JPS5661353A - Preparation of indole or indole derivative - Google Patents
Preparation of indole or indole derivativeInfo
- Publication number
- JPS5661353A JPS5661353A JP13594079A JP13594079A JPS5661353A JP S5661353 A JPS5661353 A JP S5661353A JP 13594079 A JP13594079 A JP 13594079A JP 13594079 A JP13594079 A JP 13594079A JP S5661353 A JPS5661353 A JP S5661353A
- Authority
- JP
- Japan
- Prior art keywords
- indole
- metal
- hydroxyethylaniline
- pref
- mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- SIKJAQJRHWYJAI-UHFFFAOYSA-N indole Chemical compound 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C1=CC=C2NC=CC2=C1 SIKJAQJRHWYJAI-UHFFFAOYSA-N 0.000 title 2
- 150000002475 indoles Chemical class 0.000 title 1
- LYCAIKOWRPUZTN-UHFFFAOYSA-N glycol Chemical compound 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OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 4
- 229910052751 metal Inorganic materials 0.000 abstract 4
- 239000002184 metal Substances 0.000 abstract 4
- 150000001875 compounds Chemical class 0.000 abstract 3
- MWGATWIBSKHFMR-UHFFFAOYSA-N 2-anilinoethanol Chemical compound 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OCCNC1=CC=CC=C1 MWGATWIBSKHFMR-UHFFFAOYSA-N 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 239000002994 raw material Substances 0.000 abstract 2
- DHZZPKMVVSTYLF-UHFFFAOYSA-N 2-(2-methylanilino)ethanol Chemical compound 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CC1=CC=CC=C1NCCO DHZZPKMVVSTYLF-UHFFFAOYSA-N 0.000 abstract 1
- 150000001413 amino acids Chemical class 0.000 abstract 1
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N aniline Chemical compound 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NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 229910052803 cobalt Inorganic materials 0.000 abstract 1
- 238000010574 gas phase reaction Methods 0.000 abstract 1
- 229910052742 iron Inorganic materials 0.000 abstract 1
- 150000002739 metals Chemical class 0.000 abstract 1
- 229910052759 nickel Inorganic materials 0.000 abstract 1
- 229910052763 palladium Inorganic materials 0.000 abstract 1
- 230000000737 periodic Effects 0.000 abstract 1
- 229910052697 platinum Inorganic materials 0.000 abstract 1
Abstract
PURPOSE: To prepare the titled compound useful as a raw material of perfumery and amino acids, in one step, easily, in an improved yield, from N-β-hydroxyethylaniline available at low cost, by carrying out the reaction in the presence of a catalyst containing a VIII-group metal.
CONSTITUTION: The titled compound is prepared by the gas phase reaction of N-β-hydroxyethylaniline or its nucleus-substituted derivative, e.g. N-β-hydroxyethyl-o-toluidine in the presence of a catalyst comprising a metal of the VIII group of the periodic table, i.e. Fe, Co, Ni, Pd, Pt, etc., a mixture of two or more of the above metals, or a mixture of the metal and other compounds, and pref. in the presence of ethylene glycol and/or aniline. The molar ratio of ethylene glycol to the raw material is 0.01W10 to 1, pref. 0.1W1 to 1.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP13594079A JPS6210984B2 (en) | 1979-10-23 | 1979-10-23 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP13594079A JPS6210984B2 (en) | 1979-10-23 | 1979-10-23 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5661353A true JPS5661353A (en) | 1981-05-26 |
| JPS6210984B2 JPS6210984B2 (en) | 1987-03-10 |
Family
ID=15163392
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP13594079A Expired JPS6210984B2 (en) | 1979-10-23 | 1979-10-23 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6210984B2 (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5832863A (en) * | 1981-08-19 | 1983-02-25 | Mitsui Toatsu Chem Inc | Preparation of indoles |
| JPS5910565A (en) * | 1982-07-08 | 1984-01-20 | Mitsui Toatsu Chem Inc | Preparation of indole compound |
-
1979
- 1979-10-23 JP JP13594079A patent/JPS6210984B2/ja not_active Expired
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5832863A (en) * | 1981-08-19 | 1983-02-25 | Mitsui Toatsu Chem Inc | Preparation of indoles |
| JPH0243736B2 (en) * | 1981-08-19 | 1990-10-01 | Mitsui Toatsu Chemicals | |
| JPS5910565A (en) * | 1982-07-08 | 1984-01-20 | Mitsui Toatsu Chem Inc | Preparation of indole compound |
| JPS6356222B2 (en) * | 1982-07-08 | 1988-11-07 | Mitsui Toatsu Chemicals |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6210984B2 (en) | 1987-03-10 |
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