JPH0460467B2 - - Google Patents
Info
- Publication number
- JPH0460467B2 JPH0460467B2 JP16125685A JP16125685A JPH0460467B2 JP H0460467 B2 JPH0460467 B2 JP H0460467B2 JP 16125685 A JP16125685 A JP 16125685A JP 16125685 A JP16125685 A JP 16125685A JP H0460467 B2 JPH0460467 B2 JP H0460467B2
- Authority
- JP
- Japan
- Prior art keywords
- dimethacryloylcystamine
- mol
- added
- cystamine
- bond
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- ZFNPCJYXCNZHDI-UHFFFAOYSA-N 2-methyl-n-[2-[2-(2-methylprop-2-enoylamino)ethyldisulfanyl]ethyl]prop-2-enamide Chemical compound CC(=C)C(=O)NCCSSCCNC(=O)C(C)=C ZFNPCJYXCNZHDI-UHFFFAOYSA-N 0.000 claims description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 9
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 8
- 229920000642 polymer Polymers 0.000 description 7
- 239000000126 substance Substances 0.000 description 7
- 238000004458 analytical method Methods 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 239000000178 monomer Substances 0.000 description 4
- 238000000862 absorption spectrum Methods 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- OOTFVKOQINZBBF-UHFFFAOYSA-N cystamine Chemical compound CCSSCCN OOTFVKOQINZBBF-UHFFFAOYSA-N 0.000 description 3
- 229940099500 cystamine Drugs 0.000 description 3
- VHRYZQNGTZXDNX-UHFFFAOYSA-N methacryloyl chloride Chemical compound CC(=C)C(Cl)=O VHRYZQNGTZXDNX-UHFFFAOYSA-N 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- WJFKNYWRSNBZNX-UHFFFAOYSA-N 10H-phenothiazine Chemical compound C1=CC=C2NC3=CC=CC=C3SC2=C1 WJFKNYWRSNBZNX-UHFFFAOYSA-N 0.000 description 2
- 150000001408 amides Chemical class 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 229920006037 cross link polymer Polymers 0.000 description 2
- 238000007033 dehydrochlorination reaction Methods 0.000 description 2
- 239000010410 layer Substances 0.000 description 2
- 239000012044 organic layer Substances 0.000 description 2
- 229950000688 phenothiazine Drugs 0.000 description 2
- NGDIAZZSCVVCEW-UHFFFAOYSA-M sodium;butyl sulfate Chemical compound [Na+].CCCCOS([O-])(=O)=O NGDIAZZSCVVCEW-UHFFFAOYSA-M 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- UYRFJJJSEKLZRY-UHFFFAOYSA-N 4-pyridin-3-ylbutanimidamide Chemical compound NC(=N)CCCC1=CC=CN=C1 UYRFJJJSEKLZRY-UHFFFAOYSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- HFBMWMNUJJDEQZ-UHFFFAOYSA-N acryloyl chloride Chemical compound ClC(=O)C=C HFBMWMNUJJDEQZ-UHFFFAOYSA-N 0.000 description 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 239000003431 cross linking reagent Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000000921 elemental analysis Methods 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- -1 methacrylic acid halide Chemical class 0.000 description 1
- DJVKJGIZQFBFGS-UHFFFAOYSA-N n-[2-[2-(prop-2-enoylamino)ethyldisulfanyl]ethyl]prop-2-enamide Chemical compound C=CC(=O)NCCSSCCNC(=O)C=C DJVKJGIZQFBFGS-UHFFFAOYSA-N 0.000 description 1
- 150000007523 nucleic acids Chemical class 0.000 description 1
- 102000039446 nucleic acids Human genes 0.000 description 1
- 108020004707 nucleic acids Proteins 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
Landscapes
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP16125685A JPS6222754A (ja) | 1985-07-23 | 1985-07-23 | Ｎ，ｎ′−ジメタクリロイルシスタミン |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP16125685A JPS6222754A (ja) | 1985-07-23 | 1985-07-23 | Ｎ，ｎ′−ジメタクリロイルシスタミン |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6222754A JPS6222754A (ja) | 1987-01-30 |
| JPH0460467B2 true JPH0460467B2 (enrdf_load_stackoverflow) | 1992-09-28 |
Family
ID=15731630
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP16125685A Granted JPS6222754A (ja) | 1985-07-23 | 1985-07-23 | Ｎ，ｎ′−ジメタクリロイルシスタミン |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6222754A (enrdf_load_stackoverflow) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2764214B2 (ja) * | 1989-05-30 | 1998-06-11 | 旭サナック株式会社 | 割り型を用いた圧造方法及び装置 |
| EP1660153A2 (en) * | 2003-09-04 | 2006-05-31 | The United States of America as represented by the Department of Veterans Affairs | Hydrogel nanocompsites for ophthalmic applications |
-
1985
- 1985-07-23 JP JP16125685A patent/JPS6222754A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6222754A (ja) | 1987-01-30 |
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