JPH11240814A - Insect repellent - Google Patents
Insect repellentInfo
- Publication number
- JPH11240814A JPH11240814A JP4204198A JP4204198A JPH11240814A JP H11240814 A JPH11240814 A JP H11240814A JP 4204198 A JP4204198 A JP 4204198A JP 4204198 A JP4204198 A JP 4204198A JP H11240814 A JPH11240814 A JP H11240814A
- Authority
- JP
- Japan
- Prior art keywords
- insect repellent
- clara
- water
- dissolving
- present
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Description
【０００１】[0001]
【発明の属する技術分野】本発明は虫忌避剤に関し、特
にイエ白蟻などの害虫類を忌避することのできる虫忌避
剤に関する。TECHNICAL FIELD The present invention relates to an insect repellent, and more particularly to an insect repellent capable of repelling pests such as house termites.
【０００２】[0002]
【従来の技術】従来、イエ白蟻、コガネムシ、毛虫など
の害虫類を駆除するために、人工的に合成された殺虫剤
や殺菌剤などを用いて駆除や防除を行なっている。例え
ば、有機燐剤、カルバメート剤、ピレスロイド系薬剤等
の合成薬剤が多用されている。しかし、これら合成薬剤
は、劇物や毒物に指定されているものが多く、また水質
汚濁性や、残留性にも留意する必要がある。さらに近年
においては、毒性以外に環境ホルモン性も問題となり、
合成薬剤の使用は年々その使用が制限されつつある。2. Description of the Related Art Conventionally, in order to exterminate pests such as house termites, scarabs and caterpillars, extermination and control have been carried out using artificially synthesized insecticides and fungicides. For example, synthetic agents such as organic phosphorus agents, carbamate agents, and pyrethroids are frequently used. However, many of these synthetic chemicals are specified as deleterious substances or poisonous substances, and it is necessary to pay attention to water pollution and residual properties. In recent years, in addition to toxicity, environmental hormones have become a problem,
The use of synthetic drugs is being restricted year by year.
【０００３】一方、クララは、茎葉に独特の弱い臭気が
あるクララ属マメ科の植物で、本州、四国、および朝鮮
半島、中国、モンゴル等に分布する多年草植物である。
茎は直立し、下部はやや木質で円柱状、葉は互生し、有
柄で奇数羽状複葉、花期は６〜７月で頂生は総状花序に
淡黄色、まれに帯紫色の蝶形花をつける。また、根は７
〜９月に掘り下げられる。クララは古くから漢方薬とし
て知られ、また、抗菌・防腐剤又は化粧料として、ある
いは外用駆虫剤として用いられている。例えば、このよ
うなクララの成分を含む害虫、害獣忌避剤として漢方農
芸用薬剤の製造方法が知られている（特公平５−２９２
０１号公報）。この農芸用薬剤は、クララの根のクジ
ン、オウバクおよびダイオウの通性嫌気的醗酵物を有効
成分とするものである。On the other hand, Clara is a perennial plant belonging to the genus Clara belonging to the genus Clara having a peculiar weak odor in the foliage and distributed in Honshu, Shikoku, the Korean Peninsula, China, Mongolia and the like.
Stem erect, lower part somewhat woody, columnar, leaves alternate, stalked, odd-numbered, pinnate compound, flowering from June to July, apex pale yellow in inflorescence, rarely violet butterfly Attach The root is 7
It will be dug up in September. Clara has long been known as a herbal medicine, and has been used as an antibacterial / preservative or cosmetic, or as an external anthelmintic. For example, as a pest and vermin repellent containing such a component of Clara, a method for producing a Chinese medicine agricultural chemical is known (Japanese Patent Publication No. 5-292).
No. 01). This agricultural chemical contains as an active ingredient a facultatively anaerobic fermentation product of larvae of larva root, oval and rhubarb.
【０００４】[0004]
【発明が解決しようとする課題】しかしながら、有機燐
剤やカルバメート剤などの合成薬剤は、除草剤、殺虫
剤、殺菌剤類などの種類別に多種多用あり、いずれも人
間や環境に対して安全とはいえないという問題がある。
また、殺虫剤の場合、害虫に適応して駆除性や防除性を
向上させるために、散布回数は増える傾向にあり、防除
コストが向上するという問題がある。However, there are various types of synthetic agents such as organic phosphorus agents and carbamate agents depending on the type of herbicide, insecticide, fungicide, etc., all of which are safe for humans and the environment. There is a problem that cannot be said.
