造方法ならびにその炭化チタン粉末の焼結体および炭化チタン－セラミックス複合粉末の焼結体とその製造方法 |
| US7915187B2 (en) | 2005-03-30 | 2011-03-29 | Fukuoka Prefecture | Titanium carbide powder and titanium carbide-ceramics composite powder and method for production thereof, and sintered compact from the titanium carbide powder and sintered compact from the titanium carbide/ceramics composite powders and method for production thereof |
| US8148281B2 (en) | 2005-03-30 | 2012-04-03 | Fukuoka Prefecture | Titanium carbide powder and titanium carbide-ceramics composite powder and method for production thereof, and sintered compact from the titanium carbide powder and sintered compact from the titanium carbide/ceramics composite powders and method for production thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0114167B2 (enrdf_load_stackoverflow) | 1989-03-09 |
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