JP7477911B2 - ハイブリッドエアロゲル及びその製造方法、並びにハイブリッドエアロゲルを用いた断熱材 - Google Patents

ハイブリッドエアロゲル及びその製造方法、並びにハイブリッドエアロゲルを用いた断熱材 Download PDF

Info

Publication number
JP7477911B2
JP7477911B2 JP2022536169A JP2022536169A JP7477911B2 JP 7477911 B2 JP7477911 B2 JP 7477911B2 JP 2022536169 A JP2022536169 A JP 2022536169A JP 2022536169 A JP2022536169 A JP 2022536169A JP 7477911 B2 JP7477911 B2 JP 7477911B2
Authority
JP
Japan
Prior art keywords
hollow
aerogel
particles
hollow particles
hybrid aerogel
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2022536169A
Other languages
English (en)
Japanese (ja)
Other versions
JPWO2022014194A1 (https=
Inventor
ラダー ウー
官益 李
リベラ レイモンド ビルトダゾ
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
National Institute for Materials Science
Original Assignee
National Institute for Materials Science
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by National Institute for Materials Science filed Critical National Institute for Materials Science
Publication of JPWO2022014194A1 publication Critical patent/JPWO2022014194A1/ja
Application granted granted Critical
Publication of JP7477911B2 publication Critical patent/JP7477911B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/157After-treatment of gels
    • C01B33/158Purification; Drying; Dehydrating
    • C01B33/1585Dehydration into aerogels
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/0091Preparation of aerogels, e.g. xerogels
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B30/00Compositions for artificial stone, not containing binders
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/0045Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by a process involving the formation of a sol or a gel, e.g. sol-gel or precipitation processes
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/30Particle morphology extending in three dimensions
    • C01P2004/32Spheres
    • C01P2004/34Spheres hollow
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/64Nanometer sized, i.e. from 1-100 nanometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/16Pore diameter
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16LPIPES; JOINTS OR FITTINGS FOR PIPES; SUPPORTS FOR PIPES, CABLES OR PROTECTIVE TUBING; MEANS FOR THERMAL INSULATION IN GENERAL
    • F16L59/00Thermal insulation in general
    • F16L59/06Arrangements using an air layer or vacuum

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Silicon Compounds (AREA)
  • Thermal Insulation (AREA)
JP2022536169A 2020-07-14 2021-06-04 ハイブリッドエアロゲル及びその製造方法、並びにハイブリッドエアロゲルを用いた断熱材 Active JP7477911B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2020120921 2020-07-14
JP2020120921 2020-07-14
PCT/JP2021/021299 WO2022014194A1 (ja) 2020-07-14 2021-06-04 ハイブリッドエアロゲル及びその製造方法、並びにハイブリッドエアロゲルを用いた断熱材

Publications (2)

Publication Number Publication Date
JPWO2022014194A1 JPWO2022014194A1 (https=) 2022-01-20
JP7477911B2 true JP7477911B2 (ja) 2024-05-02

Family

ID=79555175

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2022536169A Active JP7477911B2 (ja) 2020-07-14 2021-06-04 ハイブリッドエアロゲル及びその製造方法、並びにハイブリッドエアロゲルを用いた断熱材

Country Status (6)

Country Link
US (1) US20230150825A1 (https=)
EP (1) EP4183744A4 (https=)
JP (1) JP7477911B2 (https=)
CN (1) CN115997083A (https=)
TW (1) TWI859454B (https=)
WO (1) WO2022014194A1 (https=)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7603924B2 (ja) * 2020-11-20 2024-12-23 国立研究開発法人物質・材料研究機構 断熱配管
JP7607955B2 (ja) * 2020-11-20 2025-01-06 国立研究開発法人物質・材料研究機構 エアロゲル粉末の製造方法及びこれを用いた断熱材
CN113526912B (zh) * 2021-07-01 2023-02-17 中广核研究院有限公司 稀土基气凝胶复合材料及其制备方法和应用