In addition, in the case of insecticides, the frequency of application tends to increase in order to improve the extermination property and the control property by adapting to the pest, and there is a problem that the control cost is increased.
【０００５】クララの成分を含む従来の漢方農芸用薬剤
は、オウバクおよびダイオウとを必須共存成分とし、さ
らに醗酵物であり、主に植物の成育促進を目的とするの
で、ゴルフ場など駆除剤が大量に使用される場合での、
害虫駆除に対しては十分でないという問題がある。[0005] Conventional Chinese herbal agrochemicals containing the components of Clara are composed of essential ingredients such as oak and rhubarb, and are fermented products, and are mainly used for promoting plant growth. When used in large quantities,
There is a problem that pest control is not enough.
【０００６】本発明はこのような問題に対処するために
なされたもので、人間や環境に対して安全で、かつ防除
コストを下げることができる虫忌避剤を提供することを
目的とする。[0006] The present invention has been made to address such problems, and has as its object to provide an insect repellent that is safe for humans and the environment and that can reduce the control cost.
【０００７】[0007]
【課題を解決するための手段】請求項１の虫忌避剤は、
クララを水に加熱溶解してなる液を含有することを特徴
とする。The insect repellent of claim 1 is
It contains a liquid obtained by heating and dissolving Clara in water.
【０００８】請求項２の虫忌避剤は、クララと生薬とを
水に加熱溶解してなる液を含有することを特徴とする。[0008] The insect repellent of claim 2 is characterized in that it contains a liquid obtained by heating and dissolving Clara and a crude drug in water.
【０００９】請求項３の虫忌避剤は、クララ、または、
クララおよび生薬とを水に加熱溶解してなる液に、さら
に少なくとも親水性有機溶媒を含有することを特徴とす
る。The insect repellent of claim 3 is Clara or
A liquid obtained by heating and dissolving Clara and a crude drug in water further contains at least a hydrophilic organic solvent.
【００１０】本発明の虫忌避剤における虫は、草木、樹
木および農林産物を含む農作物を害する虫類をいい、線
虫、ダニ、昆虫、ねずみ、その他の害虫をいう。具体的
には、ガ類などの鱗翅目、シバオサゾウムシ・コガネ虫
類などの鞘翅目、カメムシ・カイガラムシ・ウンカ類な
どの半翅目、ケラなどの直翅目、クロヤマアリなどの膜
翅目、毛虫・ミノムシなどの樹木害虫類、ヤマト白蟻な
どのイエ白蟻類、ミミズ類などをいう。これらの害虫は
成虫、幼虫あるいは卵であってもよい。[0010] The insects in the insect repellent of the present invention refer to insects that damage agricultural crops including plants, trees, and agricultural and forestry products, and include nematodes, mites, insects, rats, and other pests. Specifically, Lepidoptera such as moths, Coleoptera such as Shibaosoruzoushi and Scarabaeidae, Hemiptera such as stink bugs, scales and planthoppers, Orthoptera such as Kera, Hymenoptera such as Black ant, It refers to tree pests such as caterpillars and bugs, house termites such as Yamato termite, earthworms, and the like. These pests may be adults, larvae or eggs.
【００１１】本発明の虫忌避剤は、天然物であるクララ
を主原料としているので、人間に対して安全であり、環
境を破壊することがない。また、害虫類の幼虫や成虫が
本発明の虫忌避剤を吸引すると、咀嚼機能が鈍くなり、
さらには食欲を減退させて衰弱する。その結果、農産
物、樹木または植物の害虫による食害を大きく減少させ
るとともに、病原菌の寄生媒介がなくなるので、病害か
らの被害も大きく減少させることができる。[0011] The insect repellent of the present invention is based on Clara, which is a natural product, and is safe for humans and does not destroy the environment. Further, when the pest larva or adult sucks the insect repellent of the present invention, the mastication function becomes dull,
In addition, it reduces appetite and weakens. As a result, it is possible to greatly reduce the damage caused by pests of agricultural products, trees, or plants, and to eliminate the parasitism of pathogenic bacteria, thereby greatly reducing damage from diseases.
