JP6970280B2 - 有機溶剤精製システム及び方法 - Google Patents
有機溶剤精製システム及び方法 Download PDFInfo
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- JP6970280B2 JP6970280B2 JP2020511679A JP2020511679A JP6970280B2 JP 6970280 B2 JP6970280 B2 JP 6970280B2 JP 2020511679 A JP2020511679 A JP 2020511679A JP 2020511679 A JP2020511679 A JP 2020511679A JP 6970280 B2 JP6970280 B2 JP 6970280B2
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- organic solvent
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- 239000003960 organic solvent Substances 0.000 title claims description 148
- 238000000746 purification Methods 0.000 title claims description 36
- 238000000034 method Methods 0.000 title claims description 24
- 238000004821 distillation Methods 0.000 claims description 71
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 56
- 239000007788 liquid Substances 0.000 claims description 36
- 239000011259 mixed solution Substances 0.000 claims description 32
- 238000001704 evaporation Methods 0.000 claims description 30
- 239000006200 vaporizer Substances 0.000 claims description 30
- 230000003204 osmotic effect Effects 0.000 claims description 29
- 239000012528 membrane Substances 0.000 claims description 28
- 238000009834 vaporization Methods 0.000 claims description 25
- 230000008016 vaporization Effects 0.000 claims description 25
- 230000008020 evaporation Effects 0.000 claims description 24
- 238000010438 heat treatment Methods 0.000 claims description 21
- 238000009835 boiling Methods 0.000 claims description 19
- 238000000926 separation method Methods 0.000 claims description 17
- 238000007738 vacuum evaporation Methods 0.000 claims description 13
- 238000011084 recovery Methods 0.000 claims description 9
- 238000007670 refining Methods 0.000 claims description 7
- 239000007791 liquid phase Substances 0.000 claims description 4
- 239000012071 phase Substances 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims 1
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 description 147
- 239000012535 impurity Substances 0.000 description 19
- 239000007864 aqueous solution Substances 0.000 description 11
- 239000000126 substance Substances 0.000 description 11
- 230000006837 decompression Effects 0.000 description 10
- 239000011550 stock solution Substances 0.000 description 10
- 239000010457 zeolite Substances 0.000 description 9
- 229910021536 Zeolite Inorganic materials 0.000 description 8
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 8
- 239000007789 gas Substances 0.000 description 8
- 238000005265 energy consumption Methods 0.000 description 7
- 238000005342 ion exchange Methods 0.000 description 7
- 239000010419 fine particle Substances 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 5
- 238000001471 micro-filtration Methods 0.000 description 5
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 4
- 239000003463 adsorbent Substances 0.000 description 4
- 230000007423 decrease Effects 0.000 description 4
- 238000007599 discharging Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 3
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 3
- 239000003456 ion exchange resin Substances 0.000 description 3
- 229920003303 ion-exchange polymer Polymers 0.000 description 3
- 229910001416 lithium ion Inorganic materials 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000012466 permeate Substances 0.000 description 3
- 239000002002 slurry Substances 0.000 description 3
- ARXJGSRGQADJSQ-UHFFFAOYSA-N 1-methoxypropan-2-ol Chemical compound COCC(C)O ARXJGSRGQADJSQ-UHFFFAOYSA-N 0.000 description 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 229910002092 carbon dioxide Inorganic materials 0.000 description 2
- 239000001569 carbon dioxide Substances 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000007872 degassing Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 238000005292 vacuum distillation Methods 0.000 description 2
