JPS56110672A - Preparation of indole or indole derivative - Google Patents
Preparation of indole or indole derivativeInfo
- Publication number
- JPS56110672A JPS56110672A JP1199880A JP1199880A JPS56110672A JP S56110672 A JPS56110672 A JP S56110672A JP 1199880 A JP1199880 A JP 1199880A JP 1199880 A JP1199880 A JP 1199880A JP S56110672 A JPS56110672 A JP S56110672A
- Authority
- JP
- Japan
- Prior art keywords
- indole
- magnesium oxide
- aniline
- ethylene glycol
- catalyst containing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- SIKJAQJRHWYJAI-UHFFFAOYSA-N indole Chemical compound 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C1=CC=C2NC=CC2=C1 SIKJAQJRHWYJAI-UHFFFAOYSA-N 0.000 title abstract 4
- 150000002475 indoles Chemical class 0.000 title abstract 2
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Chemical compound 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[Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 abstract 6
- LYCAIKOWRPUZTN-UHFFFAOYSA-N glycol Chemical compound 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OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 4
- 239000000395 magnesium oxide Substances 0.000 abstract 3
- -1 aniline compound Chemical class 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- 239000002994 raw material Substances 0.000 abstract 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicium dioxide Chemical compound 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O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 2
- 150000001413 amino acids Chemical class 0.000 abstract 1
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N aniline Chemical compound 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NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 abstract 1
- 239000003610 charcoal Substances 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000007789 gas Substances 0.000 abstract 1
- 239000007792 gaseous phase Substances 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 239000007791 liquid phase Substances 0.000 abstract 1
- RZXMPPFPUUCRFN-UHFFFAOYSA-N p-toluidine Chemical compound 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CC1=CC=C(N)C=C1 RZXMPPFPUUCRFN-UHFFFAOYSA-N 0.000 abstract 1
- 239000012071 phase Substances 0.000 abstract 1
- 239000000377 silicon dioxide Substances 0.000 abstract 1
Abstract
PURPOSE: To prepare the high-purity titled compound useful as a synthetic raw material of perfumery and amino acids, in one step and high selectivity, by reacting an aniline compound with ethylene glycol as low-cost raw materials in the presence of a catalyst containing magnesium oxide.
CONSTITUTION: An aniline compound (e.g. aniline, p-toluidine, etc.) is reacted with ethylene glycol in the presence of a catalyst containing magnesium oxide (e.g. magnesium oxide supported by silica carrer or by active charcoal) to obtain indole or an indole derivative. The reaction can be carried out in gaseous phase, liquid phase, or a mixed phase of gas and liquid. The reaction temperature is 200W 500°C, pref. 250W400°C.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP55011998A JPS6210985B2 (en) | 1980-02-05 | 1980-02-05 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP55011998A JPS6210985B2 (en) | 1980-02-05 | 1980-02-05 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS56110672A true JPS56110672A (en) | 1981-09-01 |
| JPS6210985B2 JPS6210985B2 (en) | 1987-03-10 |
Family
ID=11793248
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP55011998A Expired JPS6210985B2 (en) | 1980-02-05 | 1980-02-05 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6210985B2 (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5862160A (en) * | 1981-10-08 | 1983-04-13 | Mitsui Toatsu Chem Inc | Separation of indole |
| JPS58225061A (en) * | 1982-06-24 | 1983-12-27 | Mitsui Toatsu Chem Inc | Preparation of indole compound |
| US4474969A (en) * | 1981-08-25 | 1984-10-02 | Mitsui Toatsu Chemicals, Incorporated | Preparation process of indole |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0357488U (en) * | 1989-10-06 | 1991-06-03 |
-
1980
- 1980-02-05 JP JP55011998A patent/JPS6210985B2/ja not_active Expired
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4474969A (en) * | 1981-08-25 | 1984-10-02 | Mitsui Toatsu Chemicals, Incorporated | Preparation process of indole |
| JPS5862160A (en) * | 1981-10-08 | 1983-04-13 | Mitsui Toatsu Chem Inc | Separation of indole |
| JPS6150945B2 (en) * | 1981-10-08 | 1986-11-06 | Mitsui Toatsu Chemicals | |
| JPS58225061A (en) * | 1982-06-24 | 1983-12-27 | Mitsui Toatsu Chem Inc | Preparation of indole compound |
| US4937353A (en) * | 1982-06-24 | 1990-06-26 | Mitsui Toatsu Chemicals, Incorporated | Preparation process for indoles |
| JPH0359064B2 (en) * | 1982-06-24 | 1991-09-09 | Mitsui Toatsu Chemicals |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6210985B2 (en) | 1987-03-10 |
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