【００１２】[0012]
【発明の実施の形態】本発明に係るクララは、その根、
根茎または葉などを乾燥して使用する。乾燥の条件とし
ては、クララを粉末状に粉砕できる程度の水分量となる
まで乾燥する。乾燥は自然乾燥が好ましい。自然乾燥さ
れたクララを粉砕して濃度 30 〜 75重量％で加熱溶解
する。加熱溶解は、クララの乾燥粉末が均一な液状、あ
るいは均一な分散液状となる条件であればよい。好まし
くは、圧力釜を用いて加圧下に加熱溶解する。BEST MODE FOR CARRYING OUT THE INVENTION Clara according to the present invention has a root,
Dry the rhizome or leaves and use. Drying conditions are such that the Clara is dried until it has a water content that can be pulverized into a powder. Drying is preferably natural drying. The naturally dried Clara is crushed and dissolved by heating at a concentration of 30 to 75% by weight. The heating and dissolving may be performed under such conditions that the dry powder of Clara becomes a uniform liquid or a uniform dispersed liquid. Preferably, the mixture is heated and melted under pressure using a pressure cooker.
【００１３】本発明の虫忌避剤は、この加熱溶解した液
体を冷却後濾過して、そのままを用途別に希釈して用い
ることができる。また、さらに親水性有機溶媒を添加し
て調整することにより、より害虫忌避性能を向上させる
ことができる。忌避薬液の浸透性および保持性などが向
上するためと考えられる。親水性有機溶媒としては、メ
タノール、エタノール、１，３−ブチレングリコール、
プロピレングリコール、ｎ−ブタノール、アセトン、な
どを用いることができる。親水性有機溶媒の添加量はク
ララの溶解水溶液 100g に対して 20 〜50g 、好ましく
は 25 〜35g である。また、親水性有機溶媒の一部に補
助添加剤として松脂を加えてもよい。なお、圧力釜を用
いての加圧溶解時に親水性有機溶媒と水との混合溶媒を
用いてもよい。この場合、加熱溶解時間を短縮すること
ができる。The insect repellent of the present invention can be used by cooling the heated and dissolved liquid, filtering the liquid after cooling, and diluting the liquid as it is for each use. Further, by adding and adjusting a hydrophilic organic solvent, the pest repelling performance can be further improved. It is considered that permeability and retention of the repellent solution are improved. As the hydrophilic organic solvent, methanol, ethanol, 1,3-butylene glycol,
Propylene glycol, n-butanol, acetone, and the like can be used. The amount of the hydrophilic organic solvent to be added is 20 to 50 g, preferably 25 to 35 g, per 100 g of the aqueous solution of Clara. Further, rosin may be added to a part of the hydrophilic organic solvent as an auxiliary additive. In addition, you may use the mixed solvent of a hydrophilic organic solvent and water at the time of pressure dissolution using a pressure cooker. In this case, the heating and melting time can be reduced.
【００１４】クララ単独のみならず、クララおよび生薬
を水に加熱溶解しても本発明の害虫忌避剤を得ることが
できる。本発明に係る生薬は、漢方薬として一般に知ら
れている薬草類をいい、ニンニク、ナンテン、ナツメ、
カッコン、クズ、オウゴン、タイソウ、ショウキョウ、
カンゾウ、チンピ、ウンシュウミカン、トウキ、センキ
ュウ、トウガラシ、オウバク、ダイオウ等あるいはこれ
らの近縁植物を挙げることができる。これらの中で好ま
しい生薬は、ニンニク、ナンテン、ナツメ、ウンシュウ
ミカンである。The pest repellent of the present invention can be obtained by heating and dissolving not only Clara alone but also Clara and a crude drug in water. The crude drug according to the present invention refers to herbs generally known as Chinese herbal medicine, garlic, nanten, jujube,
Parentheses, splinters, ogre, tyres, ginger,
Licorice, chimpanzee, Satsuma Mandarin, Touki, Senkyu, Pepper, Oubak, Rhubarb, and the like, or their closely related plants. Among these, the preferred crude drugs are garlic, nanten, jujube and unshiu.
【００１５】これらの生薬は、クララと同様に乾燥して
使用する。乾燥状態での配合比率は、重量比率でクララ
1に対して 0.05 〜2 の範囲であることが好ましい。こ
の範囲であると、クララ単独よりもより多くの害虫に対
する忌避性能を向上させることができる。生薬が配合さ
れた虫忌避剤の製造は、クララ単独の場合と同一の溶解
条件で得ることができる。また、親水性有機溶媒および
補助剤としての松脂を同様に添加することが好ましい。[0015] These crude drugs are dried and used like Clara. The mixing ratio in the dry state is Clara by weight.