- 239000012808 vapor phase Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 239000003125 aqueous solvent Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- JYIMWRSJCRRYNK-UHFFFAOYSA-N dialuminum;disodium;oxygen(2-);silicon(4+);hydrate Chemical compound O.[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Na+].[Na+].[Al+3].[Al+3].[Si+4] JYIMWRSJCRRYNK-UHFFFAOYSA-N 0.000 description 1
- 239000002612 dispersion medium Substances 0.000 description 1
- 239000007772 electrode material Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- LLHKCFNBLRBOGN-UHFFFAOYSA-N propylene glycol methyl ether acetate Chemical compound COCC(C)OC(C)=O LLHKCFNBLRBOGN-UHFFFAOYSA-N 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/02—Evaporators with heating coils
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/02—Treatment of water, waste water, or sewage by heating
- C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/02—Treatment of water, waste water, or sewage by heating
- C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
- C02F1/06—Flash evaporation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D207/00—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom
- C07D207/02—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D207/18—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member
- C07D207/22—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D207/24—Oxygen or sulfur atoms
- C07D207/26—2-Pyrrolidones
- C07D207/263—2-Pyrrolidones with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to other ring carbon atoms
- C07D207/267—2-Pyrrolidones with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to other ring carbon atoms with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to the ring nitrogen atom
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Chemistry (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Heat Treatment Of Water, Waste Water Or Sewage (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2018072077 | 2018-04-04 | ||
JP2018072077 | 2018-04-04 | ||
PCT/JP2019/010767 WO2019193951A1 (ja) | 2018-04-04 | 2019-03-15 | 有機溶剤精製システム及び方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPWO2019193951A1 JPWO2019193951A1 (ja) | 2021-03-11 |
JP6970280B2 true JP6970280B2 (ja) | 2021-11-24 |
Family
ID=68100522
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2020511679A Active JP6970280B2 (ja) | 2018-04-04 | 2019-03-15 | 有機溶剤精製システム及び方法 |
Country Status (3)
Country | Link |
---|---|
JP (1) | JP6970280B2 (zh) |
CN (1) | CN111971255B (zh) |
WO (1) | WO2019193951A1 (zh) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2022224768A1 (ja) * | 2021-04-20 | 2022-10-27 | オルガノ株式会社 | 電極活物質の洗浄方法、電池、電極及び電極活物質の製造方法、並びに混合物製造システム |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4118787A1 (de) * | 1991-06-07 | 1992-12-24 | Sihi Gmbh & Co Kg | Prozessintegriertes betriebsfluessigkeitsreinigungssystem fuer verdichter |
DE4303528A1 (de) * | 1993-02-06 | 1994-08-11 | Basf Ag | Verfahren zum Trennen von Flüssigkeitsgemischen mit azeotropem Siedeverhalten durch Verschaltung von Pervaporation und Destillation |
JPH06254597A (ja) * | 1993-03-08 | 1994-09-13 | Mitsui Eng & Shipbuild Co Ltd | 芳香族化合物含有排水の処理方法 |
CN1750867A (zh) * | 2003-02-21 | 2006-03-22 | 株式会社物产纳米技术研究所 | 水溶性有机物的浓缩方法 |
JP5911228B2 (ja) * | 2011-07-12 | 2016-04-27 | オルガノ株式会社 | 電極製造工程におけるnmp精製システム |
JP5793157B2 (ja) * | 2013-03-04 | 2015-10-14 | 日本リファイン株式会社 | 溶液処理装置 |
JP6440156B2 (ja) * | 2014-07-29 | 2018-12-19 | オルガノ株式会社 | 有機溶剤精製システム及び方法 |
CN104707549B (zh) * | 2015-03-19 | 2016-09-14 | 张汉文 | 一种从有机试剂废液中回收色谱级有机试剂的装置及方法 |
CN107803319A (zh) * | 2017-11-13 | 2018-03-16 | 林州朗坤科技有限公司 | 一种nmp回收提纯系统及其回收提纯方法 |
-
2019
- 2019-03-15 WO PCT/JP2019/010767 patent/WO2019193951A1/ja active Application Filing
- 2019-03-15 JP JP2020511679A patent/JP6970280B2/ja active Active
- 2019-03-15 CN CN201980024433.1A patent/CN111971255B/zh active Active
Also Published As
Publication number | Publication date |
---|---|
CN111971255B (zh) | 2022-07-08 |
JPWO2019193951A1 (ja) | 2021-03-11 |
WO2019193951A1 (ja) | 2019-10-10 |
CN111971255A (zh) | 2020-11-20 |
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