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005525454A (ja) 2002-05-15 2005-08-25 キャボット コーポレイション エーロゲルと中空粒子バインダーの組成物、絶縁複合材料、及びそれらの製造方法
US20140059971A1 (en) 2011-03-18 2014-03-06 Bjørn Petter Jelle Thermal insulation materials
WO2017038646A1 (ja) 2015-08-28 2017-03-09 日立化成株式会社 エアロゲル複合体及び断熱材
US20170160001A1 (en) 2015-12-08 2017-06-08 Whirlpool Corporation Insulation structure for an appliance having a uniformly mixed multi-component insulation material, and a method for even distribution of material combinations therein
CN108689680A (zh) 2018-05-30 2018-10-23 巩义市泛锐熠辉复合材料有限公司 一种高效隔热保温气凝胶毡的制备方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH587979A5 (https=) * 1976-02-06 1977-05-31 Sulzer Ag
GB2048847B (en) * 1978-08-28 1983-07-06 Torobin Leonard B Method and apparatus for producing hollow microspheres
AUPR554501A0 (en) * 2001-06-07 2001-07-12 Lehmann Pacific Solar Pty Limited Radiative cooling surface coatings
CN1329333C (zh) * 2004-11-29 2007-08-01 北京科技大学 一种硅酸钙复合纳米孔超级绝热材料的制备方法
JP5615514B2 (ja) 2008-05-15 2014-10-29 ニチアス株式会社 断熱材、これを用いた断熱構造及び断熱材の製造方法
US9650500B2 (en) * 2010-11-15 2017-05-16 Dow Global Technologies Llc Nanoporous particles in a hollow latex matrix
CN105110339A (zh) * 2015-06-23 2015-12-02 北京建工新型建材有限责任公司 一种低成本柔性二氧化硅气凝胶的制备方法
CN108778996A (zh) * 2016-03-25 2018-11-09 日立化成株式会社 溶胶组合物、气凝胶复合体、带有气凝胶复合体的支撑构件和绝热材
JP2018130933A (ja) 2017-02-17 2018-08-23 日立化成株式会社 積層複合体及び断熱材
JP6932572B2 (ja) 2017-07-13 2021-09-08 株式会社トクヤマ 球状シリカエアロゲル、その製造方法、及び、その用途

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005525454A (ja) 2002-05-15 2005-08-25 キャボット コーポレイション エーロゲルと中空粒子バインダーの組成物、絶縁複合材料、及びそれらの製造方法
US20140059971A1 (en) 2011-03-18 2014-03-06 Bjørn Petter Jelle Thermal insulation materials
WO2017038646A1 (ja) 2015-08-28 2017-03-09 日立化成株式会社 エアロゲル複合体及び断熱材
US20170160001A1 (en) 2015-12-08 2017-06-08 Whirlpool Corporation Insulation structure for an appliance having a uniformly mixed multi-component insulation material, and a method for even distribution of material combinations therein
CN108689680A (zh) 2018-05-30 2018-10-23 巩义市泛锐熠辉复合材料有限公司 一种高效隔热保温气凝胶毡的制备方法

Also Published As

Publication number Publication date
US20230150825A1 (en) 2023-05-18
CN115997083A (zh) 2023-04-21
JPWO2022014194A1 (https=) 2022-01-20
TW202227361A (zh) 2022-07-16
WO2022014194A1 (ja) 2022-01-20
TWI859454B (zh) 2024-10-21
EP4183744A4 (en) 2025-06-18
EP4183744A1 (en) 2023-05-24

Similar Documents

Publication Publication Date Title
JP7477911B2 (ja) ハイブリッドエアロゲル及びその製造方法、並びにハイブリッドエアロゲルを用いた断熱材
Lin et al. Formation of hollow silica nanospheres by reverse microemulsion
Li et al. Synthesis of stable hollow silica microspheres with mesoporous shell in nonionic W/O emulsion
TWI531534B (zh) 金屬氧化物粉末及其製造方法
JP4994360B2 (ja) アルコキシシラン基で修飾したシリカ/ラテックスハイブリッドからなるモノリシックキセロゲル及びエーロゲルの臨界未満の条件下における製造方法。
US10544049B2 (en) Process for preparing a porous inorganic powder
CN104556057A (zh) 一种纳米多孔轻质二氧化硅微球的制备方法
US11951453B2 (en) Superficially porous particles and methods for forming superficially porous particles
KR20190098728A (ko) 소수성의 실리카 에어로겔 과립의 제조방법
JP2008208019A (ja) 多孔質材及びその調製方法
KR20250117475A (ko) 도액, 복합 재료 및 도막
US20230357525A1 (en) Aerogel powder manufacturing method and thermal insulation material using the same
CN104587922A (zh) 一种二氧化钛二氧化硅复合纳米多孔微球的制备方法
JP5145638B2 (ja) 樹脂組成物
Zhao et al. Microfluidic synthesis of monodisperse hierarchical silica particles with raspberry-like morphology
JP2018518438A (ja) 有機修飾エアロゲルの製造方法
CN104355313B (zh) 一种二氧化硅疏水多孔材料的简易制备方法
EP3259232A1 (en) Aerogels
US20060088470A1 (en) Inorganic beads with hierarchical pore structures
El-Safty Review on the key controls of designer copolymer-silica mesophase monoliths (HOM-type) with large particle morphology, ordered geometry and uniform pore dimension
KR101889474B1 (ko) 실리카 기공 구조체 및 그 제조 방법
JP7259857B2 (ja) 塗液の製造方法、塗液及び塗膜
JP2013237593A (ja) シリカナノ中空粒子の製造方法
CN104138733A (zh) 一种表面具有贯穿大孔的二氧化硅空心微球及其制备方法
JP2002274835A (ja) 多孔質シリカ発泡体およびその製造方法

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20221206

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20231220

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20240214

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20240401

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20240412

R150 Certificate of patent or registration of utility model

Ref document number: 7477911

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150