It is preferably in the range of 0.05 to 2 with respect to 1. Within this range, repellency against more pests than Clara alone can be improved. Production of an insect repellent containing a crude drug can be obtained under the same dissolution conditions as in the case of Clara alone. It is also preferable to add a hydrophilic organic solvent and rosin as an auxiliary in the same manner.
【００１６】本発明の虫忌避剤の使用は、忌避あるいは
駆除の対象によっては、上述の加熱溶解液、あるいは親
水性有機溶媒および松脂で調整した液そのままを使用す
ることができる。また、上述の加熱溶解液あるいは親水
性有機溶媒等で調整した液を 5〜10000倍に水で希釈し
て用いることができる。好ましい希釈倍率は 50 〜1000
倍である。なお、本発明の害虫忌避剤は濃縮乾燥して、
ペースト状、ゲル状、粉末状として用いることもでき
る。The insect repellent of the present invention can be used in the form of the above-mentioned heat-dissolved solution or a solution prepared with a hydrophilic organic solvent and rosin depending on the object of repelling or controlling. Further, the above-mentioned heated solution or a solution prepared with a hydrophilic organic solvent or the like can be used after diluting with water 5 to 10,000 times. Preferred dilution ratio is 50-1000
It is twice. The pest repellent of the present invention is concentrated and dried,
It can be used as a paste, gel, or powder.
【００１７】虫忌避剤の使用方法としては、特に制限な
く、希釈液を忌避あるいは駆除対象物に直接散布、潅注
または潅水したりすることができる。または、希釈液の
原液を直接塗布することができる。散布量としては、例
えば 500倍に希釈した虫忌避剤を駆除対象物に 0.1〜5
リットル／ｍ2 、好ましくは 0.5〜3 リットル／ｍ2 の
範囲である。散布回数は、駆除対象物の種類によっても
異なるが 3〜5 ／年が好ましい。本発明の虫忌避剤は、
害虫に対する忌避効果が高いので、この散布回数で十分
に例えばヤマト白蟻の害から樹木を守ることができる。The method for using the insect repellent is not particularly limited, and the diluent can be directly sprayed, irrigated or watered on the object to be repelled or controlled. Alternatively, a stock solution of a diluent can be directly applied. The spraying amount may be, for example, 0.1 to 5
Liters / m 2 , preferably in the range of 0.5 to 3 liters / m 2 . The frequency of spraying varies depending on the type of the object to be controlled, but is preferably 3 to 5 / year. The insect repellent of the present invention,
Since the repellent effect against pests is high, trees can be sufficiently protected from the damage of, for example, Yamato termites by this number of times of application.
【００１８】[0018]
【実施例】実施例１ 重量比で 1：1 に配合した乾燥クララとニンニクとを水
に約 60 重量％の割合で圧力釜を用いて 100℃以上の温
度で 7〜8 時間加熱溶解した。加熱溶解後室温に冷却
し、溶解液 100g に対してアルコールを 30gおよび松脂
を 5g 配合した後、フィルタープレスを用いて濾過して
虫忌避剤の原液を得た。EXAMPLES Example 1 Dried clara and garlic mixed at a weight ratio of 1: 1 were heated and dissolved in water at a temperature of at least 100 ° C. for 7 to 8 hours using a pressure cooker at a ratio of about 60% by weight. After heating and dissolving, the mixture was cooled to room temperature, 30 g of alcohol and 5 g of rosin were mixed with 100 g of the solution, and then filtered using a filter press to obtain a stock solution of an insect repellent.
【００１９】得られた原液を 50 倍から 300倍に水で希
釈して虫忌避能力を評価した。評価は、日本保存協会規
格第１３号の室内試験方法に基づき、土壌処理用防蟻剤
の室内効力試験により行なった。評価結果を表１に示
す。なお、耐候処理は処理土壌を 40 ℃の通風乾燥機内
に 28 日間保った、また、土壌処理操作は希釈溶液 3ml
を 12gの土壌に加えて攪拌した。The obtained stock solution was diluted 50-fold to 300-fold with water, and the insect repellent ability was evaluated. The evaluation was performed based on the indoor test method of Japanese Conservation Association Standard No. 13 by the indoor efficacy test of the termiticide for soil treatment. Table 1 shows the evaluation results. For the weathering treatment, the treated soil was kept in a ventilation dryer at 40 ° C for 28 days.
Was added to 12 g of soil and stirred.
【表１】 表１に示すように、本発明の虫忌避剤は、 300倍希釈液
であっても比較例として示した無処理に比較して白蟻忌
避能力が極めて優れていた。[Table 1] As shown in Table 1, the insect repellent of the present invention was extremely excellent in termite repelling ability even in a 300-fold diluted solution as compared with the untreated treatment shown as a comparative example.
【００２０】次に、木部処理剤の防蟻効力試験を、日本
白蟻対策協会ＪＴＣＡＳ−第１号総合試験に準じて行な
った。供試虫忌避剤は 50 倍希釈液を用い、耐候処理な
しで行なった。評価結果を表２に示す。Next, a termite-proofing effect test of the xylem-treating agent was performed according to the Japanese Termite Countermeasures Association, JTCAS-No. 1 comprehensive test. The test insect repellent was used in a 50-fold dilution without any weathering treatment. Table 2 shows the evaluation results.
【表２】 表２に示すように、本発明の虫忌避剤は、比較例として
示した無処理に比較して防蟻効果が極めて優れていた。[Table 2] As shown in Table 2, the insect repellent of the present invention was extremely excellent in termite-controlling effects as compared with the untreated treatment shown as a comparative example.
【００２１】この原液を 500倍に水で希釈してゴルフク
ラブ場に散布したところ、ヤマト白蟻の害がみられず、
また、本発明の虫忌避剤を使用しない場合に比較して、
農薬の使用量および散布回数を、約１／５に低減するこ
とができた。When this undiluted solution was diluted 500 times with water and sprayed on a golf club, no harm of Yamato termites was found.
Also, compared to the case where the insect repellent of the present invention is not used,
The amount of pesticide used and the frequency of application could be reduced to about 1/5.
【００２２】実施例２ 乾燥クララのみを水に加熱溶解する以外は、実施例１と
同一の条件方法で虫忌避剤を得た。得られた原液を 500
倍に水で希釈してゴルフクラブ場に散布したところ、ヤ
マト白蟻の害がみられず、また、本発明の虫忌避剤を使
用しない場合に比較して、農薬の使用量および散布回数
を、約１／４に低減することができた。Example 2 An insect repellent was obtained in the same manner as in Example 1, except that only dried clara was dissolved in water by heating. 500 of the stock solution obtained
When diluted with water twice and sprayed on a golf club, no harm of Yamato termites was observed, and the amount of pesticide used and the number of times of spraying were compared with the case where the insect repellent of the present invention was not used. It could be reduced to about 1/4.
【００２３】[0023]
【発明の効果】本発明の虫忌避剤は、クララを水に加熱
溶解してなる液を含有するので、人体に安全で環境を汚
染しない虫忌避剤を得ることができる。また、さらに生
薬を配合することにより、より広範囲の害虫を忌避する
ことができる。さらに、親水性有機溶媒を含有すること
により、害虫忌避性能がより向上する。Since the insect repellent of the present invention contains a liquid obtained by heating and dissolving Clara in water, an insect repellent that is safe for the human body and does not pollute the environment can be obtained. Further, by blending a crude drug, a wider range of pests can be repelled. Further, by containing a hydrophilic organic solvent, pest repellent performance is further improved.
Claims (3)
する虫忌避剤。An insect repellent comprising a liquid obtained by heating and dissolving Clara in water.
なる液を含有する虫忌避剤。2. An insect repellent containing a liquid obtained by heating and dissolving Clara and herbs in water.
水に加熱溶解してなる液に、さらに少なくとも親水性有
機溶媒を含有する虫忌避剤。3. An insect repellent comprising Clara or a liquid obtained by dissolving Clara and a crude drug in water, further comprising at least a hydrophilic organic solvent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP04204198A JP3716092B2 (en) | 1998-02-24 | 1998-02-24 | Insect repellent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP04204198A JP3716092B2 (en) | 1998-02-24 | 1998-02-24 | Insect repellent |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH11240814A true JPH11240814A (en) | 1999-09-07 |
| JP3716092B2 JP3716092B2 (en) | 2005-11-16 |
Family
ID=12625062
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP04204198A Expired - Fee Related JP3716092B2 (en) | 1998-02-24 | 1998-02-24 | Insect repellent |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP3716092B2 (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003321315A (en) * | 2002-04-24 | 2003-11-11 | Hiromi Nishii | Plant extract-formulated liquid agent |
| JP2009035503A (en) * | 2007-07-31 | 2009-02-19 | Univ Kurume | Noxious organism repelling sheet or paper |
-
1998
- 1998-02-24 JP JP04204198A patent/JP3716092B2/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003321315A (en) * | 2002-04-24 | 2003-11-11 | Hiromi Nishii | Plant extract-formulated liquid agent |
| JP2009035503A (en) * | 2007-07-31 | 2009-02-19 | Univ Kurume | Noxious organism repelling sheet or paper |
Also Published As
| Publication number | Publication date |
|---|---|
| JP3716092B2 (en) | 2005-11-16 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US8133921B2 (en) | Edible plant extract based insecticidal composition | |
| AU2019231662B2 (en) | Insect repellent and insecticide | |
| KR101270630B1 (en) | The composition comprising the extraction or fraction of oak vinegar having insect resistance or insecticidal activities for protection of cultural heritage | |
| AU732614B2 (en) | Ant spray containing D-limonene and methods of making and using same | |
| JP2009046433A (en) | Disease and insect pest-controlling agent for crop of fruit and vegetable, and method and apparatus for controlling disease and insect pest in greenhouse installation | |
| KR101692667B1 (en) | Mosquito repelling composition and manufacturing method thereof, and method of manufacturing water paint using the said composition and water paint produced by thereof method | |
| JPH05213711A (en) | Agent for suppressing physiological activity | |
| US6784211B1 (en) | Ant spray containing d-limonene and methods of making and using the same | |
| KR101632246B1 (en) | Pesticides using the Insect flower powder or sludge and manufacture method thereof | |
| JP3716092B2 (en) | Insect repellent | |
| KR100644750B1 (en) | Method for producing insect natual extract | |
| KR20220099794A (en) | Insecitcide Composition comprising complex extracts of Tanacetum cinerariifolium, Agastache rugosa, and Gaultheria procumbens | |
| CN105028536A (en) | Compound botanical insecticide for mosquito larvae control, preparation method therefor and applications thereof | |
| KR102384372B1 (en) | Composition for Pesticide Control for Garden Crops Using Plant Extracts and Method of Preparing the same | |
| US20020031538A1 (en) | Light activateable natural pesticide formulations | |
| CN112400908B (en) | Medicament composition for preventing and treating rhinoceros | |
| KR100710054B1 (en) | Insecticide composite for tetranyhus urticae | |
| KR20140118365A (en) | boranical insecticide Composition and preparing method thereof | |
| WO2022156882A1 (en) | Formulations containing cyclodextrin and fatty acids for controlling and repelling insects with improved effect | |
| JP2005179328A (en) | Neem bark acid benz repellent without containing agrochemical | |
| KR20230027736A (en) | Insecticide and antibacterial composition comprising pyrethrum extract and graphene as active ingredients, and method for manufacturing the same | |
| KR20220099797A (en) | Red mite acaricidal composition comprising complex extracts of Tanacetum cinerariifolium, Agastache rugosa, and Gaultheria procumbens | |
| CN1206559A (en) | Pesticide capable of killing beetle and ladybug and its preparation method | |
| JPH04321613A (en) | Insect pest repellent | |
| KR101265868B1 (en) | Simultaneous Controlling Agent for Rice Pests Comprising Botanical Extract and Controlling Method Using The Same |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A977 | Report on retrieval |
Free format text: JAPANESE INTERMEDIATE CODE: A971007 Effective date: 20050208 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20050215 |
|
| A521 | Written amendment |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20050418 |
|
| A02 | Decision of refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A02 Effective date: 20050517 |
|
| A521 | Written amendment |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20050715 |
|
| A911 | Transfer of reconsideration by examiner before appeal (zenchi) |
Free format text: JAPANESE INTERMEDIATE CODE: A911 Effective date: 20050801 |
|
| TRDD | Decision of grant or rejection written | ||
| A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20050823 |
|
| A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20050829 |
|
| R150 | Certificate of patent or registration of utility model |
Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20080902 Year of fee payment: 3 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20090902 Year of fee payment: 4 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20090902 Year of fee payment: 4 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20100902 Year of fee payment: 5 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20110902 Year of fee payment: 6 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20120902 Year of fee payment: 7 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20120902 Year of fee payment: 7 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20130902 Year of fee payment: 8 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| LAPS | Cancellation because of no payment of annual fees |